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inquiryGood quantity 4-(3-Phenylpropyl)pyridine Basic information Product Name: 4-(3-Phenylpropyl)pyridine Synonyms: 1-PHENYL-3-(4-PYRIDYL)PROPANE;4-(3-PHENYLPROPYL)PYRIDINE;4PPPY;4-PHENYL PR
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inquiry4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With methyloxorhenium(V)(2-(mercaptomethyl)thiophenolate) triphenylphosphine; triphenylphosphine In benzene at 20℃; for 0.3h; | 100% |
Conditions | Yield |
---|---|
Stage #1: allylbenzene With bis(1,5-cyclooctadiene)nickel (0); N,N′-bis(2,6-dimethylphenyl)imidazol-2-ylidene In toluene for 0.0833333h; Glovebox; Inert atmosphere; Stage #2: pyridine With bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum In toluene at 130℃; for 18h; Reagent/catalyst; Time; Sealed tube; regioselective reaction; | 95% |
With bis(1,5-cyclooctadiene)nickel (0); bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In toluene at 130℃; for 9h; Inert atmosphere; Autoclave; | 85% |
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; 1,2-bis(dimethylphosphanyl)ethane; lithium tert-butoxide In tetrahydrofuran at 80℃; for 12h; Reagent/catalyst; Inert atmosphere; regioselective reaction; | 95% |
3-Oxo-1-phenyl-3-pyridin-4-ylpropan
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With potassium hydroxide; hydrazine hydrate In various solvent(s) 120 deg C, 2 h then 160 deg C, 2 h, 195 deg C, 2 h; | 88% |
With potassium hydroxide; hydrazine hydrate Wolff-Kishner reduction; Heating; |
4-pyridinecarboxylic acid phenyl ester
9-(3-phenylpropyl)-9-borabicyclo[3.3.1]nonane
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With potassium fluoride; palladium diacetate; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 160℃; for 40h; Inert atmosphere; Glovebox; Sealed tube; | 87% |
4-pyridineboronic acid pinacol ester
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
Stage #1: 4-pyridineboronic acid pinacol ester; 3-phenylpropylmagnesium halide In tetrahydrofuran at -78 - 20℃; for 2.25h; Inert atmosphere; Stage #2: With trifluoroacetyl chloride In tetrahydrofuran at -78 - -40℃; for 18.5h; Inert atmosphere; Further stages; | 85% |
Conditions | Yield |
---|---|
With nickel(II) bromide dimethoxyethane; bathophenanthroline; lithium hexamethyldisilazane In iso-butanol at 60℃; for 16h; Suzuki-Miyaura coupling; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With nickel(II) iodide; (Z)-N'-cyanopicolinimidamide; trifluoroacetic acid; sodium iodide; zinc at 60℃; for 24h; Inert atmosphere; | 75% |
pyridine
4,4,5,5‐tetramethyl‐2‐[5‐phenyl‐1‐(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)propyl]‐1,3,2‐dioxaborolane
A
2-(3-phenylpropyl)pyridine
B
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With dimethyl zinc(II); lithium tert-butoxide In tetrahydrofuran; toluene at 120℃; for 3h; Inert atmosphere; Sealed tube; regioselective reaction; | A n/a B 50% |
picoline
1-phenyl-2-bromoethane
A
4-(3-phenylpropyl)pyridine
B
5,5-bis(phenethyl)-5,6,7,8-tetrahydroisoquinoline
Conditions | Yield |
---|---|
With potassium; ferric nitrate In ammonia | A 31% B 10% |
Conditions | Yield |
---|---|
at 250 - 350℃; under 15200 - 53200 Torr; for 3h; | 30% |
