CAS No.23582-06-1,[2-(diphenylarsino)ethyl]diphenylphosphine Suppliers

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[2-(diphenylarsino)ethyl]diphenylphosphine CAS：23582-06-1

Cas:23582-06-1

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[2-(diphenylarsino)ethyl]diphenylphosphine

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Antimex Chemical Limied

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2-di(phenyl)arsanylethyl-di(phenyl)phosphane

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Synthetic route

: 12146-37-1, 124717-04-0
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

A: 53557-42-9
(1-diphenylphosphino-2-diphenylarsinoethane)molybdenum tetracarbonyl

B: 121-46-0
bicyclo[2.2.1]hepta-2,5-diene

Conditions

Conditions	Yield
In tetrahydrofuran reaction in a calorimeter under argon;	A 100% B n/a

...Expand

: 1174037-38-7
[Pd(3,4-Me2C6H2C(Me)=NN(H)(3'-(CF3)C4H2N2))Cl]

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: sodium perchlorate

: 2923-28-6
silver trifluoromethanesulfonate

: 1174037-43-4
[Pd(3,4-Me2C6H2C(Me)=NN(H)(3'-(CF3)C4H2N2))(PPh2(CH2)2AsPh2)]ClO4

Conditions

Conditions	Yield
In acetone byproducts: AgCl; Ag salt was added to soln. of Pd complex in acetone; stirred for 4 h; filtered through Celite; P-As ligand was added to filtrate; stirred for 2 h; NaClO4 was added; stirred for 1 h; H2O added; filtered; dried (vac.); elem. anal.;	99%

...Expand

: ammonium hexafluorophosphate

: chloro(η5-cyclopentadienyl)(1,10-phenanthroline)ruthenium(II)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 109011-10-1
bis(η5-cyclopentadienyl)bis(1,10-phenanthroline)(μ-1-(diphenylphosphino)-2-(diphenylarsino)ethane)diruthenium(II) hexafluorophosphate

Conditions

Conditions	Yield
In ethanol a suspn. of Ru-complex in EtOH was treated with an ethanol soln. of dppae under inert atmosphere, mixt. was heated under reflux for 20 min, filtered, cooled to room temp., a soln. of NH4PF6 in EtOH was added; ppt. was isolated by filtration, washed with Et2O; elem. anal.;	98%

...Expand

: 84651-76-3
(η-cyclopentadienyl)(η-cyclopentadiene)nickel tetrafluoroborate

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

A: 85412-97-1
cyclopentadienylnickel(diphenylphosphino(diphenylarsino)ethylidene)

B: 542-92-7
cyclopenta-1,3-diene

Conditions

Conditions	Yield
In chloroform under Ar, Ni complex and ligand stirred in CHCl3 for 5 min; filtered, filtrate dropped in ether, filtered, dried in vac., elem. anal.;	A 93% B n/a

...Expand

: ammonium hexafluorophosphate

: 174865-79-3
[Pd(5-(COH)C6H3C(H)N(cyclohexyl)-C2,N)(μ-Cl)]2

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 523977-74-4
[Pd(4-(COH)C6H3C(H)=NCy-C2,N)(1-diphenylphosphino-2-diphenylarsinoethane-P,As)][PF6]

Conditions

Conditions	Yield
In acetone ligand (2 equiv.) added to soln. of Pd complex in acetone; stirred at room temp. for 2 h; NH4PF6 (1 equiv.) added; stirred for 1 h; water added dropwise; stirred for 2 h; filtered; ppt. washed with water; dried in vac. over anhyd. CaCl2; recrystd. from CH2Cl2-n-hexane; elem. anal.;	88%

...Expand

: [Pd(CH2CMe2PtBu2)(μ-Cl)]2

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: Pd(2+)*Cl(1-)*((CH3)3C)2PC4H8(1-)*(C6H5)2PCH2CH2As(C6H5)2=(PdCl(((CH3)3C)2PC(CH3)2CH2)((C6H5)2PCH2CH2As(C6H5)2))

