DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:2378-95-2
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryAbout Product Technical Details CAS: 2378-95-2 MF: C17H24N2O5 MW: 336.38 EINECS: 219-161-5 Product Categories: Heterocyclic Compounds Mol File: 2378-95-2.mol
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryName: N-(4-Methylaminobenzoyl)-L-lutamic acid diethylester Synonyms: diethyl N-[4-(methylamino)benzoyl]-L-glutamate CAS: 2378-95-2 MF: C17H24N2O5 Appearance: White powder Storage:Store in cool and dry place, away from sun light. Package:25KG/Drum
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inquiryAppearance:Off-white to light brown powder Storage:Room temperature Package:25kg/drum Application:Chemicals Transportation:Express/Sea/Air Port:Any port in china
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquirydiethyl N-[4-(methylamino)benzoyl]-L-glutamate CAS:2378-95-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance:off white or light brown powder Storage:Stored in a dark, cool, ventilated and dry place Package:NW 1kg/foil bag; 20-25kg/drum or carton Application:pharmaceutical intermediate. Transportation:by air/sea/express,according to demand. Port:
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryProduct name: N-(4-Methylaminiobenzoyl)-L-Glutamic Acid Diethylester CAS No.:2378-95-2 Molecule Formula:C17H24N2O5 Molecule Weight:336.38 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise St
Cas:2378-95-2
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inquirydiethyl N-[4-(methylamino)benzoyl]-L-glutamate Chemical Properties Melting point 88-89 °C Boiling point 518.3±50.0 °C(Predicted) density 1.165±0.06 g/cm3(Predicted) storage temp. Keep in dark place,Sealed in dry,
Cas:2378-95-2
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryN-(4-Methylaminobenzoyl)-L-lutamic acid diethylesterAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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inquirybest seller Application:API
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inquirydiethyl N--L-glutamate
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol under 2482.3 Torr; for 3h; | 80% |
diethyl N-(p-aminobenzoyl)-L-glutamate
methyl iodide
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 26h; | 23% |
With N-ethyl-N,N-diisopropylamine In toluene at 90℃; for 18h; |
N-(4-iodo-benzoyl)L-glutamic acid
methylamine
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With sodium hydroxide; copper at 125℃; Behandeln des Dinatrium-Salzes der erhaltenen N-<4-Methylamino-benzoyl>-L-glutaminsaeure mit Chlorwasserstoff enthaltendem Aethanol; |
diethyl N-(p-aminobenzoyl)-L-glutamate
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 94 percent / sodium cyanoborohydride, bromocresol green, acetic acid / ethanol / 48 h / Ambient temperature 2: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature 3: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr View Scheme |
diethyl N--L-glutamate
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature 2: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr View Scheme |
N-(4-aminobenzoyl)-L-glutamic acid
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium nitrite; aqueous hydrochloric acid; aqueous potassium iodide solution / Diazotization 2: aq. NaOH solution; copper / 125 °C / Behandeln des Dinatrium-Salzes der erhaltenen N-<4-Methylamino-benzoyl>-L-glutaminsaeure mit Chlorwasserstoff enthaltendem Aethanol View Scheme |
diethyl N-(p-aminobenzoyl)-glutamate
potassium carbonate
methyl iodide
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
In dichloromethane; ethyl acetate; N,N-dimethyl-formamide |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
<6-(bromomethyl)-4-oxo-3(4H)-quinazolinyl>methyl 2,2-dimethylpropanoate
Diethyl N-(4-(N-((3,4-dihydro-4-oxo-3-((pivaloyl)oxy) methyl-6-quinazolinyl)methyl)methylamino)benzoyl)-L-glutamate
Conditions | Yield |
---|---|
With calcium carbonate In dimethyl amine at 50℃; for 24h; | 89.3% |
Iodoethanol
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
diethyl N-<4-benzoyl>-L-glutamate
Conditions | Yield |
---|---|
In various solvent(s) at 100℃; for 5h; | 86% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
4-methoxy-6-oxo-7-chloro-5H-pyrimido<4,5-b><1,4>thiazine
