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inquiryDayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. Near 20 years DayangChem has provided dif
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inquiry2,2-DIMETHYLETHENYLBORONIC ACID CAS:14559-88-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryMelting point 87 °C Boiling point 190.6±23.0 °C(P
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:As cu
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirySuperior quality Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used as Pharmaceutical Intermediates Transportation:BY AIR Por
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryStock products, own laboratoryAppearance:White to off-white solid Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiry1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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2,2-DIMETHYLETHENYLBORONIC ACIDAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Type:Lab/Research institutions
inquiryTriisopropyl borate
2-methyl-1-propenylbromide
water
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
Stage #1: Triisopropyl borate; 2-methyl-1-propenylbromide With lithium In tetrahydrofuran at -50 - -40℃; Inert atmosphere; Stage #2: water With hydrogenchloride In tetrahydrofuran at 0 - 10℃; pH=3 - 4; Temperature; Reagent/catalyst; Inert atmosphere; | 60.3% |
2-methylpropen-1-ylmagnesium bromide
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With Trimethyl borate; lithium chloride In tetrahydrofuran; diethyl ether at -78 - 20℃; Inert atmosphere; | 55% |
With Trimethyl borate In diethyl ether at -78 - 20℃; | 41% |
Stage #1: 2-methylpropen-1-ylmagnesium bromide With Trimethyl borate In tetrahydrofuran at -78 - 20℃; Inert atmosphere; Stage #2: With hydrogenchloride; water In tetrahydrofuran at 0 - 20℃; for 1.5h; Inert atmosphere; | |
Stage #1: 2-methylpropen-1-ylmagnesium bromide With Trimethyl borate In tetrahydrofuran at -70 - 20℃; for 3.58333h; Inert atmosphere; Stage #2: With N-methyliminodiacetic acid In tetrahydrofuran; dimethyl sulfoxide at 120 - 150℃; for 1h; Inert atmosphere; Stage #3: With water; sodium hydroxide In tetrahydrofuran at 20℃; for 0.25h; |
2-methyl-1-propenylbromide
chloro-bis(dimethylamino)borane
water
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
Stage #1: 2-methyl-1-propenylbromide; chloro-bis(dimethylamino)borane With lithium In tetrahydrofuran at -78 - -70℃; Inert atmosphere; Stage #2: water With hydrogenchloride In tetrahydrofuran at 0 - 10℃; pH=3 - 4; Inert atmosphere; | 46.9% |
Trimethyl borate
2-methylprop-1-enyllithium
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
und anschliessend mit wss.HCl; |
Trimethyl borate
2-methylpropen-1-ylmagnesium bromide
2,2-dimethylethenylboronic acid
tris(ethylenedioxyboryl)methane
acetone
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
(i) MeLi, Et2O, THF, CH2Cl2, (ii) /BRN= 635680/; Multistep reaction; |
Trimethyl borate
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
und Erwaermen des Reaktionsprodukts mit wss.H2SO4; |
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With water; ammonium chloride In pentane at 20℃; for 0.5h; |
C6H13BO2
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water In tetrahydrofuran at 0 - 20℃; for 1.5h; |
2,2-dimethylethenylboronic acid
methyl 3-bromo-4-(tetrahydro-2H-pyran-2-yloxy)benzoate
methyl 3-(2-methyl-1-propenyl)-4-(tetrahydro-2H-pyran-2-yloxy)benzoate
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate In water; N,N-dimethyl-formamide at 70℃; for 23h; Inert atmosphere; | 100% |
With potassium phosphate; 2-dicyclohexylphosphino-2′,6′-dimethoxybiphenyl; palladium diacetate In water; N,N-dimethyl-formamide at 70℃; for 23h; Suzuki Coupling; Inert atmosphere; | 100% |
2,2-dimethylethenylboronic acid
(E)-4-(pyrazin-2-yl)but-3-en-2-one
Conditions | Yield |
---|---|
With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; magnesium 2-methylpropan-2-olate In toluene at 70℃; for 8h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 99% |
