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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

1H,1H-2,5-BIS(TRIFLUOROMETHYL)-3,6-DIOXAPERFLUORONONANOL

Cas:14548-74-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1-Propanol,2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)propoxy]-

Cas:14548-74-4

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1H,1H-2,5-Di(trifluoromethyl)-3,6-dioxaundecafluorononanol

Cas:14548-74-4

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

1H,1H-2,5-DI(TRIFLUOROMETHYL)-3,6-DIOXAUNDECAFLUORONONANOL

Cas:14548-74-4

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

14548-74-4 CAS NO.14548-74-4

Cas:14548-74-4

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Name: 1Hforce 1Hlica 2je 5muri DI (TRIFLUOROMETHYL)-3meme 6copyright DIOXAUNDECAFLUORONONANOL. English synonym: 1HMJ 1HLFLUORO (2Jing 5mm DIMETHYLQ 3Met 6MJ Dioxanananlue 1LFOL); 1HMJ 1HMJ 2MY5HIXANONANLLYL); 1HMJ 1HMJ 5HIXANONANLL5 BIS (TRIFLUOR

1H,1H-2,5-Di(Trifluoromethyl)-3,6-dioxanonan-1-ol manufacture

Cas:14548-74-4

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1H,1H-2,5-Bis(trifluoromethyl)-3,6-dioxaperfluorononanol

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

14548-74-4

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1H,1H-2,5-DI(TRIFLUOROMETHYL)-3,6-DIOXAUNDECAFLUORONONANOL

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1H,1H-2,5-DI(TRIFLUOROMETHYL)-3,6-DIOXAUNDECAFLUORONONANOL

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#14548-74-4;CAT#A808378

Cas:14548-74-4

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

National Research Platform ISO 9001 14548-74-4

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

14548-74-4 CAS NO.14548-74-4

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

suzhou BetterBioChem Co., Ltd.

Betterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in

1H,1H-2,5-BIS(TRIFLUOROMETHYL)-3,6-DIOXAPERFLUORONONANOL

Cas:14548-74-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 1H,1H-2,5-DI(TRIFLUOROMETHYL)-3,6-DIOXAUNDECAFLUORONONANOL, CAS:14548-74-4 with the m

1H,1H-2,5-DI(TRIFLUOROMETHYL)-3,6-DIOXAUNDECAFLUORONONANOL

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Pure Chemistry Scientific Inc.

1-Propanol,2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(1,1,2,2,3,3,3-heptafluoropropoxy)propoxy]- Application:80063302

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

1H,1H-2,5-Di(trifluoromethyl)-3,6-dioxaundecafluorononanol

Cas:14548-74-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

Synthetic route

perfluoro-2,5-dimethyl-3,6-dioxanonanoyl fluoride
2641-34-1

perfluoro-2,5-dimethyl-3,6-dioxanonanoyl fluoride

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether at 20℃; for 2h; Inert atmosphere; Reflux;90%
Multi-step reaction with 2 steps
1: 86.3 percent / Na2CO3; MgSO4; silica gel / diethyl ether / 20 °C
2: 81.1 percent / NaBH4 / diethyl ether; methanol / 12 h / Heating
View Scheme
methyl 2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonanoate
26131-32-8

methyl 2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonanoate

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

Conditions
ConditionsYield
With sodium tetrahydroborate In methanol; diethyl ether for 12h; Heating;81.1%
With sodium tetrahydroborate In methanol; diethyl ether for 11h; Reflux; Inert atmosphere;75%
With sodium tetrahydroborate; isopropyl alcohol
With sodium tetrahydroborate In methanol at 20℃; for 2h; Cooling with ice;
2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl trifluoromethanesulfonate
1173110-39-8

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl trifluoromethanesulfonate

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

Conditions
ConditionsYield
With sodium hydride; phenol In dimethyl sulfoxide at 130℃; Inert atmosphere;
2,3,4,5,6-pentafluorostyrene
653-34-9

2,3,4,5,6-pentafluorostyrene

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C17H5F21O3

C17H5F21O3

Conditions
ConditionsYield
Stage #1: 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]propan-1-ol With sodium hydride In tetrahydrofuran at 20℃; Inert atmosphere;
Stage #2: 2,3,4,5,6-pentafluorostyrene In tetrahydrofuran at 0℃; Reflux; Inert atmosphere;
90%
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

2-(trifluoromethyl)acrylic chloride
90715-73-4

2-(trifluoromethyl)acrylic chloride

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(perfluoropropoxy)propoxy]propyl 2-(trifluoromethyl)acrylate

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(perfluoropropoxy)propoxy]propyl 2-(trifluoromethyl)acrylate

Conditions
ConditionsYield
Stage #1: 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]propan-1-ol With pyridine at -10℃; for 0.333333h; Inert atmosphere;
Stage #2: 2-(trifluoromethyl)acrylic chloride at -10 - 20℃; for 17h; Inert atmosphere;
85%
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

Methacryloyl chloride
920-46-7

Methacryloyl chloride

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl methacrylate

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl methacrylate

Conditions
ConditionsYield
With 2,2-diphenyl-1-picrylhydrazyl; triethylamine In diethyl ether at 20℃; for 4h;82%
3-Bromopropionic acid
590-92-1

