DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiry3-Methyl-5-(phenylmethoxy)-2-[4-(phenylmethoxy)phenyl]-1H-indole CAS No.:198479-63-9 Name: 3-Methyl-5-(phenylmethoxy)-2-[4-(phenylmethoxy)phenyl]-1H-indole Molecular Structure Molecular F
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiry3-METHYL-5-(PHENYLMETHOXY)-2-[4-(PHENYLMETHOXY)PHENYL]-1H-INDOLE Basic information Product Name: 3-METHYL-5-(PHENYLMETHOXY)-2-[4-(PHENYLMETHOXY)PHENYL]-1H-INDOLE Synonyms: 3-METHYL-5-(PH
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryName 3-methyl-5-(phenylmethoxy)-2-[4-(phenylmethoxy)phenyl]-1h-indole Synonyms 5-(benzyloxy)-2-(4-(benzyloxy)phenyl)-3-methyl-1h-indole;
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Crystalline Powder Storage:Store in sealed conta
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inquiry3-METHYL-5-(PHENYLMETHOXY)-2-[4-(PHENYLMETHOXY)PHENYL]-1H-INDOLE CAS:198479-63-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermedia
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua
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inquiryOur company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: 3-Methyl-5-(Phenylmethoxy)-2-[4-(Phenylmethoxy)Phenyl]-1H-Indole CAS No.:198479-63-9 Molecule Formula:C29H25NO2 Molecule Weight:419.53 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enter
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiry3-METHYL-5-(PHENYLMETHOXY)-2-[4-(PHENYLMETHOXY)PHENYL]-1H-INDOLE Basic information Product Name: 3-METHYL-5-(PHENYLMETHOXY)-2-[4-(PHENYLMETHOXY)PHENYL]-1H-INDOLE Synonyms: 3-METHYL-5-(PHENYLMETHOXY)-2-[4-(PHENYLMETHOXY)PHENYL]-1H-INDOLE;1H-Ind
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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inquiryMy Company Changchun Artel Import and Export trade companyImport and Export Trade Co., Ltd.is located in Changchun, a national historical and cultural city, Jilin Province, China. It covers an area of 22,000 square meters, construction area
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Min.Order:20 Metric Ton
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:198479-63-9
Min.Order:1 Gram
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryWuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
Cas:198479-63-9
Min.Order:100 Gram
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
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Min.Order:1 Kilogram
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry1-<4-(benzyloxy)phenyl>-2-bromo-1-propanone
4-benzyloxyaniline hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 115℃; for 4h; Temperature; Reagent/catalyst; | 94.6% |
Stage #1: 1-<4-(benzyloxy)phenyl>-2-bromo-1-propanone; 4-benzyloxyaniline hydrochloride With triethylamine In butan-1-ol at 118℃; for 3h; Bischler-Moehlau Indole Synthesis; Stage #2: With hydrogenchloride In water; butan-1-ol at 118℃; for 7h; Temperature; Reagent/catalyst; Bischler-Moehlau Indole Synthesis; | 90.5% |
With triethylamine In N,N-dimethyl-formamide at 120 - 150℃; for 4h; Bischler indole synthesis; Inert atmosphere; | 84.9% |
4-benzyloxypropiophenone
4-benzyloxyphenylhydrazine hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
With acetic acid In ethanol at 75 - 80℃; Product distribution / selectivity; | 94% |
acetic acid In ethanol at 75 - 80℃; for 12h; Product distribution / selectivity; | 94% |
With hydrogenchloride In ethanol for 2h; Reflux; | 84% |
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol; dimethyl sulfoxide at 100℃; for 20h; | 85% |
With sodium ethanolate In dimethyl sulfoxide at 130℃; | 72% |
4-benzyloxyaniline hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
In chlorobenzene at 125 - 130℃; for 8h; Large scale; | 83.5% |
1-(4-benzyloxyphenyl)-2-(4-benzyloxy-phenylamino)-1-propanone
4-benzyloxyaniline hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
In isopropyl alcohol at 110 - 115℃; for 5h; Product distribution / selectivity; | 82% |
In ethanol at 110 - 115℃; for 5h; Product distribution / selectivity; | 79% |
1-(4-benzyloxyphenyl)-2-(4-benzyloxy-phenylamino)-1-propanone
p-benzyloxyaniline
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
In 2-ethoxy-ethanol for 6h; Reflux; | 80.5% |
4-benzyloxyaniline hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide for 2.5h; Reflux; | 65% |
p-benzyloxyaniline
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
In dichloromethane; ethyl acetate; N,N-dimethyl-formamide | 33% |
In dichloromethane; ethyl acetate; N,N-dimethyl-formamide | 33% |
In dichloromethane; ethyl acetate; N,N-dimethyl-formamide | 33% |
p-benzyloxyaniline
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
In dichloromethane; ethyl acetate; N,N-dimethyl-formamide | 33% |
p-benzyloxyaniline
4-benzyloxypropiophenone
