Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryGlutacondianil hydrochloride Basic information Product Name: Glutacondianil hydrochloride Synonyms: n-[5-(phenylamino)-2,4-pentadienylidene]-benzenaminmonohydrochloride;N-[5-(Phenyla
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inquiryProduct name Glutacondianil hydrochloride Synonyms N-[5-(Phenylamino)-2,4-pentadienylidene]aniline hydrochloride; N-(5-Anilino-2,4-pentadienylidene)aniline hydrochloride CAS No.
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Glutacondianil hydrochloride cas 1497-49-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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pyridine
perchloro-2-cyclopentene-1-one
aniline
A
2,4,4,5,5-Pentachloro-3-(phenylamino)-2-cyclopenten-1-one
B
2,4,4,5,5-Pentachloro-3-amino-2-cyclopenten-1-one
C
glutacondianil hydrochloride
Conditions | Yield |
---|---|
In 1,4-dioxane for 4h; | A 31% B 12.9% C 37.5% |
pyridine
N-phenyl-benzimidoyl chloride
aniline
glutacondianil hydrochloride
pyridine
aniline
p-toluenesulfonyl chloride
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With phosphorus pentachloride |
5-(2,4-dinitro-anilino)-penta-2,4-dienal
A
glutacondianil hydrochloride
B
2,4-Dinitroanilin
Conditions | Yield |
---|---|
With hydrogenchloride; water; acetic acid Abfiltrieren vom 2.4-Dinitro-anilin, Zufuegen Anilin zum Filtrat; |
1-(2,4-dinitrophenyl)-pyridinium chloride
aniline
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With hydrogenchloride |
malondialdehyde bis(diethyl acetal)
trimethylsiloxyethene
aniline hydrochloride
A
1,1,3,5,7,7-hexaethoxy-heptane
B
glutacondianil hydrochloride
C
3,5,7,7-tetraethoxy-1-heptanal
Conditions | Yield |
---|---|
With zinc(II) chloride 1.) ethyl acetate, 40 deg C, 0.25 hr., 2.) ethanol, 20 deg C, 4 hrs.; Yield given. Multistep reaction. Yields of byproduct given; |
aniline
A
glutacondianil hydrochloride
B
2-amino-3-cyano-5-nitropyridine
Conditions | Yield |
---|---|
With hydrogenchloride 1.) H2O, reflux, 5 min, 2.) H2O, pH=1; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94 percent / acetonitrile / 3.5 h / 15 °C 2: 2.) HCl / 1.) H2O, reflux, 5 min, 2.) H2O, pH=1 View Scheme |
5-(2,4-dinitro-anilino)-penta-2,4-dienal
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: glacial acetic acid; hydrogen chloride / 100 °C / im Rohr 2: alcohol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: alkali; water 2: glacial acetic acid; concentrated hydrochloric acid; water / Abfiltrieren vom 2.4-Dinitro-anilin, Zufuegen Anilin zum Filtrat View Scheme |
1,5-dioxaspiro[5.5]undecane-2,4-dione
glutacondianil hydrochloride
C23H26O8
Conditions | Yield |
---|---|
With triethylamine In DMF (N,N-dimethyl-formamide) at 20℃; for 8h; | 97% |
With triethylamine In isopropyl alcohol at 20 - 30℃; for 3h; |
2,4,5,7-tetranitro-9H-fluorene
acetic anhydride
glutacondianil hydrochloride
N-phenyl-N-[(1E,3E)-5-(2,4,5,7-tetranitro-9H-fluoren-9-ylidene)penta-1,3-dienyl]acetamide
Conditions | Yield |
---|---|
Reflux; | 96% |
acetic anhydride
glutacondianil hydrochloride
1,1,2-trimethyl-3-(6-carboxylatohexyl)benzindolium
Conditions | Yield |
---|---|
at 100℃; for 1h; Inert atmosphere; | 95% |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With sodium acetate; acetic anhydride at 60℃; for 2h; | 95% |
3,4-dihydro-1-ethyl-2,1-benzothiazin-4-one-7-carboxylic acid 2,2-dioxide
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Stage #1: 3,4-dihydro-1-ethyl-2,1-benzothiazin-4-one-7-carboxylic acid 2,2-dioxide; glutacondianil hydrochloride With triethylamine In ethanol at 20℃; Stage #2: With acetic acid at 0℃; | 92% |
1,2,3,3-tetramethyl-3H-indolium iodide
acetic anhydride
glutacondianil hydrochloride
1,3,3-trimethyl-2-(6-(N-phenylacetamido)hexa-1,3,5-trienyl)-3H-indolium iodide
Conditions | Yield |
---|---|
With pyridine at 25℃; for 0.666667h; Inert atmosphere; | 90% |
4-(1,1,2-trimethyl-1H-benzo[e]indol-3-ium-3-yl)butane-1-sulfonate
acetic anhydride
glutacondianil hydrochloride
4-(1,1-dimethyl-2-(6-(N-phenylacetamido)hexa-1,3,5-trien-1-yl)-1H-benzo[e]indol-3-ium-3-yl)butane-1-sulfonate
Conditions | Yield |
---|---|
at 100℃; for 1h; Inert atmosphere; | 88% |
for 0.5h; Reflux; Inert atmosphere; | 86.1% |
With acetic acid at 120℃; for 3h; | 42% |
In acetic acid Heating; | |
With triethylamine Heating; |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Stage #1: glutacondianil hydrochloride With acetic anhydride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 5℃; for 3h; Stage #2: 1-(2-hydroxycarbonylethyl)-2,3,3-trimethylbenzo[e]indoleninium bromide With sodium acetate In dichloromethane; water; acetonitrile for 18h; Reflux; Darkness; | 88% |