3-Bromopropionic acid

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C12H6BrF17O4
820958-27-8

C12H6BrF17O4

Conditions
ConditionsYield
With trifluoroacetic anhydride at 20 - 30℃; for 4.5h;80%
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

1-Adamantanecarbonyl chloride
2094-72-6

1-Adamantanecarbonyl chloride

C20H17F17O4
709615-35-0

C20H17F17O4

Conditions
ConditionsYield
With pyridine at 20 - 50℃; for 5h;74.4%
With pyridine at 25 - 50℃; for 5h;74.4 %Spectr.
trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl trifluoromethanesulfonate
1173110-39-8

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl trifluoromethanesulfonate

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere;70.2%
With pyridine In dichloromethane Inert atmosphere;70%
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C9H2Cl2F17O4P
1429405-66-2

C9H2Cl2F17O4P

Conditions
ConditionsYield
With lithium chloride; trichlorophosphate63%
vinyl acetate
108-05-4

vinyl acetate

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

1,1-Dihydro-2,5-bis(trifluoromethyl)-3,6-dioxa-2,4,4,5,7,7,8,8,9,9,9,-undecafluorononyl vinyl ether

1,1-Dihydro-2,5-bis(trifluoromethyl)-3,6-dioxa-2,4,4,5,7,7,8,8,9,9,9,-undecafluorononyl vinyl ether

Conditions
ConditionsYield
With sulfuric acid; mercury(II) diacetate at 0 - 10℃; for 8h;30%
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

1,1-Dihydro-2,5-bis(trifluoromethyl)-3,6-dioxa-2,4,4,5,7,7,8,8,9,9,9,-undecafluorononyl 1,2-dichloroethyl ether
156731-88-3

1,1-Dihydro-2,5-bis(trifluoromethyl)-3,6-dioxa-2,4,4,5,7,7,8,8,9,9,9,-undecafluorononyl 1,2-dichloroethyl ether

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 30 percent / mercuric acetate, conc. H2SO4 / 8 h / 0 - 10 °C
2: 88 percent / Cl2 / 10 - 15 °C
View Scheme
Nonafluorobutanesulfonyl fluoride
375-72-4

Nonafluorobutanesulfonyl fluoride

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C13H2F26O5S
1357369-86-8

C13H2F26O5S

Conditions
ConditionsYield
Stage #1: 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]propan-1-ol With sodium hydride
Stage #2: Nonafluorobutanesulfonyl fluoride
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

1-[2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl]imidazole
1173110-41-2

1-[2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl]imidazole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride
2: acetonitrile / 10 h / Reflux; Inert atmosphere
View Scheme
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

1,3-bis[2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl]imidazolium nonafluorobutanesulfonate
1357369-98-2

1,3-bis[2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonyl]imidazolium nonafluorobutanesulfonate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride
2: sodium carbonate / 4.25 h / 63 - 70 °C / Microwave irradiation; Inert atmosphere; Neat (no solvent); sealed vial
View Scheme
Multi-step reaction with 2 steps
1: sodium hydride
2: 3 h / 63 - 70 °C / Microwave irradiation; Inert atmosphere; Neat (no solvent); sealed vial
View Scheme
Multi-step reaction with 3 steps
1: sodium hydride
2: acetonitrile / 10 h / Reflux; Inert atmosphere
3: 3 h / 63 - 70 °C / Microwave irradiation; Inert atmosphere; Neat (no solvent); sealed vial
View Scheme
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C4F9O3S(1-)*C17H7F26N2O4(1+)
1357370-09-2

C4F9O3S(1-)*C17H7F26N2O4(1+)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride
2: 63 °C / Microwave irradiation; Neat (no solvent); Inert atmosphere; sealed vial
View Scheme
Multi-step reaction with 3 steps
1: sodium hydride
2: acetonitrile / 10 h / Reflux; Inert atmosphere
3: 63 °C / Microwave irradiation; Neat (no solvent); Inert atmosphere; sealed vial
View Scheme
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C4F9O3S(1-)*C19H7F30N2O5(1+)
1357370-13-8

C4F9O3S(1-)*C19H7F30N2O5(1+)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydride
2: 63 °C / Microwave irradiation; Neat (no solvent); Inert atmosphere; sealed vial
View Scheme
Multi-step reaction with 3 steps
1: sodium hydride
2: acetonitrile / 10 h / Reflux; Inert atmosphere
3: 63 °C / Microwave irradiation; Neat (no solvent); Inert atmosphere; sealed vial
View Scheme
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonylazide
1173110-46-7

2,4,4,5,7,7,8,8,9,9,9-undecafluoro-2,5-bis(trifluoromethyl)-3,6-dioxanonylazide

Conditions
ConditionsYield
Stage #1: 2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]propan-1-ol With pyridine; trifluoromethylsulfonic anhydride In dichloromethane at 0℃; for 2h;
Stage #2: With sodium azide In N,N-dimethyl-formamide at 50℃; for 48h;
127g
2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol
14548-74-4

2,3,3,3-tetrafluoro-2-[1,1,2,3,3,3-hexafluoro-2-(heptafluoropropoxy)propoxy]-1-propanol

C15H8F17N3O4

C15H8F17N3O4

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 2 h / 0 °C
1.2: 48 h / 50 °C
2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / N,N-dimethyl-formamide; water / 2 h / 20 °C
View Scheme

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