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 125℃; for 6h; | 23% |
4-benzyloxypropiophenone
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: bromine / acetic acid / 3 h / 0 - 20 °C 2: triethylamine / N,N-dimethyl-formamide / 4 h / 120 - 150 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: bromine / 1,4-dioxane; methanol / 1 h / 20 °C 2: triethylamine / ethanol / 5 h / 20 °C 3: 2-ethoxy-ethanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: aluminum (III) chloride; bromine / toluene; methanol / 40 - 45 °C / Large scale 2: toluene / 2 h / 110 °C / Reflux; Large scale 3: chlorobenzene / 8 h / 125 - 130 °C / Large scale View Scheme | |
Multi-step reaction with 2 steps 1: bromine; acetic acid / 1 h / 0 °C 2: triethylamine / N,N-dimethyl-formamide / 5 h / 120 - 150 °C View Scheme |
benzyl bromide
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / acetone / 60 °C 2: bromine / acetic acid / 3 h / 0 - 20 °C 3: triethylamine / N,N-dimethyl-formamide / 4 h / 120 - 150 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetone / 60 °C 2: triethylamine / N,N-dimethyl-formamide / 6 h / 125 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / acetone / 18 h / Reflux 2: bromine; acetic acid / 1 h / 0 °C 3: triethylamine / N,N-dimethyl-formamide / 5 h / 120 - 150 °C View Scheme |
4-hydroxypropiophenone
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / acetone / 60 °C 2: bromine / acetic acid / 3 h / 0 - 20 °C 3: triethylamine / N,N-dimethyl-formamide / 4 h / 120 - 150 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetonitrile / 16 h / 20 °C / Inert atmosphere 2: hydrogenchloride / ethanol / 2 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / acetone / 24 h / Reflux 2: bromine / 1,4-dioxane; methanol / 1 h / 20 °C 3: triethylamine / ethanol / 5 h / 20 °C 4: 2-ethoxy-ethanol / 6 h / Reflux View Scheme |
1-<4-(benzyloxy)phenyl>-2-bromo-1-propanone
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / ethanol / 5 h / 20 °C 2: 2-ethoxy-ethanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: toluene / 2 h / 110 °C / Reflux; Large scale 2: chlorobenzene / 8 h / 125 - 130 °C / Large scale View Scheme |
4-nitro-phenol
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / acetone / 24 h / Reflux 2: tin(ll) chloride / ethanol / 24 h / 45 °C / Inert atmosphere 3: 2-ethoxy-ethanol / 6 h / Reflux View Scheme |
benzyl chloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / acetone / 24 h / Reflux 2: tin(ll) chloride / ethanol / 24 h / 45 °C / Inert atmosphere 3: 2-ethoxy-ethanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: potassium carbonate / acetone / 24 h / Reflux 2: bromine / 1,4-dioxane; methanol / 1 h / 20 °C 3: triethylamine / ethanol / 5 h / 20 °C 4: 2-ethoxy-ethanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1.1: tetrabutylammomium bromide / toluene; water / 90 °C / Reflux; Large scale 1.2: Reflux; Large scale 2.1: aluminum (III) chloride; bromine / toluene; methanol / 40 - 45 °C / Large scale 3.1: toluene / 2 h / 110 °C / Reflux; Large scale 4.1: chlorobenzene / 8 h / 125 - 130 °C / Large scale View Scheme |
benzyl 4-nitrophenyl ether
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tin(ll) chloride / ethanol / 24 h / 45 °C / Inert atmosphere 2: 2-ethoxy-ethanol / 6 h / Reflux View Scheme |
1-{2-[4-(chloromethyl)phenoxy]ethyl}hexahydro-1H-azepine hydrochloride
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1-[4-(2-azepan-1-yl-ethoxy)-benzyl]-1H-indole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 10h; Time; Reagent/catalyst; | 93.7% |
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydroxide In water; dimethyl sulfoxide at 20℃; for 1h; Large scale; Stage #2: 1-{2-[4-(chloromethyl)phenoxy]ethyl}hexahydro-1H-azepine hydrochloride In dimethyl sulfoxide; N,N-dimethyl-formamide at 20℃; for 1h; Solvent; Time; Large scale; | 91.8% |
With sodium hydride In N,N-dimethyl acetamide at 0 - 10℃; for 0.5h; Large scale; | 82.6% |
(4-chloromethylphenoxy)acetonitrile
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
{4-[5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-indol-1-ylmethyl]-phenoxy}-acetonitrile
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium amide In N,N-dimethyl-formamide at 10 - 15℃; for 0.25h; Stage #2: 4-chloromethyl phenoxy acetonitrile In N,N-dimethyl-formamide at 10 - 15℃; | 80% |
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
2-(4-hydroxyphenyl)-3-methyl-1H-indol-5-ol
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In tetrahydrofuran; ethanol at 20℃; | 78.3% |
