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inquiryItems Standard Result Appearance A clear intense yellow, viscous, oily liquid Conforms Assay ≥
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inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White powder Storage:Cool dry place Package:1kg/foill bag;25kg/drum Application:pharmaceut
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1186.html Product Name Methyl 6-methyl-2-pyridinecarboxylate CAS No.
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquirymethyl 6-methylpyridine-2-carboxylate Basic information Product Name: methyl 6-methylpyridine-2-carboxylate Synonyms: methyl 6-methylpyridine-2-carboxylate;2-Pyridi
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, in
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryCAS: 13602-11-4 MF: C8H9NO2 MW: 151.16 EINECS: 237-085-0 Mol File: 13602-11-4.mol methyl 6-methylpyridine-2-carboxylate Structure methyl 6-methylpyridine-2-carboxylate Chemical Properties Melting point 18 °C Boiling point
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryTAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryMethyl 6-methyl-2-pyridinecarboxylate cas 13602-11-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquirymethanol
6-methyl-2-pyridinecarboxylic acid
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: methanol In thionyl chloride at -10 - 20℃; for 1h; Stage #2: 6-methyl-2-pyridinecarboxylic acid In thionyl chloride at 80℃; for 5h; Time; | 93% |
Stage #1: methanol; 6-methyl-2-pyridinecarboxylic acid With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; Stage #2: at 20℃; for 6h; | 92% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 6h; | 92% |
6-methyl-2-pyridinecarboxylic acid
diazomethyl-trimethyl-silane
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
In methanol; diethyl ether; dichloromethane at 20℃; for 0.5h; | 91% |
2-bromo-6-methylpyridine
methanol
carbon monoxide
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine; palladium diacetate at 65℃; | 60% |
diazomethane
6-methyl-2-pyridinecarboxylic acid
6-methylpicolinic acid methyl ester
methanol
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
With sulfuric acid |
methanol
6-methyl-pyridine-2-carbonyl chloride
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
With sodium methylate for 4h; Inert atmosphere; Reflux; |
6-methyl-2-pyridinecarboxylic acid
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / 1 h / Inert atmosphere; Reflux 2: sodium methylate / 4 h / Inert atmosphere; Reflux View Scheme |
carbon dioxide
2-methyl-6-(trimethylsilyl)-pyridine
methyl iodide
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
With tetrabutylammonium triphenyldifluorosilicate In tetrahydrofuran-d8 at 20℃; under 750.075 Torr; for 18h; Inert atmosphere; Schlenk technique; | > 97 %Spectr. |
2-bromo-6-methylpyridine
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C / Inert atmosphere; Schlenk technique 1.2: 18 h / -78 - 20 °C / Inert atmosphere; Schlenk technique 2.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran-d8 / 18 h / 20 °C / 750.08 Torr / Inert atmosphere; Schlenk technique View Scheme |
2,6-dimethylpyridine
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium permanganate / water-d2 / 5 h / 20 - 60 °C 2.1: thionyl chloride / 1 h / -10 - 20 °C 2.2: 5 h / 80 °C View Scheme |
6-hydroxy-2-methylpyridine
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: fluorosulfonyl fluoride; triethylamine / dichloromethane / 24 h / 20 °C / 760.05 Torr 2: bis(triphenylphosphine)nickel(II) chloride; 2.9-dimethyl-1,10-phenanthroline; manganese / N,N-dimethyl-formamide / 20 h / 20 °C / 760.05 Torr / Schlenk technique; Inert atmosphere; Glovebox 3: methanol View Scheme |
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: bis(triphenylphosphine)nickel(II) chloride; 2.9-dimethyl-1,10-phenanthroline; manganese / N,N-dimethyl-formamide / 20 h / 20 °C / 760.05 Torr / Schlenk technique; Inert atmosphere; Glovebox 2: methanol View Scheme |
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
With platinum(IV) oxide; palladium 10% on activated carbon; hydrogen; acetic acid at 20℃; for 24h; | 97% |
6-methylpicolinic acid methyl ester
6-methyl-2-picolinic acid hydrazide
Conditions | Yield |
---|---|
With hydrazine In methanol at 20℃; for 0.5h; | 94% |
With hydrazine In methanol at 20℃; for 18h; | 93% |
With hydrazine hydrate In ethanol for 1.5h; Reflux; | 71% |
6-methylpicolinic acid methyl ester
methylamine
N,6-dimethylpyridine-2-carboxamide
Conditions | Yield |
---|---|
In methanol at 20℃; for 72h; | 92% |
3,3-dimethyl-butan-2-one
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: 3,3-dimethyl-butan-2-one With sodium hydride In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere; Schlenk technique; Reflux; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran; mineral oil for 4h; Reflux; Inert atmosphere; Schlenk technique; Further stages; | 85% |
