Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:22862-76-6
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inquiry17-year experience in Phytochemicals Each product has passed very strict tests (NMR\MS\HPLC) Agents in 13 countries Certified by ISO 9001:2008 quality management system Leader Supplier of Botanical Reference Materials in China
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:22862-76-6
Min.Order:1 Gram
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Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:22862-76-6
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:22862-76-6
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FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:22862-76-6
Min.Order:1 Kilogram
FOB Price: $289.0 / 499.0
Type:Trading Company
inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Onchem specialized in APIs, chemical intermediate
Cas:22862-76-6
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
Cas:22862-76-6
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryANISOMYCIN CAS:22862-76-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
Cas:22862-76-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:22862-76-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C
Cas:22862-76-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:22862-76-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:22862-76-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryAnisomycinAppearance:Solid powder Storage:Dry, dark and at 0 - 4 C for short term (days to weeks) or -20 C for long term (months to years). Package:according to customers' requirements Application:Inhibitor Transportation:By air(EMS or EUB or FedEx o
high quality with GMP grade, EP, USP standard etc large scale with Competitive price Our products includes: Generic bulk peptide APIs, Cosmetic peptide, custom peptides and veterinary peptides. Application:Antibiotics
Cas:22862-76-6
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:22862-76-6
Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiryHigh quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle
Cas:22862-76-6
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:22862-76-6
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Cas:22862-76-6
Min.Order:0
Negotiable
Type:Manufacturers
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Why is SINOWAY:1) Specialized in pharmaceutical and healthcare industrial since 19872) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days.4) We have warehouse in USA with quickly shipment . Application:API
Cas:22862-76-6
Min.Order:0
Negotiable
Type:Trading Company
inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:22862-76-6
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
(2R,3S,4S)-3-acetoxy-N-(benzyloxycarbonyl)-4-hydroxy-2-(4-methoxybenzyl)pyrrolidine
(-)-anisomycin
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol under 760 Torr; for 0.25h; | 95% |
(2R,3S,4S)-3-Acetoxy-1-(tert-butoxycarbonyl)-4-(tert-butyldimethylsilyloxy)-2-(4-methoxybenzyl)pyrrolidine
(-)-anisomycin
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20℃; | 88% |
C19H27NO6
(-)-anisomycin
Conditions | Yield |
---|---|
With hydrogenchloride In methanol | 78% |
(2R,3S,4S)-3-acetoxy-1-benzyl-4-hydroxy-2-(4-methoxybenzyl)-pyrrolidine
(-)-anisomycin
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal In methanol; water for 3h; Yield given; |
(2R,3S,4S)-3-acetoxy-4-allyloxy-1-benzyl-2-(p-methoxybenzyl)pyrrolidine
(-)-anisomycin
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal 1.) MeOH, reflux, 2.) MeOH; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: HCl, water / palladium-charcoal 10percent / methanol / 48 h / Heating 2: HCl, H2 / palladium-charcoal 10percent / methanol; H2O / 3 h View Scheme |
Acetic acid (1S,2R)-2-azido-1-((R)-2-bromo-1-hydroxy-ethyl)-3-(4-methoxy-phenyl)-propyl ester
(-)-anisomycin
Conditions | Yield |
---|---|
With sodium acetate In methanol for 10h; Heating; Yield given; |
(-)-anisomycin
Conditions | Yield |
---|---|
With hydrogen; palladium dihydroxide In methanol; acetic acid at 20℃; under 3878.71 Torr; for 24h; | 76 mg |
(4R,5S,6S)-5-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyl)-2-phenyl-6-vinyl-5,6-dihydro-4H-1,3-oxazine
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 89 percent / Bu4NF / tetrahydrofuran / 1 h / 20 °C 2: 98 percent / pyridine / CH2Cl2 3: O3; O2 / methanol / -78 °C 4: 76 mg / H2 / Pd(OH)2 / methanol; acetic acid / 24 h / 20 °C / 3878.71 Torr View Scheme |
