DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Lorcaserin(856681-05-5)is an orally administered agent and a selective 5-HT2C receptor agonist for the treatment of obesity. It had been approved for marketing in US by FDA on 27 June in 2012. In clinical studies, lorcaserin h
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiry2-Chloro-6-fluorophenol Basic information Product Name: 2-Chloro-6-fluorophenol Synonyms: 2-CHLORO-6-FLUOROPHENOL;Chlorofluorophenol3;2-Chloro-6-fluorophenol, 97+%;6-CHLORO-2-FLUORO PHENOL;2-Chloro-6-flurophenol;2-Chloro-6-fluorophenol, 98%,
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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2-chloro-6-fluorophenyl isopropylcarbamate
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; ethanol at 20℃; for 2h; | 98% |
(2-chloro-6-fluorophenyl)(isopropoxy)dimethylsilane
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol; water at 20℃; for 16h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With 1,3-dichloro-5,5-dimethylhydantoin; diisopropylamine hydrochloride In toluene at 0℃; for 4h; Darkness; regioselective reaction; | 91% |
With tetrachloromethane; chlorine | |
With chlorine In tetrachloromethane | |
Multi-step reaction with 5 steps 1.1: TMEDA / diethyl ether; pentane / 0.5 h / 20 °C 2.1: n-butyllithium; TMEDA / diethyl ether; pentane / 1 h / -78 °C 2.2: C2Cl6 / diethyl ether; pentane / 1 h / -78 °C 3.1: 0.210 g / aq. HCl / methanol / -78 - 20 °C 4.1: 98 percent / aq. NaOH / ethanol; tetrahydrofuran / 2 h / 20 °C View Scheme | |
With diisobutylamine; sulfuryl dichloride In toluene at 20℃; |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
Stage #1: 2-(2-fluoro-6-chlorophenyl)oxypyridine With methyl trifluoromethanesulfonate In toluene at 100℃; for 2h; Inert atmosphere; Stage #2: With sodium ethanolate for 1h; Reflux; Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With acetic acid; Selectfluor; eosin y In water at 20℃; for 6h; Irradiation; Green chemistry; | 77% |
Multi-step reaction with 3 steps 1.1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / dimethyl sulfoxide / 24 h / 80 °C / Inert atmosphere 2.1: bis(dibenzylideneacetone)-palladium(0); N-fluorobis(benzenesulfon)imide / ethyl acetate / 5 h / 80 °C 3.1: methyl trifluoromethanesulfonate / toluene / 2 h / 100 °C / Inert atmosphere 3.2: 1 h / Reflux; Inert atmosphere View Scheme |
1-chloro-3-fluoro-2-methoxybenzene
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With pyridine hydrochloride | |
With boron tribromide In dichloromethane at -78 - 20℃; for 16h; |
2-fluorophenyl isopropylcarbamate
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: TMEDA / diethyl ether; pentane / 0.5 h / 20 °C 2.1: n-butyllithium; TMEDA / diethyl ether; pentane / 1 h / -78 °C 2.2: C2Cl6 / diethyl ether; pentane / 1 h / -78 °C 3.1: 0.210 g / aq. HCl / methanol / -78 - 20 °C 4.1: 98 percent / aq. NaOH / ethanol; tetrahydrofuran / 2 h / 20 °C View Scheme |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: n-butyllithium; TMEDA / diethyl ether; pentane / 1 h / -78 °C 1.2: C2Cl6 / diethyl ether; pentane / 1 h / -78 °C 2.1: 0.210 g / aq. HCl / methanol / -78 - 20 °C 3.1: 98 percent / aq. NaOH / ethanol; tetrahydrofuran / 2 h / 20 °C View Scheme |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0.210 g / aq. HCl / methanol / -78 - 20 °C 2: 98 percent / aq. NaOH / ethanol; tetrahydrofuran / 2 h / 20 °C View Scheme |
2,2,6-trichloro-6-fluoro-1,1-cyclohexane-diol
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
Å molecular sieve In pyridine |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium hydrogencarbonate In tetrahydrofuran; methanol; water at 20℃; for 16h; Inert atmosphere; | 277 mg |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: bis(dibenzylideneacetone)-palladium(0); N-fluorobis(benzenesulfon)imide / ethyl acetate / 5 h / 80 °C 2.1: methyl trifluoromethanesulfonate / toluene / 2 h / 100 °C / Inert atmosphere 2.2: 1 h / Reflux; Inert atmosphere View Scheme |
trifluoromethylsulfonic anhydride
2-chloro-6-fluorophenol
