As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryHigh quality and best price of 4-Benzofurancarboxylic acid from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:As
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiry4-Benzofurancarboxylic acid cas 166599-84-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
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inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
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inquirymethyl benzofuran-4-carboxylate
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran; methanol at 20℃; for 16h; | 99% |
Stage #1: methyl benzofuran-4-carboxylate With lithium hydroxide In tetrahydrofuran; methanol; water at 20℃; for 16h; Stage #2: With hydrogenchloride In water | 99% |
With potassium hydroxide In methanol for 1h; Heating; | 97% |
methyl 2-hydroxy-2,3-dihydrobenzofuran-4-carboxylate
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: methyl 2-hydroxy-2,3-dihydrobenzofuran-4-carboxylate; toluene-4-sulfonic acid In toluene for 5.46667h; Heating / reflux; Stage #2: With sodium hydroxide; water In toluene at 60℃; for 9h; Stage #3: With hydrogenchloride In water at 2 - 14℃; for 14.5h; Heating / reflux; | 62% |
Multi-step reaction with 2 steps 1: 67 percent / 85percent H3PO4 / a) RT, 10 min, b) 100 deg C, 15 min 2: 97 percent / 35percent KOH / methanol / 1 h / Heating View Scheme |
methyl 3-(prop-2-enyloxy)benzoate
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 41 percent / 1 h / 230 °C 2: 1.) O3, 2.) (CH3)2S / 1.) MeOH, -70 deg C, 30 min, 2.) MeOH, RT, overnight 3: 67 percent / 85percent H3PO4 / a) RT, 10 min, b) 100 deg C, 15 min 4: 97 percent / 35percent KOH / methanol / 1 h / Heating View Scheme |
2-allyl-3-hydroxy-benzoic acid methyl ester
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) O3, 2.) (CH3)2S / 1.) MeOH, -70 deg C, 30 min, 2.) MeOH, RT, overnight 2: 67 percent / 85percent H3PO4 / a) RT, 10 min, b) 100 deg C, 15 min 3: 97 percent / 35percent KOH / methanol / 1 h / Heating View Scheme |
benzofuran-4-yl trifluoromethanesulfonate
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 18 h / 80 °C / 3102.97 Torr 2: lithium hydroxide; water / tetrahydrofuran; methanol / 16 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1,3-bis-(diphenylphosphino)propane; palladium diacetate; triethylamine / dimethyl sulfoxide / 18 h / 80 °C / 3102.97 Torr 2: lithium hydroxide / tetrahydrofuran; water; methanol / 16 h / 20 °C View Scheme |
4-hydroxybenzofuran
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine; dmap / dichloromethane / 2 h / 0 °C 2: 1,3-bis-(diphenylphosphino)propane; palladium diacetate; triethylamine / dimethyl sulfoxide / 18 h / 80 °C / 3102.97 Torr 3: lithium hydroxide / tetrahydrofuran; water; methanol / 16 h / 20 °C View Scheme |
N,O-dimethylhydroxylamine*hydrochloride
benzofuran-4-carboxylic acid
N-methoxy-N-methylbenzofuran-4-carboxamide
Conditions | Yield |
---|---|
Stage #1: benzofuran-4-carboxylic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With pyridine In dichloromethane at 0 - 20℃; for 18h; | 93% |
Stage #1: benzofuran-4-carboxylic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: N,O-dimethylhydroxylamine*hydrochloride With pyridine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 18h; | 93% |
benzofuran-4-carboxylic acid
2,3-dihydrobenzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
With hydrogen; palladium 10% on activated carbon In acetic acid under 3102.97 Torr; for 12h; | 83% |
With hydrogen; palladium 10% on activated carbon In ethanol at 20℃; under 3000.3 Torr; for 16h; | |
With hydrogen; palladium 10% on activated carbon In ethanol at 20℃; under 3000.3 Torr; for 16h; |
tert-butyl (3R)3-aminopiperidine-1-carboxylate
benzofuran-4-carboxylic acid
(R)-3-[(benzofuran-4-carbonyl)-amino]-piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 20h; | 82% |
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 20h; | 82% |
(2RS)-(2-aminomethyl-azetidin-1-yl)-[5-(4-fluoro-phenyl)-2-methyl-thiazol-4-yl]-methanone
benzofuran-4-carboxylic acid
(2S)-Benzofuran-4-carboxylic acid{1-[5-(4-fluoro-phenyl)-2-methyl-thiazole-4-carbonyl]-azetidin-2-ylmethyl}-amide
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 20h; | 78% |
(S)-3-methylamino-4-phenyl-butyronitrile hydrochloride
benzofuran-4-carboxylic acid
benzofuran-4-carboxylic acid ((S)-1-benzyl-2-cyanoethyl)(methyl)amide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 20h; | 78% |
bis(2-fluorophenyl)iodonium trifluoromethanesulfonate
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate In N,N-dimethyl-formamide at 110℃; for 24h; | 50% |
6a-naltrexamine hydrochloride
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: benzofuran-4-carboxylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide for 1h; Molecular sieve; Cooling with ice; Inert atmosphere; Stage #2: 6a-naltrexamine hydrochloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Stage #3: With potassium carbonate In methanol at 20℃; Inert atmosphere; | 45% |