Multi-step reaction with 2 steps 1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 1.2: 2.5 h / 0 °C / Inert atmosphere; Reflux 2.1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; ethyl acetate / 0.5 h View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 1.2: 2.5 h / 0 °C / Inert atmosphere; Reflux 2.1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; ethyl acetate / 0.5 h View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere 1.2: 2.5 h / 0 °C / Inert atmosphere; Reflux 2.1: hydrogen; 20% palladium hydroxide-activated charcoal / methanol; ethyl acetate / 0.5 h View Scheme |
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: tert-butyl (4-(4-(bromomethyl)phenoxy)butyl)carbamate In N,N-dimethyl-formamide at 0 - 20℃; for 12h; | 73% |
4-(benzyloxy)benzyl bromide
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 4-(benzyloxy)benzyl bromide In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; Reflux; | A 68% B 30% |
4-Fluorobenzyl bromide
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 4-Fluorobenzyl bromide In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; Reflux; | A 23% B 68% |
1-[(S)-2-(4-Chloromethyl-phenoxy)-1-methyl-ethyl]-pyrrolidine
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1-[4-(2-pyrrolidin-1-yl-propoxy)-benzyl]-1H-indole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 67% |
(R)-1-[2-(4-Chloromethyl-phenoxy)-ethyl]-3-methyl-pyrrolidine
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1-{4-[2-(3-methyl-pyrrolidin-1-yl)-ethoxy]-benzyl}-1H-indole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 67% |
1 ,6-dibromohexane
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1 ,6-dibromohexane In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | A 26% B 66% C 12% |
1-(bromomethyl)-4-(triphenylmethoxy)benzene
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.166667h; Stage #2: 1-(bromomethyl)-4-(triphenylmethoxy)benzene In N,N-dimethyl-formamide at 0℃; for 2h; | 66% |
1,5-dibromo-pentane
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1,5-dibromo-pentane In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | A 22% B 9% C 65% |
1,4-dibromo-butane
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1,4-dibromo-butane In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | A 63% B 17% C 20% |
1,4-bis(bromomethyl)benzene
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1,4-bis(bromomethyl)benzene In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | A 22% B 63% |
1,4-dibromo-butane
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide for 0.666667h; Stage #2: 1,4-dibromo-butane With N,N-dimethyl-formamide at 20℃; for 2.5h; | 60.6% |
2-(4-bromomethylphenoxy)ethyl 4-methylbenzenesulfonate
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
B
2-(4-{[5-(benzyloxy)-2-[4-(benzyloxy)phenyl]-3-methyl-1H-indol-1-yl]methyl}phenoxy)ethyl 4-methylbenzene-1-sulfonate
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at -10 - -5℃; for 0.5h; Stage #2: 2-(4-bromomethylphenoxy)ethyl 4-methylbenzenesulfonate In N,N-dimethyl-formamide at -5 - 0℃; for 3h; Stage #3: With acetic acid In N,N-dimethyl-formamide | A n/a B 60% |
1,8-dibromooctane
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1,8-dibromooctane In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | A 60% B 22% C 13% |
ethyl [p-(chloromethyl)phenoxy]acetate
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
{4-[5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-indol-1-ylmethyl]-phenoxy}-acetic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.333333h; Stage #2: ethyl [p-(chloromethyl)phenoxy]acetate In N,N-dimethyl-formamide at 20℃; for 18h; Further stages.; | 59% |
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.333333h; Stage #2: ethyl [p-(chloromethyl)phenoxy]acetate In N,N-dimethyl-formamide at 20℃; | 29.7% |
1,12-dibromododecane
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1,12-dibromododecane In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | A 11% B 59% C 30% |
3,4,5-trimethoxybenzyl bromide
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 3,4,5-trimethoxybenzyl bromide In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; Reflux; | A 17% B 51% |
3-phenoxypropyl bromide
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 1h; Inert atmosphere; Stage #2: 3-phenoxypropyl bromide In N,N-dimethyl-formamide at 0 - 20℃; for 2h; Inert atmosphere; | 46.7% |
bromoethyl-2-benzyl ether
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Inert atmosphere; Stage #2: bromoethyl-2-benzyl ether In tetrahydrofuran at 0℃; for 2.5h; Inert atmosphere; Reflux; | 43% |
phenoxyethyl bromide
5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole
Conditions | Yield |
---|---|
Stage #1: 5-benzyloxy-2-(4-benzyloxy-phenyl)-3-methyl-1H-indole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 1h; Inert atmosphere; Stage #2: phenoxyethyl bromide In N,N-dimethyl-formamide at 0 - 20℃; for 2h; Inert atmosphere; | 41.2% |
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