6-methylpicolinic acid methyl ester
4-methylquinoline-6-carbonitrile
4-(2-(6-methylpyridin-2-yl)-2-oxoethyl)quinoline-6-carbonitrile
Conditions | Yield |
---|---|
Stage #1: 4-methylquinoline-6-carbonitrile With sodium t-butanolate In tetrahydrofuran at 5 - 25℃; for 0.5h; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at 20 - 25℃; for 2.33333 - 2.66667h; Product distribution / selectivity; | 81% |
methanol
6-methylpicolinic acid methyl ester
4,6-dimethyl-pyridine-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With Ethyl 2-mercaptopropionate; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; toluene-4-sulfonic acid In dimethyl sulfoxide at 23℃; UV-irradiation; | 81% |
6-methylpicolinic acid methyl ester
3,5-dimethyl-4-nitro-1H-pyrazole
methyl 6-(bromomethyl)picolinate
Conditions | Yield |
---|---|
Stage #1: 6-methylpicolinic acid methyl ester With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane at 70℃; for 2h; Stage #2: 3,5-dimethyl-4-nitro-1H-pyrazole With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 12h; | 79% |
2-methyl-[1,5]naphthyridine
6-methylpicolinic acid methyl ester
1-(6-methylpyridin-2-yl)-2-(1,5-naphthyridin-2-yl)ethan-1-one
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In tetrahydrofuran; toluene at -78 - 20℃; for 21h; | 76% |
With potassium hexamethylsilazane In tetrahydrofuran; toluene at -78 - 21℃; for 21h; Inert atmosphere; | 30.5% |
With potassium hexamethylsilazane In tetrahydrofuran; toluene at -78 - 21℃; for 21h; Inert atmosphere; | 30.5% |
With potassium hexamethylsilazane In tetrahydrofuran; toluene at -78 - 21℃; for 21h; Inert atmosphere; | 30.5% |
With potassium hexamethylsilazane In tetrahydrofuran; toluene at -78 - 21℃; for 21.0833h; Inert atmosphere; | 30.5% |
2-acetyl-6-methylpyridine
6-methylpicolinic acid methyl ester
1,3-bis-(6-methyl-pyridin-2-yl)-propane-1,3-dione
Conditions | Yield |
---|---|
With sodium ethanolate In toluene | 75% |
6-methylpicolinic acid methyl ester
acetophenone
2-methyl-6-(5-phenyl-1H-pyrazol-3-yl)pyridine
Conditions | Yield |
---|---|
Stage #1: acetophenone With sodium hydride In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere; Schlenk technique; Reflux; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran; mineral oil for 4h; Reflux; Inert atmosphere; Schlenk technique; Further stages; | 75% |
6-methylpicolinic acid methyl ester
4-methyl-6-bromoquinoline
Conditions | Yield |
---|---|
Stage #1: 6-bromo-4-methylquinoline With potassium hexamethylsilazane In tetrahydrofuran at -70 - -65℃; for 3h; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at -70 - 20℃; for 7h; | 73.8% |
Stage #1: 6-bromo-4-methylquinoline With sodium hexamethyldisilazane In tetrahydrofuran at -78℃; for 3h; Inert atmosphere; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at -78 - 20℃; Inert atmosphere; | 53% |
Stage #1: 6-bromo-4-methylquinoline With potassium hexamethylsilazane In tetrahydrofuran at -65 - -60℃; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at -65 - -60℃; Further stages.; | 50% |
2-Bromo-4-picoline
6-methylpicolinic acid methyl ester
2-(2-bromopyridin-4-yl)-1-(6-methylpyridin-2-yl)ethan-1-one
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran at -30 - 20℃; | 70% |
Stage #1: 2-Bromo-4-picoline With sodium hexamethyldisilazane In tetrahydrofuran at -30℃; for 1h; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at 20℃; | 70% |
Stage #1: 2-Bromo-4-picoline With sodium hexamethyldisilazane In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at 21℃; for 16h; Inert atmosphere; | 65.4% |
6-methylpicolinic acid methyl ester
4-methyl-6-(trifluoromethoxy)quinoline
1-(6-methylpyridin-2-yl)-2-(6-(trifluoromethoxy)quinolin-4-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: 4-methyl-6-(trifluoromethoxy)quinoline With potassium hexamethylsilazane In tetrahydrofuran at -65 - -60℃; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at -65 - -60℃; Further stages.; | 69% |
6-methylpicolinic acid methyl ester
2-acetyl-6-methylpyridine
Conditions | Yield |
---|---|
With sodium ethanolate In ethyl acetate Acidic conditions; | 68% |
6-methylpicolinic acid methyl ester
methyl 6-(bromomethyl)picolinate
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane for 5h; Reflux; | 66% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane at 48℃; for 5h; Wohl-Ziegler Bromination; | 66% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In tetrachloromethane for 12h; Inert atmosphere; Reflux; | 51.3% |
6-methylpicolinic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: 7-bromo-4-methylquinoline With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 0.666667h; Stage #2: 6-methylpicolinic acid methyl ester In tetrahydrofuran at -78℃; for 2h; Stage #3: at 0 - 20℃; for 2h; | 66% |
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