6β-naltrexamine
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: benzofuran-4-carboxylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide for 1h; Molecular sieve; Cooling with ice; Inert atmosphere; Stage #2: 6β-naltrexamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Stage #3: With potassium carbonate In methanol at 20℃; Inert atmosphere; | 42% |
tert-butyl (2S)-2-(aminomethyl)azetidine-1-carboxylate
benzofuran-4-carboxylic acid
(2S)-{[(benzofuran-4-carbonyl)-amino]-methyl}-azetidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide Inert atmosphere; | 30% |
benzofuran-4-carboxylic acid
2-iodo-benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: benzofuran-4-carboxylic acid With tert.-butyl lithium In diethyl ether; pentane at -78℃; for 0.5h; Inert atmosphere; Stage #2: With iodine In diethyl ether; pentane at -78 - 20℃; | 23% |
(RS)-2-Cyclopropyl-2-[methyl-(2-methyl-5-phenyl-thiazole-4-carbonyl)-amino]-ethyl-ammonium chloride
benzofuran-4-carboxylic acid
2-methyl-5-phenyl-thiazole-4-carboxylic acid {(RS)-2-[(benzofuran-4-carbonyl)-amino]-1-cyclopropyl-ethyl}-methyl-amide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide | 22% |
benzofuran-4-carboxylic acid
2-methyl-5-phenyl-thiazole-4-carboxylic acid {(RS)-2-[(benzofuran-4-carbonyl)-amino]-1-cyclopropyl-ethyl}-methyl-amide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide | 22% |
benzofuran-4-carboxylic acid
benzofuran-4-carbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide Ambient temperature; | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 19 - 20℃; for 2.5h; | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 5h; | |
With thionyl chloride for 2h; Heating / reflux; |
benzofuran-4-carboxylic acid
tert-butyl alcohol
tert-butyl (1-benzofuran-4-yl)carbamate
Conditions | Yield |
---|---|
With diphenyl phosphoryl azide; triethylamine for 18h; Heating; |
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.166667h; |
benzofuran-4-carboxylic acid
4-aminobenzofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenoxyphosphoryl azide; Et3N / 18 h / Heating 2: 0.35 g / TFA / CH2Cl2 / 2.5 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: diphenylphosphoranyl azide; triethylamine / tert-butyl alcohol 2: trifluoroacetic acid / dichloromethane View Scheme |
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diphenoxyphosphoryl azide; Et3N / 18 h / Heating 2: 0.35 g / TFA / CH2Cl2 / 2.5 h / 0 - 20 °C 3: 76 percent / HCl(g) / propan-2-ol / 90 °C View Scheme |
benzofuran-4-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2, DMF / Ambient temperature 2: EtAlCl2 / CH2Cl2; toluene / -78 - 20 °C View Scheme |
2-allyl-3-hydroxy-benzoic acid methyl ester
benzofuran-4-carboxylic acid
tert-butyl (1-benzofuran-4-yl)carbamate
Conditions | Yield |
---|---|
With diphenylphosphoranyl azide; triethylamine In tert-butyl alcohol |
(1S,3S,5S)-3-aminomethyl-2-aza-bicyclo[3.1.0]hexane-2-carboxylic acid tert-butyl ester
benzofuran-4-carboxylic acid
(1S,3S,5S)-3-{[(benzofuran-4-carbonyl)-amino]-methyl}-2-aza-bicyclo[3.1.0]hexane-2-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine for 2h; |
tert-butyl (1S,2S,5R)-2-(aminomethyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate
benzofuran-4-carboxylic acid
(1S,2S,5R)-2-{[(benzofuran-4-carbonyl)-amino]-methyl}-3-aza-bicyclo[3.1.0]hexane-3-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: benzofuran-4-carboxylic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.166667h; Stage #2: tert-butyl (1S,2S,5R)-2-(aminomethyl)-3-azabicyclo[3.1.0]hexane-3-carboxylate In N,N-dimethyl-formamide |
(1R,3S,4S)-3-aminomethyl-2-aza-bicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester
benzofuran-4-carboxylic acid
(1R,3S,4S)-3-{[(benzofuran-4-carbonyl)-amino]-methyl}-2-aza-bicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: benzofuran-4-carboxylic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide Stage #2: (1R,3S,4S)-3-aminomethyl-2-aza-bicyclo[2.2.1]heptane-2-carboxylic acid tert-butyl ester In dichloromethane; N,N-dimethyl-formamide |
(R)-tert-butyl 4-(aminomethyl)thiazolidine-3-carboxylate
benzofuran-4-carboxylic acid
(R)-4-{[(benzofuran-4-carbonyl)-amino]-methyl}-thiazolidine-3-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane |
(2RS)-(2-aminomethyl-azetidin-1-yl)-biphenyl-2-yl-methanone
benzofuran-4-carboxylic acid
(2S)-Benzofuran-4-carboxylic acid [1-(biphenyl-2-carbonyl)-azetidin-2-ylmethyl]-amide
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 20h; |
(2RS)-[1-(biphenyl-2-sulfonyl)azetidin-2-yl]methylamine
benzofuran-4-carboxylic acid
(2S)-Benzofuran-4-carboxylic acid [1-(biphenyl-2-sulfonyl)-azetidin-2-ylmethyl]-amide
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 20h; |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl acetamide |
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