Conditions

Conditions	Yield
In benzene to stirred soln. (Pt2Cl2(Bu2tPCMe2CH2)2) in benzene added ape and react. mixt. stirred at 40°C for 5 h under N2 atm.; soln. concd., hexane added, solid filtered, washed with ether and vac. dried; elem. anal.;	86%

: 50978-00-2
chloro(methyl)(1,5-cyclooctadiene)platinum(II)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: PtCH3Cl(C6H5)2AsCH2CH2P(C6H5)2

Conditions

Conditions	Yield
In dichloromethane ligand was added to soln. of the Pt complex in CH2Cl2, mixt. stirred at room temp. for 1 h; concd., filtered, washed with hexane and ether, dried under reduced pressure; elem. anal.;	86%

: ammonium hexafluorophosphate

: 174865-79-3
[Pd(5-(COH)C6H3C(H)N(cyclohexyl)-C2,N)(μ-Cl)]2

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 521070-28-0
[Pd(5-(COH)C6H3C(H)=NCy-C2,N)(1-diphenylphosphino-2-diphenylarsinoethane-P,As)][PF6]

Conditions

Conditions	Yield
With silver trifluorosulfonate In acetone byproducts: AgCl; AgOSO2CF3 (1 equiv.) added to soln. of Pd complex in acetone; stirred for 1 h; filtered through Celite; ligand (2 equiv.) and NH4PF6 (3 equiv.) added to soln.; stirred for 12 h; filtered; ppt. recrystd. from CHCl3-n-hexane; elem. anal.;	86%

...Expand

: 13755-29-8
sodium tetrafluoroborate

: 308108-82-9
[Pt(6-neo-pentyl-2,2'-bipyridine(1-)κC,κ2N,N')Cl]

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 507271-10-5
[Pt(C10H7N2CH2C(CH3)2CH2)(C6H5)2PCH2CH2As(C6H5)2](1+)*BF4(1-)=[[PtC10H7N2CH2C(CH3)2CH2](C6H5)2PCH2CH2As(C6H5)2](BF4)

Conditions

Conditions	Yield
In acetone NaBF4 was added to Me2CO soln. of 1 equiv. of Pt- and 1 equiv. of P-compd., resp., mixt. was stirred in for 4 h; solvent was evapd. to dryness, residue was recrystd. from CH2Cl2/Et2O, elem. anal.;	84%

...Expand

: Rh(1,5-cyclooctadiene)(η3-2-Me-allyl)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 81178-02-1
[η3-(2-Me-C3H4)Rh(arphos)]

Conditions

Conditions	Yield
In hexane; dichloromethane a soln. of ligand in CH2Cl2 was added a soln. of complex in hexane and stirred for 0.5 h, N2 atm.; evapn. in vac., repptn. from CH2Cl2 with hexane at -30°C; elem. anal.;	83%

: 7647-01-0
hydrogenchloride

: 10466-65-6
potassium perrhenate

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 181574-50-5
ReOCl3(1-diphenylphosphino-2-diphenylarsinoethane)

Conditions

Conditions	Yield
In hydrogenchloride; propan-1-ol refluxing in concd. HCl/PrOH=1:7 v/v for 24 h (pptn.); collection (filtration), washing (EtOH), drying (vac.);	83%

...Expand

: (C5Me5)MoCo2(CO)8CCO2-iPr

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: {C5(CH3)5}MoCo2(CO)6CCO2CH(CH3)2((C6H5)2AsCH2CH2P(C6H5)2)

Conditions

Conditions	Yield
In tetrahydrofuran soln. of MoCo2 complex and arphos in THF stirred at ambient temp. for 45 min under dry N2; chromy. (SiO2; ether/hexane, 10/90); elem. anal.;	82%

: 13755-29-8
sodium tetrafluoroborate

: PtCl(C10H7N2C(CH3)2)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: Pt(C10H7N2C(CH3)2)((C6H5)2AsCH2CH2P(C6H5)2)(1+)*BF4(1-)=[Pt(C10H7N2C(CH3)2)((C6H5)2PCH2CH2As(C6H5)2)]BF4