With potassium hexamethylsilazane In benzene at 80℃; for 60h; Schlenk technique; Sealed tube; | 26 %Spectr. |
Conditions | Yield |
---|---|
With water; zinc In acetonitrile Inert atmosphere; Reflux; regioselective reaction; | 13% |
Conditions | Yield |
---|---|
With ammonia; potassium amide anschl. mit Phenaethylbromid; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) Mg / 1.) ether, 40 deg C, 1 h, 2.) room temp., 3 h then 40 deg C, 2 h 2: 88 percent / 80percent aq. NH2NH2*H2O, KOH / various solvent(s) / 120 deg C, 2 h then 160 deg C, 2 h, 195 deg C, 2 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) Mg / 1.) ether, 40 deg C, 1 h, 2.) room temp., 3 h then 40 deg C, 2 h 2: 88 percent / 80percent aq. NH2NH2*H2O, KOH / various solvent(s) / 120 deg C, 2 h then 160 deg C, 2 h, 195 deg C, 2 h View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide; n-butyllithium In tetrahydrofuran; water |
pentaammine 1-phenyl-3-(4-pyridyl)propane cobalt(III) cation
A
4-(3-phenylpropyl)pyridine
C
(ethylenediaminetetraacetato)cobalt(II)(2-)
Conditions | Yield |
---|---|
In water Kinetics; determination of pseudo first order rate constant at 25°C; total ionic strength = 0.08 M, pH = 7.0; |
pyridine
allylbenzene
A
4-(1-phenylpropyl)pyridine
B
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 2-(3-mesityl-2,3-dihydro-1H-imidazol-1-yl)-N,N-dimethylethanamine; trimethylaluminum In toluene at 130℃; for 18h; Reagent/catalyst; regioselective reaction; | |
Stage #1: allylbenzene With bis(1,5-cyclooctadiene)nickel (0); 3-(2-(dimethylamino)ethyl)-1-mesityl-1H-imidazol-3-ium chloride; sodium hexamethyldisilazane In toluene for 0.0833333h; Glovebox; Inert atmosphere; Stage #2: pyridine With trimethylaluminum In toluene at 130℃; for 18h; Sealed tube; Overall yield = 88 %; regioselective reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene / 2 h / 60 °C / Inert atmosphere; Glovebox; Sealed tube 2: potassium fluoride; palladium diacetate; 1,2-bis-(dicyclohexylphosphino)ethane / toluene / 40 h / 160 °C / Inert atmosphere; Glovebox; Sealed tube View Scheme |
pyridine
4,4,5,5‐tetramethyl‐2‐[5‐phenyl‐1‐(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)propyl]‐1,3,2‐dioxaborolane
A
2-(3-phenylpropyl)pyridine
B
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With dimethyl zinc(II); lithium tert-butoxide In tetrahydrofuran; toluene at 120℃; for 3h; | A 9 %Spectr. B 12 %Spectr. C 42 %Spectr. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrazine hydrate 2: [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; 1,2-bis(dimethylphosphanyl)ethane; lithium tert-butoxide / tetrahydrofuran / 12 h / 80 °C / Inert atmosphere View Scheme |
4-(3-phenylpropyl)pyridine
manganese(II) thiocyanate
Conditions | Yield |
---|---|
In ethanol at 20℃; for 72h; Solvent; | 97.1% |
Conditions | Yield |
---|---|
In acetone for 0.5h; Heating; | 94% |
In acetone for 1h; Heating; | 94% |
In diethyl ether for 168h; Ambient temperature; | 66% |
In acetone Reflux; |
4-(3-phenylpropyl)pyridine
Conditions | Yield |
---|---|
With dihydrogen peroxide; methyltrioxorhenium(VII) In dichloromethane; water at 24℃; for 17h; | 94% |
With Oxone; sodium hydroxide In methanol | 93% |
With dihydrogen peroxide In water; acetone at 75℃; |
4-(3-phenylpropyl)pyridine
nickel(II) thiocyanate
