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manganese (II) acetate tetrahydrate
phthalonitrile
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
In ethanol at 190℃; for 3h; Autoclave; High pressure; Green chemistry; | 45% |
In ethanol at 190℃; for 1h; Temperature; Solvent; Autoclave; | 40% |
Conditions | Yield |
---|---|
With (NH4)2Mo2O7 In neat (no solvent) other Radiation; mixt. of O-phthalic anhydride, urea, metal salt and (NH4)2Mo2O7 irradiated in microwave oven at 460W for 8 min. the at 800W for 8 min, cooling to room temp.; washed (H2O, acetone, MeOH, 6M HCl), reflux with acetone, MeOH and CHCl3resp. about 12 h; elem. anal.; | 31% |
Conditions | Yield |
---|---|
With I2 In neat (no solvent) tube was loaded with ligand, Mn, I2 and (NH4)6Mo7O24*4H2O under N2, tube was immersed in a 300°C salt bath, after a few min mixt. was solidified, mixt. was left at 300°C for 6 h, cooled; powder was sublimed in a tube furnace in vac. over 2 d at 480°C, crude ppt. was resublimed in vac. at <=460°C (caution: unsublimed material is pyrophoric); elem. anal.; | 21% |
oxovanadium phthalocyanine
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
With imidazole In N,N-dimethyl acetamide soln. of complex in DMA was degassed, imidazole was added, 10 min; product was not isolated; analyzed by ESR or UV; |
Conditions | Yield |
---|---|
In not given react. of phthalonitrile with Mn(2+); washing, sublimation; |
Conditions | Yield |
---|---|
In methanol React. at 65-100°C, 9-11.5 kbar for 1.75-18 h in presence of hydroquinone.; Extg. with MeOH and acetone, sublimed in vac.; | 2-50 |
Mn(OH)-phthalocyanine
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
In not given Irradiation (UV/VIS); |
(phthalocyaninato)bis(pyridine)manganese(II)
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
In neat (no solvent) above 180°C; |
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
In tetrahydrofuran; N,N-dimethyl-formamide Irradiation (UV/VIS); |
Conditions | Yield |
---|---|
With ammonium heptamolybdate; urea Microwave irradiation; |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In pentan-1-ol at 140℃; for 2h; Inert atmosphere; | 162 mg |
Tetrafluorophthalonitrile
manganese (II) acetate tetrahydrate
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
at 250℃; for 3h; Inert atmosphere; | 613 mg |
manganese (II) acetate tetrahydrate
29H,31H-Phthalocyanine
manganese(II) phthalocyanin
Conditions | Yield |
---|---|
With tributyl-amine In pentan-1-ol at 160℃; for 2h; Inert atmosphere; | 12 mg |
manganese(II) phthalocyanin
[2-(dimethylamino)ethyl]trimethylazanium iodide
fullerene-C60
1,2-dichloro-benzene
sodium thioethylate
Conditions | Yield |
---|---|
In benzonitrile (under inert atm.); C60, Na-salt, ligand, Mn-complex stirred in C6H4Cl2-C6H5CN 6:1 mixt. for 4 h at 60°C, cooled to 20°C; filtered, hexane layered, diffused for 1 month, solvent poured down, collected, washed with hexane; elem. anal.; | 50% |
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone
manganese(II) phthalocyanin
2,3,5,6-tetrafluoro-7,7',8,8'-tetracyanoquinodimethane
water
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 20℃; for 336h; | 49.1% |
Conditions | Yield |
---|---|
Stage #1: manganese(II) phthalocyanin; 1,2-dichloro-benzene at 100℃; for 6h; Glovebox; Stage #2: 4,4'-bipyridine In hexane Glovebox; | 48% |
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