Conditions

Conditions	Yield
In acetone addn. of 1 equiv. of ligand to Pt-complex soln., then addn. of excess NaBF4, stirring (room temp.); evapn., dissoln. in CH2Cl2, filtration, concn., crystn. on Et2O addn.; elem. anal.;	81.4%

...Expand

: rhenium (III) chloride

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: Re3Cl9(arphos)1.5

Conditions

Conditions	Yield
In ethanol combining of Re3Cl9 and arphos as solids, addn. of ethanol, pptn.; elem. anal.;	80%

: 13755-29-8
sodium tetrafluoroborate

: 308108-82-9
[Pt(6-neo-pentyl-2,2'-bipyridine(1-)κC,κ2N,N')Cl]

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: [Pt2(C10H7N2CH2C(CH3)2CH2)2(μ-(1-diphenylphosphino-2-diphenylarsinoethane))](BF4)2

Conditions

Conditions	Yield
In acetone NaBF4, Pt-compd. and 0.5 equiv. of P-compd. were stirred in Me2CO soln.at room temp. for 1 d; solvent was evapd. to dryness, residue was recrystd. from CH2Cl2/Et2O, elem. anal.;	80%

...Expand

: 26042-63-7
silver(I) hexafluorophosphate

: [Pd(CH2CMe2PtBu2)(μ-Cl)]2

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 99279-36-4
(Pd(((CH3)3C)2PC(CH3)2CH2)((C6H5)2PCH2CH2As(C6H5)2))(1+)*PF6(1-)=(Pd(((CH3)3C)2PC(CH3)2CH2)((C6H5)2PCH2CH2As(C6H5)2))PF6

Conditions

Conditions	Yield
In methanol; dichloromethane byproducts: AgCl; to stirred soln. (Pd2Cl2(But2PCMe2CH2)2) in CH2Cl2 added 2 equiv. AgPF6in methanol and mixt. stirred for 30 min, AgCl centrifuged and filtered, ape added and react. mixt. stirred at room temp. for 4 h under N2 atm.; soln. concd., ether added; elem. anal.;	78%

...Expand

: [Pt2((COMe)2H)2(μ-Cl)2]

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 264142-17-8, 263870-12-8
trans-P-Pt-Cl-[Pt(COMe)Cl(1-(diphenylarsino)-2-(diphenylphosphino)ethane]

: 263870-12-8, 264142-17-8
trans-P-Pt-COMe-[Pt(COMe)Cl(1-(diphenylarsino)-2-(diphenylphosphino)ethane)]

Conditions

Conditions	Yield
In acetone byproducts: CH3CHO; arsinophosphinoethane deriv. was dropped in acetone to acetone soln. of Pt-complex at -30 °C (ratio 2:1), mixt. was slowly warmed up to room temp.; isomer ratio trans-P-Pt-Cl : trans-P-Pt-COMe = 9:1 (detn. by (13)P-NMR);crystn. of trans-P-Pt-Cl isomer within 12 h, filtration, dried in vac.;	A 78% B n/a

...Expand

: 13755-29-8
sodium tetrafluoroborate

: PtCl(C10H7N2C(CH3)2)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: [Pt2(C10H7N2C(CH3)2)2(μ-Ph2PCH2CH2AsPh2)](BF4)2

Conditions

Conditions	Yield
In acetone addn. of 0.5 equiv. of ligand to Pt-complex soln., then addn. of excessNaBF4, stirring (room temp., 3 h); evapn., dissoln. in CH2Cl2, filtration, concn., crystn. on Et2O addn.; elem. anal.;	76%

...Expand

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: C26H24AsF2P

Conditions

Conditions	Yield
With Carbonyl fluoride In dichloromethane at 25℃;	75%

: cis-dichloro(2,2′-bipyridine)ruthenium(II)chloride

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 2923-28-6
silver trifluoromethanesulfonate