Conditions | Yield |
---|---|
In ethanol at 20℃; for 144h; Solvent; | 93.8% |
Conditions | Yield |
---|---|
In ethanol; water at 20℃; for 72h; Solvent; | 90.1% |
4-(3-phenylpropyl)pyridine
[(2-(benzoimidazol-2-yl)-6-(3,5-dimethylpyrazol-1-yl)pyridine(-1H))RuCl(PPh3)]
Conditions | Yield |
---|---|
In methanol; dichloromethane at 25℃; for 5h; Inert atmosphere; Schlenk technique; | 90% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 168h; | 89.2% |
Conditions | Yield |
---|---|
Stage #1: 4-(3-phenylpropyl)pyridine; 1,12-dibromododecane In 4-methyl-2-pentanone for 18h; Heating / reflux; Stage #2: With Lewatit MP-64 anion resin (Cl-) In ethanol | 88% |
Conditions | Yield |
---|---|
In water for 72h; | 87.2% |
4-(3-phenylpropyl)pyridine
1-Bromo-3-phenylpropane
1,4-bis(3-phenylpropyl)pyridin-1-ium bromide
Conditions | Yield |
---|---|
In acetone Reflux; | 86% |
Conditions | Yield |
---|---|
In water for 72h; | 85.7% |
In ethanol at 20℃; |
4-(3-phenylpropyl)pyridine
nickel(II) thiocyanate
Conditions | Yield |
---|---|
In ethanol for 168h; Time; | 80.2% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In chloroform at 80℃; for 2h; | 78% |
Conditions | Yield |
---|---|
In ethanol for 168h; Time; | 75.8% |
4-(3-phenylpropyl)pyridine
3-Oxo-1-phenyl-3-pyridin-4-ylpropan
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; iron(II) tetrafluoroborate hexahydrate; oxygen; potassium tris(1-pyrazolyl)borate In benzonitrile at 90℃; for 18h; | 71% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 25℃; for 8h; | 70% |
4-(3-phenylpropyl)pyridine
α-(2-oxo-3-hydroxy-(5-bromo)indolinyl<3>)-2-methylpyridine
5-bromo-3-(pyridin-2-ylmethyl)-3-(4-(3-(pyridin-4-yl)propyl)phenyl)indolin-2-one
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 60℃; for 2h; Inert atmosphere; regioselective reaction; | 70% |
Conditions | Yield |
---|---|
In water; acetonitrile for 72h; | 70% |
Conditions | Yield |
---|---|
In butanone for 1.5h; Heating / reflux; | 66% |
4-(3-phenylpropyl)pyridine
1-phenyl-3-(pyridin-4-yl)propan-1-one
Conditions | Yield |
---|---|
With hydrogenchloride; tetrakis(tetrabutylammonium)decatungstate(VI); oxygen In water; acetonitrile at 20℃; for 0.75h; Flow reactor; Irradiation; | 66% |
With ammonium cerium (IV) nitrate; (1,4,7-trimethyl-1,4,7-triazacyclononane)ruthenium-(III) trichloride; silver perchlorate In water; tert-butyl alcohol at 20℃; for 4h; Reagent/catalyst; | 60% |
With N-hydroxyphthalimide; oxygen; cobalt(II) diacetate tetrahydrate In acetic acid at 90℃; for 18h; |
(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II)
4-(3-phenylpropyl)pyridine
[RuH(SCN)(CO)(4-(3-phenylpropyl)pyridine)(triphenylphosphine)2]
Conditions | Yield |
---|---|
In methanol by a react. of Ru-contg. compd. (0.1 mmol), a ligand (0.12 mmol) and NH4NCS in methanol soln.; the mixt. was refluxed for 3 h; cooling; the mixt. was filtered; | 65% |
(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II)
4-(3-phenylpropyl)pyridine
[RuHCl(CO)(4-(3-phenylpropyl)pyridine)(triphenylphosphine)2]
Conditions | Yield |
---|---|
In methanol by a react. of Ru-contg. compd. (0.1 mmol) and a ligand (0.12 mmol) in methanol soln.; the mixt. was refluxed for 3 h; cooling; the mixt. was filtered; | 62% |
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