C20H21NO3
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 98 percent / pyridine / CH2Cl2 2: O3; O2 / methanol / -78 °C 3: 76 mg / H2 / Pd(OH)2 / methanol; acetic acid / 24 h / 20 °C / 3878.71 Torr View Scheme |
(4R,5S,6S)-4-(4-methoxybenzyl)-2-phenyl-6-vinyl-5,6-dihydro-4H-1,3-oxazin-5-yl acetate
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: O3; O2 / methanol / -78 °C 2: 76 mg / H2 / Pd(OH)2 / methanol; acetic acid / 24 h / 20 °C / 3878.71 Torr View Scheme |
(2S,3S)-pentene-1,2,3-triol
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1: DBU / acetonitrile / -30 °C 2: 1.) I2, NaHCO3, 2.) aq. HCl / 1.) MeCN, 0 deg C, 2.) MeOH, 20 deg C 3: NaHCO3 / methanol / 0 °C 5: NaHCO3 / methanol / 0 °C 6: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 7: imidazole / dimethylformamide / 20 °C 8: DMAP, Et3N / CH2Cl2 / 20 °C 9: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: NaHCO3 / methanol / 0 °C 3: NaHCO3 / methanol / 0 °C 4: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 5: imidazole / dimethylformamide / 20 °C 6: DMAP, Et3N / CH2Cl2 / 20 °C 7: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
(S,S)-2,2-dimethyl-4-(tert-butyldimethylsilyloxy)methyl-5-hydroxymethyl-1,3-dioxolane
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1: aq. HCl / tetrahydrofuran / 20 °C 2: DBU / acetonitrile / -30 °C 3: 1.) I2, NaHCO3, 2.) aq. HCl / 1.) MeCN, 0 deg C, 2.) MeOH, 20 deg C 4: NaHCO3 / methanol / 0 °C 6: NaHCO3 / methanol / 0 °C 7: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 8: imidazole / dimethylformamide / 20 °C 9: DMAP, Et3N / CH2Cl2 / 20 °C 10: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
(2S,3S,4R)-4-Amino-5-(4-methoxy-phenyl)-pentane-1,2,3-triol
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: NaHCO3 / methanol / 0 °C 2: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 3: imidazole / dimethylformamide / 20 °C 4: DMAP, Et3N / CH2Cl2 / 20 °C 5: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
(2R,3S,4S)-1-(tert-Butoxycarbonyl)-3,4-dihydroxy-2-(4-methoxybenzyl)pyrrolidine
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: imidazole / dimethylformamide / 20 °C 2: DMAP, Et3N / CH2Cl2 / 20 °C 3: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
[(1R,2S,3S)-2,3,4-Trihydroxy-1-(4-methoxy-benzyl)-butyl]-carbamic acid tert-butyl ester
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 2: imidazole / dimethylformamide / 20 °C 3: DMAP, Et3N / CH2Cl2 / 20 °C 4: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
(2R,3S,4S)-1-(tert-Butoxycarbonyl)-4-(tert-butyldimethylsilyloxy)-3-hydroxy-2-(4-methoxybenzyl)pyrrolidine
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: DMAP, Et3N / CH2Cl2 / 20 °C 2: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
2,2,2-Trichloro-acetimidic acid (1S,2S)-2-(2,2,2-trichloro-acetimidoyloxy)-1-(2,2,2-trichloro-acetimidoyloxymethyl)-but-3-enyl ester
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: 1.) I2, NaHCO3, 2.) aq. HCl / 1.) MeCN, 0 deg C, 2.) MeOH, 20 deg C 2: NaHCO3 / methanol / 0 °C 4: NaHCO3 / methanol / 0 °C 5: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 6: imidazole / dimethylformamide / 20 °C 7: DMAP, Et3N / CH2Cl2 / 20 °C 8: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
((1S,2S,3S)-2,3,4-Trihydroxy-1-iodomethyl-butyl)-carbamic acid tert-butyl ester
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 2: NaHCO3 / methanol / 0 °C 3: DEAD, Ph3P, PPTS / tetrahydrofuran / 0 °C 4: imidazole / dimethylformamide / 20 °C 5: DMAP, Et3N / CH2Cl2 / 20 °C 6: 88 percent / aq. HCl / methanol / 20 °C View Scheme |
divinylcarbinol
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 13 steps 1: D-(-)-DIPT, TBHP, Ti(O-i-Pr)4 / CH2Cl2 / -20 °C 2: Et3N, DMAP / CH2Cl2 3: 85 percent / copper(I) iodide / tetrahydrofuran / -10 °C 4: 94 percent / pyridine / CH2Cl2 / Ambient temperature 5: NaN3 / dimethylformamide / 7 h / 80 °C 6: 2N aq. HCl / 0.5 h 7: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 8: 89 percent / imidazole / dimethylformamide / 0 °C 9: pyridine / CH2Cl2 / 2 h / Ambient temperature 10: pyridine / 4 h / Ambient temperature 11: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 12: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 13: NaOAc / methanol / 10 h / Heating View Scheme |
(2S,3R)-1,2-epoxy-4-penten-3-ol