: [{Ru(2,2'-bipyridine)2Cl}2{μ-Ph2P(CH2)2AsPh2}][CF3SO3]2

Conditions

Conditions	Yield
Stage #1: cis-dichloro(2,2′-bipyridine)ruthenium(II)chloride; silver trifluoromethanesulfonate In acetone at 20℃; for 2h; Inert atmosphere; Stage #2: 1-diphenylarsino-2-diphenylphosphinoethane In ethanol; toluene at 20℃; for 456h; Sealed tube; Inert atmosphere;	74%

...Expand

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: {N(PPh3)2}2{Ru4(μ-H)2(CO)12}

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: Cu2Ru4H2*12CO*(C6H5)2AsCH2CH2P(C6H5)2=Cu2Ru4H2((C6H5)2As(CH2)2P(C6H5)2)(CO)12

Conditions

Conditions	Yield
In dichloromethane under N2; Ru containing salt treated with Cu-complex at -30°C; stirred for 1 min; bidentate ligand added; warmed to ambient temp. with stirring; solvent removed (reduced pressure);; extn. (CH2Cl2:Et2O 1:4); extract filtered (Celite); solvent removed (reduced pressure); chromy. (Florisil, -20°C, CH2Cl2-light petroleum); crystn. (CH2Cl2-light petroleum), elem. anal.;;	72%

...Expand

: 92390-26-6
chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: (η5-pentamethylcyclopentadienyl)ruthenium(II)chloro[(1-diphenylarsanyl-2-diphenylphosphanyl)ethylene]

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: cyclooctadiene; stirring a soln. of (C5Me5)Ru(COD)Cl and the ligand for 24 h, all manipulations under argon, nitrogen or vacuum contg. less than 1 ppm oxygen and water; filtn., removal of the solvent in vacuum, addn. of hexane and THF at -78°C, warming to 40°C, stirring for 15 min, filtn., standing at room temp. overnight, filtn., washing with hexane, drying in vacuum, elem. anal.;	72%

Yield

In tetrahydrofuran byproducts: cyclooctadiene; stirring a soln. of (C5Me5)Ru(COD)Cl and the ligand for 24 h, all manipulations under argon, nitrogen or vacuum contg. less than 1 ppm oxygen and water; filtn., removal of the solvent in vacuum, addn. of hexane and THF at -78°C, warming to 40°C, stirring for 15 min, filtn., standing at room temp. overnight, filtn., washing with hexane, drying in vacuum, elem. anal.;

72%

: 82581-56-4
NEt4{Nb(CO)6}

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: [Nb(CO)4((C6H5)2P(CH2)2As(C6H5)2)2](1-)

B: 83536-55-4
[(C2H5)4N](1+)*[Nb(CO)4(C6H5)2As(CH2)2P(C6H5)2](1-)=[(C2H5)4N][Nb(CO)4(C6H5)2As(CH2)2P(C6H5)2]

Conditions

Conditions	Yield
In tetrahydrofuran Irradiation (UV/VIS); under N2, about equimolar amts. of (Et4N)Nb(CO)6 and phosphine dissolved in THF, irradiated (UV, Duran filter) for 70 min; pptd. by stirring concd. soln. with heptane, ppt. filtered off, washed with THF/heptane, dried under high vac. (0.01 Torr, 5 h);	A n/a B 71%

...Expand

: 117707-13-8
Co3(CO)9CCO2(menthyl)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: (Ph2AsCH2CH2PPh2)Co3O2(CO)7CCO2(menthyl)

Conditions

Conditions	Yield
In tetrahydrofuran stirred under N2; 15 min at 40°C, 30 min at room temp.; progress of reaction followed by TLC (ether/hexane: 15/85); chromd. (silica gel; ether/hexane: 15/85); elem. anal.;	69%

: 174865-79-3
[Pd(5-(COH)C6H3C(H)N(cyclohexyl)-C2,N)(μ-Cl)]2

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 523977-71-1
[(Pd[4-(COH)C6H3C(H)=NCy-C2,N](Cl))2(μ-1-diphenylphosphino-2-diphenylarsinoethane)]