2,2-dimethylethenylboronic acid
(E)-4-(2,4,6-trimethoxyphenyl)but-3-en-2-one
Conditions | Yield |
---|---|
With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; magnesium 2-methylpropan-2-olate In toluene at 115℃; for 1h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 99% |
2,2-dimethylethenylboronic acid
(E)-4-(2-thienyl)but-3-en-2-one
Conditions | Yield |
---|---|
With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; magnesium 2-methylpropan-2-olate In toluene at 115℃; for 2h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 99% |
2,2-dimethylethenylboronic acid
(Z)-7-[(3R)-3-(tert-butyldimethylsilanyloxy)-5-oxo-cyclopent-1-enyl]hept-5-enoic acid isopropyl ester
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide In methanol; water at 3℃; for 72h; Temperature; Inert atmosphere; diastereoselective reaction; | 99% |
2,2-dimethylethenylboronic acid
N-(5-chloro[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide
Conditions | Yield |
---|---|
Stage #1: 2,2-dimethylethenylboronic acid; N-(5-chloro[1,2,4]triazolo[1,5-a]pyridin-2-yl)nicotinamide With cesium fluoride; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran; water at 120℃; Suzuki-Miyaura reaction; Stage #2: With hydrogenchloride In diethyl ether; dichloromethane | 96% |
2,2-dimethylethenylboronic acid
(E)-4-(quinolin-2-yl)but-3-en-2-one
Conditions | Yield |
---|---|
With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; magnesium 2-methylpropan-2-olate In toluene at 70℃; for 5h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 96% |
2,2-dimethylethenylboronic acid
(E)-4-(1-methyl-1H-imidazol-2-yl)but-3-en-2-one
Conditions | Yield |
---|---|
With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; magnesium 2-methylpropan-2-olate In toluene at 115℃; for 12h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 94% |
2,2-dimethylethenylboronic acid
2-(3-bromo-2-methylbenzoylamino)indan-2-carboxylic acid ethyl ester
2-[2-methyl-3-(2-methyl-1-propenyl)benzoylamino]indan-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) In water; N,N-dimethyl-formamide at 110℃; for 5h; | 92% |
2,2-dimethylethenylboronic acid
4-(pyridin-4-yl)-3-buten-2-one
Conditions | Yield |
---|---|
With (R)-3,3’-bis(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-1,1’-binaphthyl-2,2’-diol; magnesium 2-methylpropan-2-olate In toluene at 115℃; for 22h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 91% |
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; caesium carbonate In water; toluene at 50℃; for 6h; Inert atmosphere; Darkness; | 90% |
2,2-dimethylethenylboronic acid
1,1-dimethylethyl 9-bromo-2,3-dihydro-1,4-benzoxazepine-4(5H)-carboxylate
tert-butyl 9-(2-methylpropa-1-ene-1-yl)-2,3-dihydro-1,4-benzoxazepine-4(5H)-carboxylate
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water at 85℃; for 12h; Inert atmosphere; Saturated solution; | 89.1% |
2,2-dimethylethenylboronic acid
(E)-4-pyridin-3-ylbut-3-en-2-one
Conditions | Yield |
---|---|
With (1R,3'r)-3,3'-bis(perfluorophenyl)[1,1'-binaphthalene]-2,2'-diol; magnesium 2-methylpropan-2-olate In toluene at 115℃; for 15h; Molecular sieve; Inert atmosphere; enantioselective reaction; | 88% |
2,2-dimethylethenylboronic acid
benzo[e][1,2,3]oxathiazine 2,2-dioxide
Conditions | Yield |
---|---|
With nickel(II) perchlorate hexahydrate; C30H28NOP In 2,2,2-trifluoroethanol at 70℃; for 48h; | 87% |
With (1R,1’R,2S,2’S)-2,2’-di-tert-butyl-2,3,2’,3’-tetrahydro-1H,1‘H-(1,1‘)biisophosphindolyl; potassium carbonate; cobalt(II) bromide In tetrahydrofuran at 70℃; for 24h; Inert atmosphere; enantioselective reaction; | 70% |
1-Benzenesulfonyl-5-bromo-3-[2-(1-methyl-piperidin-4-yl)-thiazol-4-yl]-1H pyrrolo[2,3-b]pyridine
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With sodium carbonate; lithium chloride; bis-triphenylphosphine-palladium(II) chloride In ethanol; water; toluene Suzuki-Miaura reaction; Heating / reflux; | 86% |
With sodium carbonate; lithium chloride; bis-triphenylphosphine-palladium(II) chloride In ethanol; water; toluene at 110℃; for 1.5h; Suzuki Coupling; | 86% |