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 12 steps 1: Et3N, DMAP / CH2Cl2 2: 85 percent / copper(I) iodide / tetrahydrofuran / -10 °C 3: 94 percent / pyridine / CH2Cl2 / Ambient temperature 4: NaN3 / dimethylformamide / 7 h / 80 °C 5: 2N aq. HCl / 0.5 h 6: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 7: 89 percent / imidazole / dimethylformamide / 0 °C 8: pyridine / CH2Cl2 / 2 h / Ambient temperature 9: pyridine / 4 h / Ambient temperature 10: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 11: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 12: NaOAc / methanol / 10 h / Heating View Scheme |
(3S,4S)-trimethylsilyloxy oxirane
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 11 steps 1: 85 percent / copper(I) iodide / tetrahydrofuran / -10 °C 2: 94 percent / pyridine / CH2Cl2 / Ambient temperature 3: NaN3 / dimethylformamide / 7 h / 80 °C 4: 2N aq. HCl / 0.5 h 5: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 6: 89 percent / imidazole / dimethylformamide / 0 °C 7: pyridine / CH2Cl2 / 2 h / Ambient temperature 8: pyridine / 4 h / Ambient temperature 9: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 10: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 11: NaOAc / methanol / 10 h / Heating View Scheme |
(2S,3R)-1-(4-Methoxy-phenyl)-3-trimethylsilanyloxy-pent-4-en-2-ol
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1: 94 percent / pyridine / CH2Cl2 / Ambient temperature 2: NaN3 / dimethylformamide / 7 h / 80 °C 3: 2N aq. HCl / 0.5 h 4: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 5: 89 percent / imidazole / dimethylformamide / 0 °C 6: pyridine / CH2Cl2 / 2 h / Ambient temperature 7: pyridine / 4 h / Ambient temperature 8: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 9: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 10: NaOAc / methanol / 10 h / Heating View Scheme |
(3R,4R)-4-Azido-5-(4-methoxy-phenyl)-pent-1-en-3-ol
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 2: 89 percent / imidazole / dimethylformamide / 0 °C 3: pyridine / CH2Cl2 / 2 h / Ambient temperature 4: pyridine / 4 h / Ambient temperature 5: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 6: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 7: NaOAc / methanol / 10 h / Heating View Scheme |
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: 2N aq. HCl / 0.5 h 2: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 3: 89 percent / imidazole / dimethylformamide / 0 °C 4: pyridine / CH2Cl2 / 2 h / Ambient temperature 5: pyridine / 4 h / Ambient temperature 6: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 7: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 8: NaOAc / methanol / 10 h / Heating View Scheme |
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 89 percent / imidazole / dimethylformamide / 0 °C 2: pyridine / CH2Cl2 / 2 h / Ambient temperature 3: pyridine / 4 h / Ambient temperature 4: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 5: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 6: NaOAc / methanol / 10 h / Heating View Scheme |
Acetic acid (1S,2R)-2-azido-3-(4-methoxy-phenyl)-1-(S)-oxiranyl-propyl ester
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 2: NaOAc / methanol / 10 h / Heating View Scheme |
Methanesulfonic acid (1S,2R)-1-(4-methoxy-benzyl)-2-trimethylsilanyloxy-but-3-enyl ester
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1: NaN3 / dimethylformamide / 7 h / 80 °C 2: 2N aq. HCl / 0.5 h 3: 95 percent / OsO4, K3Fe(CN)6, K2CO3, DHQ-CLB, water / 2-methyl-propan-2-ol 4: 89 percent / imidazole / dimethylformamide / 0 °C 5: pyridine / CH2Cl2 / 2 h / Ambient temperature 6: pyridine / 4 h / Ambient temperature 7: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 8: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 9: NaOAc / methanol / 10 h / Heating View Scheme |
(-)-anisomycin
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: pyridine / CH2Cl2 / 2 h / Ambient temperature 2: pyridine / 4 h / Ambient temperature 3: 91 percent / n-Bu4NF / tetrahydrofuran / 1 h / 0 °C 4: 90 percent / lithium bromide / acetic acid; tetrahydrofuran / 24 h / Ambient temperature 5: NaOAc / methanol / 10 h / Heating View Scheme |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In tetrahydrofuran; water at 20℃; for 3h; | 100% |
(-)-anisomycin
propargyl bromide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 9h; | 95% |
(-)-anisomycin
benzyl bromide
(2R,3S,4S)-3-acetoxy-1-benzyl-4-hydroxy-2-(4-methoxybenzyl)-pyrrolidine
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; | 89% |
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