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inquiry2,2,4,4,6,6-hexaamino-2,2,4,4,6,6-hexahydro-1,3,5,2,4,6-triazatriphosphorine CAS:13597-92-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical
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inquiryProduct Name: 2,2,4,4,6,6-hexaamino-2,2,4,4,6,6-hexahydro-1,3,5,2,4,6-triazatriphosphorine Synonyms: 2,2,4,4,6,6-hexaamino-2,2,4,4,6,6-hexahydro-1,3,5,2,4,6-triazatriphosphorine;1,3,5,2,4,6-Triazatriphosphorine-2,2,4,4,6,6-hexaamine;2,2,4,4,6,6-He
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inquiry2l5,4l5,6l5-1,3,5,2,4,6-Triazatriphosphorine-2,2,4,4,6,6-hexamine cas 13597-92-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry2,2,4,4,6,6-HEXAAMINO-2,2,4,4,6,6-HEXAHYDRO-1,3,5,2,4,6-TRIAZATRIPHOSPHORINEAppearance:Pls see the Details Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediate
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inquiryHigh Quality Best Price Storage:Store in dry, dark and ventilated place Application:Chemical Synthesis Intermediate
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine
ammonia
A
hexaaminocyclotriphosphazene
Conditions | Yield |
---|---|
In neat (no solvent) direct react. of (PNCl2)3 with a large excess of liquid NH3 under pressure; react. completed after 48 h;; | A 36% B n/a |
In neat (no solvent) direct react. of (PNCl2)3 with a large excess of liquid NH3 under pressure; react. completed after 48 h;; | A 36% B n/a |
In benzene passing gaseous NH3 in a soln. of (NPCl2)3 in C6H6 for a longer period of time; formation of a mixt. of P3N3(NH2)6 and NH4Cl;; |
phosphorus pentachloride
ammonia
A
hexaaminocyclotriphosphazene
Conditions | Yield |
---|---|
In chloroform addn. of a soln. of PCl5 in CHCl3 to an excess of liquid NH3 at -50 °C;; extraxtion with liquid NH3;; | |
In chloroform addn. of a soln. of PCl5 in CHCl3 to an excess of liquid NH3 at -50 °C;; extraxtion with liquid NH3;; |
phosphorus pentachloride
ammonia
B
hexaaminocyclotriphosphazene
C
P4N12H16
Conditions | Yield |
---|---|
In not given react. of PCl5 with NH3;; |
phosphorus pentachloride
ammonia
A
hexaaminocyclotriphosphazene
B
P4N12H16
Conditions | Yield |
---|---|
In not given react. of PCl5 with NH3; formation of P4N4(NH2)8 and P3N3(NH2)6 as decompn. products of intermediate P(NH2)5;; | |
In not given react. of PCl5 with NH3; formation of an excess of P3N3(NH2)6, P4N4(NH2)8 and higher polymers as decompn. products of intermediate P(NH2)5;; | |
In not given react. of PCl5 with NH3; formation of P4N4(NH2)8 and P3N3(NH2)6 as decompn. products of intermediate P(NH2)5;; | |
In not given react. of PCl5 with NH3; formation of an excess of P3N3(NH2)6, P4N4(NH2)8 and higher polymers as decompn. products of intermediate P(NH2)5;; |
2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine
ammonia
hexaaminocyclotriphosphazene
hexaaminocyclotriphosphazene
Conditions | Yield |
---|---|
With KNH2 In ammonia NH3 (liquid); High Pressure; react. of semi ammoniate and KNH2 (molar ratio 1:12), 130°C, 110 bar, 5d; |
Conditions | Yield |
---|---|
In water hydrolysis;; | |
In water hydrolysis;; |
hexaaminocyclotriphosphazene
Conditions | Yield |
---|---|
In neat (no solvent) heating in vac. at 380°C for 100 h;; | >99 |
In neat (no solvent) heating for a longer period of time;; | |
In neat (no solvent) heating in vac. at 220°C for several days;; | >99 |
Conditions | Yield |
---|---|
In neat (no solvent) evolution of NH3 on air starting at 125 °C;; | |
In neat (no solvent) heating; decompn. rate depending on material of the vessel;; | |
In neat (no solvent) evolution of NH3 on air starting at 125 °C;; | |
In neat (no solvent) heating in vacuum at 380 °C for 100 h; evolution of NH3 starting in vacuum at 40 °C; evolution of a large amount of NH3 at 200-300 °C; no evolution of NH3 at 400-450 °C;; |
hexaaminocyclotriphosphazene
phosphoric acid
Conditions | Yield |
---|---|
With HNO3 or acetic acid; H2O In water hydrolysis with acetic acid or diluted HNO3;; | |
With H2O In water hydrolysis in the heat;; |
hexaaminocyclotriphosphazene
B
ammonium dihydrogen phosphate
Conditions | Yield |
---|---|
With H2SO4 In not given react. with H2SO4; formation of a mixture of NH4H2PO4 and (NH4)2SO4 and white vapors of volatile N compounds;; |
hexaaminocyclotriphosphazene
ammonia
Conditions | Yield |
---|---|
With sodium hydroxide In not given heating with an excess of NaOH soln.; evolution of 3 mol NH3/mol P3N3(NH2)6;; | |
With NaOH In not given heating with an excess of NaOH soln.; evolution of 3 mol NH3/mol P3N3(NH2)6;; |
Conditions | Yield |
---|---|
In acetic acid evolution of N2 by react. of NaNO2 with a soln. in abs. glacial acetic acid;; | |
In acetic acid evolution of N2 by react. of NaNO2 with a soln. in abs. glacial acetic acid;; |
Conditions | Yield |
---|---|
In acetone stirring (6-12 h), Hg:hexaaminocyclotriphosphazene ratio 6-12; washing (acetone), drying in air; elem. anal.; |
hexaaminocyclotriphosphazene
mercury(II) diacetate
Conditions | Yield |
---|---|
In acetone stirring (6-12 h), Hg:hexaaminocyclotriphosphazene ratio 2-3; washing (acetone), drying in air; elem. anal.; |
hexaaminocyclotriphosphazene
mercury(II) diacetate
Conditions | Yield |
---|---|
In acetone stirring (2-28 h) in eqimolar ratio; washing (acetone), drying in air; elem. anal.; |
Conditions | Yield |
---|---|
In not given react. with methanol forming PNNH4OH and PN(NH2)(NHCH3) (molar ratio 3:10);; | |
In not given react. with methanol forming PNNH4OH and PN(NH2)(NHCH3) (molar ratio 3:10);; |
hexaaminocyclotriphosphazene
P3N9H12*H2O
Conditions | Yield |
---|---|
In water pptn. of aq. P3N3(NH2)6 with the same volume of alcohol or on evaporating at ambient temp.;; |
Conditions | Yield |
---|---|
In neat (no solvent) |
Conditions | Yield |
---|---|
In neat (no solvent) |
hexaaminocyclotriphosphazene
cobalt(II) chloride
Conditions | Yield |
---|---|
In neat (no solvent) |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: NH4Cl; 24-72 h, 250-750°C; sublimation, boiling (conc. HCl), washing (H2O); |
Conditions | Yield |
---|---|
In neat (no solvent) |
Conditions | Yield |
---|---|
In neat (no solvent) |
Conditions | Yield |
---|---|
In neat (no solvent) |
Conditions | Yield |
---|---|
In neat (no solvent) |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: NH4Cl; 72 h, 700°C; sublimation, boiling (conc. HCl), washing (H2O); |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: NH4Cl; 72 h, 700°C; sublimation, boiling (conc. HCl), washing (H2O); |
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