Conditions

Conditions	Yield
In acetone ligand (1 equiv.) added to soln. of Pd complex in acetone; stirred at room temp. for 12 h; filtered; solid dried in vac.; recrystd. from CHCl3-n-hexane; elem. anal.;	68%

: 157072-60-1, 166941-05-5, 16971-33-8, 61521-25-3
carbonylchlorohydridotris(triphenylphosphine)ruthenium(II)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: [RuHCl(CO)(P(C6H5)3)((C6H5)2PCH2CH2As(C6H5)2)]

Conditions

Conditions	Yield
In toluene (N2); reflux (1.5 h); filtration, concn., pptn. with n-pentane, filtration, washing (CH2Cl2/n-pentane, then n-pentane), drying (vac.); elem. anal.;	66%

: {N(PPh3)2}2{Ru4(μ-H)2(CO)12}

: 86728-82-7
tetrakis(acetonitrile)silver(I) hexafluorophosphate

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: Ag2Ru4H2*12CO*(C6H5)2AsCH2CH2P(C6H5)2=Ag2Ru4H2((C6H5)2As(CH2)2P(C6H5)2)(CO)12

Conditions

Conditions	Yield
In dichloromethane under N2; Ru containing salt treated with Ag-complex at -30°C; stirred for 1 min; bidentate ligand added; warmed to ambient temp. with stirring; solvent removed (reduced pressure);; extn. (CH2Cl2:Et2O 1:4); extract filtered (Celite); solvent removed (reduced pressure); chromy. (alumina, -20°C, CH2Cl2-light petroleum); crystn. (CH2Cl2-light petroleum); elem. anal.;;	65%

...Expand

: {dicarbonylnitrosyl(cyclohexadienyl(phenyl))manganese}{PF6}

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 142042-19-1
{(C6H5C6H6)Mn(NO)(CH2P(C6H5)2)(CH2As(C6H5)2)}(1+)*PF6(1-)={(C6H5C6H6)Mn(NO)(CH2P(C6H5)2)(CH2As(C6H5)2)}PF6

Conditions

Conditions	Yield
In dichloromethane Mn complex and ligand suspd. in CH2Cl2 and refluxed, color changed from yellow to reddish; after 5.5 h concd., pptn. with diethyl ether, extd. (overnight, Soxhlet, toluene), pptn. (room temp., CH3CN soln. layered with Et2O), elem. anal.;	65%

: 84433-24-9, 61793-17-7
hexacarbonyl(μ-1,1,3,3-teramethyl-2-thiocarbonylcyclohexane)diiron

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

A: 128178-28-9
hexacarbonyl(1-diphenylphosphino-2-diphenylarsinoethane)(μ-1,1,3,3-teramethyl-2-thiocarbonylcyclohexane)diiron(Fe-Fe)

B: 128178-29-0
pentacarbonyl(1-diphenylphosphino-2-diphenylarsinoethane)(μ-1,1,3,3-teramethyl-2-thiocarbonylcyclohexane)diiron(Fe-Fe)

Conditions

Conditions	Yield
In hexane; toluene dropwise addn. of ligand in toluene to the Fe compd. in hexane under N2 and stirring at 20°C for 18 h; concn. (vac.), chromy. on silica gel, eluating with toluene-hexane, evapn. (vac.) and recrystn. from hexane; elem. anal.;	A 64% B 11%

...Expand

: 22337-78-6
carbonyldihydridotris(triphenylphosphine)ruthenium(II)

: 23582-06-1
1-diphenylarsino-2-diphenylphosphinoethane

: 80515-25-9
RuH2(CO)P(C6H5)3(P(C6H5)2C2H4As(C6H5)2)

Conditions

Conditions	Yield
In toluene A soln. of reagents in toluene was refluxed for 1.5 h (inert atm.);; elem. anal.;;	64%

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