Conditions | Yield |
---|---|
Stage #1: C18H23NO2; glutacondianil hydrochloride With acetic anhydride; triethylamine In dichloromethane at 20 - 40℃; for 15h; Stage #2: With sodium iodide In dichloromethane for 2h; | 86% |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With sodium acetate; acetic anhydride; acetic acid at 120℃; for 0.75h; Inert atmosphere; Schlenk technique; | 85% |
tetramethyl ammoniumhydroxide
glutacondianil hydrochloride
malononitrile
tetramethylammonium 1,1,7,7-tetracyano-1,3,5-heptatrienide
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide for 1h; | 84% |
(1r,3r,5r,7r)-spiro-[adamantane-2,2′-[1,3]dioxane]-4′,6′-dione
glutacondianil hydrochloride
C31H34O8
Conditions | Yield |
---|---|
With triethylamine In DMF (N,N-dimethyl-formamide) at 20℃; for 5h; | 84% |
1-(4-sulfophenyl)-pyrazol-5-on-3-carboxylic acid
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1-(4-sulfophenyl)-pyrazol-5-on-3-carboxylic acid; glutacondianil hydrochloride In N,N-dimethyl-formamide for 1h; Reflux; Stage #2: With triethylamine In N,N-dimethyl-formamide at 45 - 60℃; for 3h; Stage #3: With potassium carbonate In water; N,N-dimethyl-formamide at 20℃; for 1.5h; Concentration; Reagent/catalyst; Solvent; | 84% |
2,3,3-trimethyl-1-(ethyl)-3H-benzindolinium-5,7-disulfonate
acetic anhydride
glutacondianil hydrochloride
C30H30N2O7S2
Conditions | Yield |
---|---|
at 100℃; for 1h; | 83% |
Conditions | Yield |
---|---|
Stage #1: 1-methyl-2-phenylindolizine With perchloric acid; acetic anhydride at 20℃; for 0.0833333h; Stage #2: glutacondianil hydrochloride With triethylamine at 20℃; for 24h; | 82% |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With acetic anhydride at 10℃; for 0.5h; Inert atmosphere; | 81% |
1,3-dimethylbarbituric acid
glutacondianil hydrochloride
5-<5-(hexahydro-1,3-dimethyl-2,4,6-trioxo-5-pyrimidinyl)-2,4-pentadienylidene>-1,3-dimethyl-2,4,6(1H,3H,5H)-pyrimidinetrione
Conditions | Yield |
---|---|
With C6H15N*C25H31N3O5S2 In DMF (N,N-dimethyl-formamide) at 20℃; for 2h; | 80% |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With pyridine In acetic anhydride for 0.5h; Heating; | 77% |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Stage #1: 4-(1-methylindolizin-2-yl)benzonitrile With perchloric acid; acetic anhydride at 20℃; for 0.0833333h; Stage #2: glutacondianil hydrochloride With triethylamine at 20℃; for 24h; | 77% |
Conditions | Yield |
---|---|
With acetic anhydride at 75℃; for 0.5h; | 76% |
glutacondianil hydrochloride
acetic acid
1-Ethyl-2,3,3-Trimethylindolenineninium 5-Sulfone
C26H28N2O4S
Conditions | Yield |
---|---|
at 100℃; for 1h; | 76% |
glutacondianil hydrochloride
2-[5-(1-ethyl-1,3-dihydro-5-acetylamino-3,3-dimethyl-2H-indol-2-ylidene)-1,3,5-heptatrien-1-yl]-1-ethyl-5-acetylamino-3,3-dimethyl-3H-indolium iodide
Conditions | Yield |
---|---|
Stage #1: glutacondianil hydrochloride With N-ethyl-N,N-diisopropylamine In dichloromethane; acetic anhydride at 20℃; for 3h; Stage #2: 5-acetamido-1-ethyl-2,3,3-trimethyl-3H-indol-1-ium iodide With sodium acetate In methanol; acetic anhydride for 8h; Reflux; | 76% |
2,3,3-trimethyl-1-(pent-4-yn-1-yl)-3H-indol-1-ium iodide
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Stage #1: 2,3,3-trimethyl-1-(pent-4-yn-1-yl)-3H-indol-1-ium iodide; glutacondianil hydrochloride With sodium acetate; acetic acid at 50℃; for 3h; Stage #2: With perchloric acid In water | 75% |
Conditions | Yield |
---|---|
With pyridine at 25℃; for 1h; Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
Heating; | 71% |
Conditions | Yield |
---|---|
With sodium acetate In acetic acid at 120℃; for 0.5h; | 70% |
C10H14O6
1,5-dioxaspiro[5.5]undecane-2,4-dione
glutacondianil hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1,5-dioxaspiro[5.5]undecane-2,4-dione; glutacondianil hydrochloride With triethylamine In isopropyl alcohol at 30℃; for 48h; Stage #2: C10H14O6 In isopropyl alcohol at 35℃; for 3h; | 66% |
C17H27N2(1+)*I(1-)
acetic anhydride
glutacondianil hydrochloride
C30H38N3O(1+)*Cl(1-)
Conditions | Yield |
---|---|
With acetic acid for 1h; Reflux; Inert atmosphere; | 65% |
glutacondianil hydrochloride
Conditions | Yield |
---|---|
With triethylamine In acetic anhydride for 0.05h; Reflux; | 65% |
cycl-isopropylidene malonate
glutacondianil hydrochloride
5-[5-(6-hydroxy-2,2-dimethyl-4-oxo-1,3-dioxin-5-yl)-2,4-pentadienylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione
Conditions | Yield |
---|---|
With triethylamine In methanol at 20℃; for 3h; | 63.6% |
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