2-chloro-6-fluorophenyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; | 100% |
With pyridine In dichloromethane at 0 - 20℃; for 3h; | |
With pyridine In dichloromethane at 0℃; for 3h; | 1.25 g |
With pyridine In dichloromethane at 0℃; for 3h; |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 97% |
2-chloro-6-fluorophenol
4-methyl-benzoyl chloride
2-chloro-6-fluorophenyl 4-methylbenzoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 96% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 96% |
With triethylamine In dichloromethane at 0℃; for 5h; | 96% |
With sodium hydroxide at 0℃; for 3h; |
2-chloro-6-fluorophenol
4-chloro-benzoyl chloride
4-chloro-benzoic acid 2-chloro-6-fluoro-phenyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 95% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 95% |
With triethylamine In dichloromethane at 0℃; for 5h; | 95% |
With sodium hydroxide In water at 0 - 5℃; | 85% |
With sodium hydroxide at 0 - 5℃; | 82% |
2-chloro-6-fluorophenol
methyl iodide
1-chloro-3-fluoro-2-methoxybenzene
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 20℃; for 3h; | 94% |
2-chloro-6-fluorophenol
4-fluorobenzoyl chloride
2-chloro-6-fluorophenyl 4-fluorobenzoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 94% |
With triethylamine In dichloromethane at 0℃; for 5h; | 94% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 92% |
With sodium hydroxide at 0℃; for 3h; |
2-chloro-6-fluorophenol
4-iodobenzoic acid chloride
2-chloro-6-fluorophenyl 4-iodobenzoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 93% |
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 93% |
With sodium hydroxide at 0℃; for 3h; |
2-chloro-6-fluorophenol
benzyl bromide
2-chloro-6-fluorophenyl phenylmethyl ether
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide for 12h; | 92% |
With potassium carbonate In acetone at 65℃; for 16h; |
2-chloro-6-fluorophenol
tert-butyldimethylsilyl chloride
(2-chloro-6-fluorophenoxy)(tert-butyl)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 25℃; | 90% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 20℃; for 1h; | 89% |
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 20℃; for 1h; | 89% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol Inert atmosphere; Schlenk technique; | 87% |
3-bromo-2-chloropyridine
2-chloro-6-fluorophenol
3-bromo-2-(2-chloro-6-fluorophenoxy)pyridine
Conditions | Yield |
---|---|
With caesium carbonate In dimethyl sulfoxide at 140℃; | 80% |
With caesium carbonate In dimethyl sulfoxide at 120℃; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 12h; | 78% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; | 74% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 20℃; for 1h; | 73% |
With di-isopropyl azodicarboxylate; triphenylphosphine at 20℃; for 1h; | 73% |
Ethyl 2-butynoate
2-chloro-6-fluorophenol
(E)-3-(2-chloro-6-fluoro-phenoxy)-but-2-enoic acid ethyl ester
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran Reflux; | 71% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 20℃; Mitsunobu Displacement; | 69% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In 1,2-dichloro-ethane at 60℃; | 67% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In 1,2-dichloro-ethane at 60℃; | 18 mg |
Conditions | Yield |
---|---|
With sodium hydroxide at 90℃; for 16h; | 64.5% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 16h; | 63% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 2h; | 62% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With sulfuric acid; potassium nitrate at 0℃; for 0.25h; | 61% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 20℃; Mitsunobu Displacement; | 44% |
2-chloro-6-fluorophenol
2-(tert-butoxycarbonylamino)ethyl methanesulfonate
Conditions | Yield |
---|---|
Stage #1: 2-chloro-6-fluorophenol With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: 2-(tert-butoxycarbonylamino)ethyl methanesulfonate In N,N-dimethyl-formamide at 100℃; for 16h; | 42% |
2-chloro-6-fluorophenol
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 80℃; for 12h; | 41.5% |
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