4-(1-Benzenesulfonyl-5-bromo-1H-pyrrolo[2,3-b]pyridin-3-yl)-thiazole-2-carboxylic acid ethyl ester
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With sodium carbonate; lithium chloride; bis-triphenylphosphine-palladium(II) chloride In ethanol; water; toluene at 110℃; for 1.5h; Suzuki-Miaura reaction; Heating / reflux; | 85% |
With sodium carbonate; lithium chloride; bis-triphenylphosphine-palladium(II) chloride In ethanol; water; toluene at 110℃; for 1.5h; Suzuki Coupling; | 85% |
2,2-dimethylethenylboronic acid
indole-2,3-dione
Conditions | Yield |
---|---|
With (1R,1’R,2S,2’S)-2,2’-di-tert-butyl-2,3,2’,3’-tetrahydro-1H,1‘H-(1,1‘)biisophosphindolyl; potassium carbonate; cobalt(II) bromide In tetrahydrofuran at 70℃; for 40h; Inert atmosphere; enantioselective reaction; | 80% |
2,2-dimethylethenylboronic acid
N-methyl-2-iodoaniline
N-methyl-N-[2-(2-methylpropenyl)phenyl]amine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 80℃; for 12h; | 80% |
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 90℃; for 16h; Inert atmosphere; | 79.9% |
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In 1,4-dioxane; water at 100℃; for 12h; Sealed tube; Inert atmosphere; | 78.1% |
2,2-dimethylethenylboronic acid
2-(2-iodo-3-methyl-benzoylamino)-indane-2-carboxylic acid ethyl ester
2-[3-methyl-2-(2-methyl-propenyl)-benzoylamino]-indan-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In 1,4-dioxane; water at 110℃; for 2h; Microwave irradiation; | 78% |
2,2-dimethylethenylboronic acid
anthranilic acid amide
Conditions | Yield |
---|---|
With dibromobis(triphenylphosphine)nickel(II); triethylamine; palladium dichloride In ethanol at 20℃; for 2h; Green chemistry; chemoselective reaction; | 75% |
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In 1,4-dioxane; water at 100℃; for 12h; Sealed tube; Inert atmosphere; | 74.6% |
2,2-dimethylethenylboronic acid
tris(2-methylpropene-1-yl) boroxine
Conditions | Yield |
---|---|
With magnesium sulfite In pyridine; diethyl ether at 20℃; | 73% |
byproducts: H2O; dehydration;; | |
byproducts: H2O; dehydration;; |
2,2-dimethylethenylboronic acid
5-fluoro-2-(2-iodo-3-methyl-benzoylamino)indan-2-carboxylic acid ethyl ester
5-fluoro-2-[3-methyl-2-(2-methyl-propenyl)-benzoylamino]-indan-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With potassium carbonate; palladium anchored homogeneous catalyst, FibreCatPd(0) (4.84percentPd) In 1,4-dioxane; ethanol; water at 120℃; for 7h; Microwave irradiation; | 73% |
2,2-dimethylethenylboronic acid
Conditions | Yield |
---|---|
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; caesium carbonate In water; toluene at 50℃; for 6h; Suzuki-Miyaura Coupling; Sonication; Darkness; | 71% |
2,2-dimethylethenylboronic acid
3-methyl-3-phenylcyclopropene
Conditions | Yield |
---|---|
With potassium carbonate; cobalt(II) chloride; [2R-[1(2'R*,5'R*),2a,5b]]-1,1'-(1,2-phenylene)bis[2,5-dimethylphospholane] In tetrahydrofuran at 70℃; for 12h; Inert atmosphere; Sealed tube; stereoselective reaction; | 70% |
Conditions | Yield |
---|---|
With palladium diacetate; cesium fluoride; tris-(o-tolyl)phosphine In 1,4-dioxane at 75℃; for 20h; Temperature; Solvent; Inert atmosphere; | 68.2% |
2,2-dimethylethenylboronic acid
1-(4-bromo-2-chloro-phenyl)-1-cyclopropyl-2-(1,2,4-triazol-1-yl)ethanol
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 90℃; for 14h; | 67% |
4-(2-(4-(5-bromo-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridin-3-yl)-1H-pyrazol-1-yl)ethyl)morpholine
2,2-dimethylethenylboronic acid
1-Benzenesulfonyl-5-(2-methyl-propenyl)-3-[1-(2-morpholin-4-yl-ethyl)-1H-pyrazol-4-yl]-1H-pyrrolo[2,3-b]pyridine
Conditions | Yield |
---|---|
With sodium carbonate; lithium chloride; bis-triphenylphosphine-palladium(II) chloride In ethanol; water; toluene for 3h; Suzuki-Miaura reaction; Heating / reflux; | 66% |
With sodium carbonate; lithium chloride; bis-triphenylphosphine-palladium(II) chloride In ethanol; water; toluene at 115℃; for 3h; Suzuki Coupling; | 66% |
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