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Cas:1470-91-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
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Cas:1470-91-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:1470-91-3
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
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Cas:1470-91-3
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
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Cas:1470-91-3
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
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Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the BUT-3-ENOYL CHLORIDE, CAS:1470-91-3 with the most competitive price and the best qual
Conditions | Yield |
---|---|
With thionyl chloride at 40℃; for 1h; | 67% |
With thionyl chloride | |
With thionyl chloride |
carbon monoxide
3-chloroprop-1-ene
A
phosgene
B
propene
C
3-chlorobutanoyl chloride
D
isopropyl chloride
E
but-3-enoyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride; palladium dichloride In dichloromethane at 100℃; for 16h; Product distribution; chlorocarbonylation of unsaturated substrates; other allylic halides, other catalysts, other solvents, var. temp., time, pressure; also with phosgene; | A n/a B 18 % Chromat. C 11 % Chromat. D 27 % Chromat. E 2 % Chromat. F 31 % Chromat. G n/a |
3-allyloxy-3-chlorodiazirine
A
but-3-enoyl chloride
B
3-chloroprop-1-ene
Conditions | Yield |
---|---|
In cyclohexane at 25℃; Product distribution; Further Variations:; Solvents; photolysis; |
2-cyano-N-(4-trifluoromethylphenyl)acetamide
A
but-3-enoyl chloride
Conditions | Yield |
---|---|
In tetrahydrofuran | A n/a B 2.4 g (31%) |
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; diethyl ether at 20℃; for 16h; | 100% |
5,5-dimethyl-oxazolidin-2-one
but-3-enoyl chloride
3-but-3-enoyl-5,5-dimethyl-oxazolidin-2-one
Conditions | Yield |
---|---|
Stage #1: 5,5-dimethyl-oxazolidin-2-one With n-butyllithium In tetrahydrofuran at -78℃; Metallation; Stage #2: but-3-enoyl chloride In tetrahydrofuran Acylation; | 97% |
but-3-enoyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; | 97% |
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; for 1.5h; Under N2; | 97% |
but-3-enoyl chloride
Conditions | Yield |
---|---|
With triethylamine In diethyl ether addn. at -15°C, then 0°C, 1 h; | 95% |
but-3-enoyl chloride
acetic acid 2,2-bis(methylsulfanyl)-1-(2-oxopiperidin-3-yl)ethyl ester
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 15h; | 94% |
With 4 A molecular sieve In dichloromethane at 25℃; for 15h; | 94% |
With 4 A molecular sieve Acylation; |
but-3-enoyl chloride
acetic acid 2,2-bis(methylsulfanyl)-1-(2-oxopiperidin-3-yl)ethyl ester
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 25℃; for 15h; | 94% |
but-3-enoyl chloride
acetic acid 2-methoxy-1-(2-oxopiperidin-3-yl)-2-phenylsulfanyl ethyl ester
Conditions | Yield |
---|---|
With molecular sieve In dichloromethane at 20℃; | 94% |
but-3-enoyl chloride
acetic acid 2-methoxy-2-(methylsulfanyl)-1-(2-oxopiperidin-3-yl)ethyl ester
Conditions | Yield |
---|---|
With molecular sieve In dichloromethane at 20℃; | 94% |
but-3-enoyl chloride
trans-4-aminocyclohexanecarboxylic acid
4-But-3-enoylamino-cyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water 1.) 0 deg C to 5 deg C, 2.) room temp., 20 min; | 92% |
but-3-enoyl chloride
N-acetyl-4-amino-phenylalanine
Conditions | Yield |
---|---|
With sodium hydroxide In water 1.) 0 deg C to 5 deg C, 2.) room temp., 20 min; | 92% |
but-3-enoyl chloride
(2R,3S,4R)-(+)-N-(vinylacetyl)-2-vinyl-3,4-dibenzyloxypyrrolidine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 4h; | 92% |
1-vinyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
but-3-enoyl chloride
1-(6,7-dimethoxy-1-vinyl-3,4-dihydro-1H-isoquinolin-2-yl)but-3-en-1-one
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 1h; | 91% |
Conditions | Yield |
---|---|
Stage #1: C9H11NO3S With tri-n-butylstannyl chloride; sodium hydrogencarbonate In diethyl ether; water Stage #2: but-3-enoyl chloride In hexane at 60℃; | 90% |
but-3-enoyl chloride
p-methoxylphenyl 3,4-di-O-benzoyl-α-L-rhamnopyranoside
Conditions | Yield |
---|---|
With pyridine; dmap In dichloromethane at -10℃; for 3h; | 90% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide at 0℃; for 1.5h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; | 89% |
but-3-enoyl chloride
2,2-dimethylpropanoic acid 1-[(methylcarbamoyl)methyl]-2,2-bis(methylsulfanyl)ethyl ester
2,2-dimethylpropionic acid 1-(bis(methylsulfanyl)methyl)-3-(but-3-enoylmethylamino)-3-oxopropyl ester
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; | 87% |
Conditions | Yield |
---|---|
With dmap In dichloromethane | 87% |
Conditions | Yield |
---|---|
at 120℃; for 3h; | 86% |
but-3-enoyl chloride
3-[1-(bis(methylsulfanyl)methyl)-1-hydroxypropyl]piperidin-2-one
3-[1-(bis(methylsulfanyl)methyl)-1-hydroxypropyl]-1-but-3-enoylpiperidin-2-one
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 15h; | 86% |
but-3-enoyl chloride
Conditions | Yield |
---|---|
With 4-methyl-morpholine; dmap In dichloromethane at 0 - 20℃; | 86% |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; | 86% |
but-3-enoyl chloride
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With sodium hydroxide In water 1.) 0 deg C to 5 deg C, 2.) room temp., 20 min; | 85% |
In diethyl ether at 20℃; for 10h; | 80% |
but-3-enoyl chloride
(S)-(+)-2-(N-methylamino)-3-phenylpropanol
(2S)-2-<3-butenoyl(methyl)amino>-3-phenylpropyl 3-butenoate
Conditions | Yield |
---|---|
With triethylamine In tetrachloromethane at 0 - 25℃; for 6.5h; | 85% |
but-3-enoyl chloride
acetic acid 2,2-bis(methylsulfanyl)-1-(2-oxo-azepan-3-yl)ethyl ester
acetic acid 1-(1-but-3-enoyl-2-oxoazepan-3-yl)-2,2-bis(methylsulfanyl) ethyl ester
Conditions | Yield |
---|---|
With 4 A molecular sieve In dichloromethane at 20℃; for 15h; | 85% |
With 4 A molecular sieve Acylation; |
but-3-enoyl chloride
5-amino-pyridine-2-carboxylic acid thiazol-2-ylamide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; | 85% |
but-3-enoyl chloride
(2S,6S)-1-But-3-enoyl-5,6-divinyl-piperidine-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 2h; | 83% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 24h; | 83% |
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