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inquirysodium dimethyldithiocarbamate
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In chloroform; acetone mixing of Fe-complex (in CHCl3) with excess of Na2S2CNEt2 (in acetone); concn. (vac.), crystn. on EtOH addn., filtration, washing (EtOH); |
sodium dimethyldithiocarbamate
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In water iron(III) salt;; |
sodium dimethyldithiocarbamate
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In acetone addn. of excess NaS2CNMe2 to Fe-complex, stirring (room temp., 30 min); concn. (vac.), addn. of EtOH, concn. (vac., crystn.), filtration, washing (EtOH, acetone); elem. anal.; |
iron(II)
sodium dimethyldithiocarbamate
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In water iron(II) salt;; |
sodium dimethyldithiocarbamate
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In chloroform; acetone addn. of Fe-complex (in CHCl3) to excess of Na2S2CNMe2 (in acetone); pptn. on concn. (vac.), filtration; |
methylmercury(II) chloride
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In dichloromethane room temp., 10 min (pptn.); collection, washing (CH2Cl2), drying (vac., 100°C, several days); | 99% |
In benzene room temp., 10 min (pptn.); collection, washing (C6H6), drying (vac., 100°C, several days); elem. anal.; | 99% |
tris(N,N-dimethyldithiocarbamato)iron(III)
ethylmercury(II) chloride
Conditions | Yield |
---|---|
In benzene room temp., 10 min (pptn.); collection, washing (C6H6), drying (vac., 100°C, several days); | 99% |
In dichloromethane room temp., 10 min (pptn.); collection, washing (CH2Cl2), drying (vac., 100°C, several days); | 99% |
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
With oxalic acid In methanol; benzene Kinetics; kinetic runs at 30°C in MeOH-C6H6, at least 10-fold excess of oxalic acid over the complex; not isolated; measuring absorbance at 348 nm; |
tris(N,N-dimethyldithiocarbamato)iron(III)
sodium diethyldithiocarbamate trihydrate
Conditions | Yield |
---|---|
In acetone addn. of excess NaS2CNEt2 to Fe-complex; concn. (vac.), addn. of EtOH (pptn.), filtration, washing (EtOH), drying (70°C); |
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
addn. of diethyl ether;; elem. anal.;; |
iodine
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
In dichloromethane addn. of hexane, mixt. was left for 3 h, crystals were collected, washed with hexane, recrystd. from CH2Cl2-hexane mixt.; |
tris(N,N-dimethyldithiocarbamato)iron(III)
bis(N,N-dimethyldithiocarbamato)iron(III) diiodide
Conditions | Yield |
---|---|
With iodine In dichloromethane addn. of hexane, mixt. was left for 3 h, crystals were collected, washed with hexane, recrystd. from CH2Cl2-hexane mixt.; |
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
With iodomethane In further solvent(s) standing of Fe-complex in iodomethane (room temp., crystn.); recrystn. (CH2Cl2 or CH2Cl2/C6H6 or hexane), drying (vac., 80°C, several days); |
tris(N,N-dimethyldithiocarbamato)iron(III)
Conditions | Yield |
---|---|
With I2 In benzene addn. of excess I2 to soln. of Fe-complex; crystn. on standing, collection, washing (C6H6), recrystn. (CH2Cl2/C6H6), drying (vac., 80°C); elem. anal.; |
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