diethyl N-methyl-N-<4-methoxy-6-oxo-5H-pyrimido<4,5-b><1,4>thiazin-7-yl>-p-aminobenzoyl-L-glutamate
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane; water at 18 - 20℃; for 5h; | 81% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
2,4-diamino-6-(bromomethyl)pyrido<3,2-d>pyrimidine
diethyl N-[4-[(2,4-diaminopyrido[3,2-d]pyrimidin-6-ylmethyl)methylamino]benzoyl]-L-glutamate
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 20℃; for 2h; | 72% |
In N,N-dimethyl acetamide for 6h; Heating; Yield given; |
2,4-diamino-5-(chloromethyl)furo[2,3-d]pyrimidine
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 40℃; for 72h; | 68% |
diethyl N--L-glutamate
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol under 2482.3 Torr; for 3h; | 80% |
diethyl N-(p-aminobenzoyl)-L-glutamate
methyl iodide
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 26h; | 23% |
With N-ethyl-N,N-diisopropylamine In toluene at 90℃; for 18h; |
N-(4-iodo-benzoyl)L-glutamic acid
methylamine
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With sodium hydroxide; copper at 125℃; Behandeln des Dinatrium-Salzes der erhaltenen N-<4-Methylamino-benzoyl>-L-glutaminsaeure mit Chlorwasserstoff enthaltendem Aethanol; |
diethyl N-(p-aminobenzoyl)-L-glutamate
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 94 percent / sodium cyanoborohydride, bromocresol green, acetic acid / ethanol / 48 h / Ambient temperature 2: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature 3: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr View Scheme |
diethyl N--L-glutamate
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / sodium cyanoborohydride, bromocresol green, aq. acetic acid / acetonitrile / 1 h / Ambient temperature 2: 80 percent / hydrogen, HCl / palladium on carbon / ethanol / 3 h / 2482.3 Torr View Scheme |
N-(4-aminobenzoyl)-L-glutamic acid
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium nitrite; aqueous hydrochloric acid; aqueous potassium iodide solution / Diazotization 2: aq. NaOH solution; copper / 125 °C / Behandeln des Dinatrium-Salzes der erhaltenen N-<4-Methylamino-benzoyl>-L-glutaminsaeure mit Chlorwasserstoff enthaltendem Aethanol View Scheme |
diethyl N-(p-aminobenzoyl)-glutamate
potassium carbonate
methyl iodide
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
In dichloromethane; ethyl acetate; N,N-dimethyl-formamide |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
<6-(bromomethyl)-4-oxo-3(4H)-quinazolinyl>methyl 2,2-dimethylpropanoate
Diethyl N-(4-(N-((3,4-dihydro-4-oxo-3-((pivaloyl)oxy) methyl-6-quinazolinyl)methyl)methylamino)benzoyl)-L-glutamate
Conditions | Yield |
---|---|
With calcium carbonate In dimethyl amine at 50℃; for 24h; | 89.3% |
Iodoethanol
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
diethyl N-<4-benzoyl>-L-glutamate
Conditions | Yield |
---|---|
In various solvent(s) at 100℃; for 5h; | 86% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
4-methoxy-6-oxo-7-chloro-5H-pyrimido<4,5-b><1,4>thiazine
diethyl N-methyl-N-<4-methoxy-6-oxo-5H-pyrimido<4,5-b><1,4>thiazin-7-yl>-p-aminobenzoyl-L-glutamate
Conditions | Yield |
---|---|
With triethylamine In 1,4-dioxane; water at 18 - 20℃; for 5h; | 81% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
2,4-diamino-6-(bromomethyl)pyrido<3,2-d>pyrimidine
diethyl N-[4-[(2,4-diaminopyrido[3,2-d]pyrimidin-6-ylmethyl)methylamino]benzoyl]-L-glutamate
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 20℃; for 2h; | 72% |
In N,N-dimethyl acetamide for 6h; Heating; Yield given; |
2,4-diamino-5-(chloromethyl)furo[2,3-d]pyrimidine
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 40℃; for 72h; | 68% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
9-bromomethyl-3-methylbenzo[f]quinazolin-1(2H)-one
diethyl N-(4-(((1,2-dihydro-3-methyl-1-oxobenzoquinazolin-9-yl)methyl)methylamino)benzoyl)-L-glutamate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100 - 110℃; | 53% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
3,9-dimethylbenzo(f)-quinazolin-1(2H)-one
diethyl N-(4-(((1,2-dihydro-3-methyl-1-oxobenzoquinazolin-9-yl)methyl)methylamino)benzoyl)-L-glutamate
Conditions | Yield |
---|---|
53% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
6-(Bromomethyl)-2,4-dimethoxyquinazoline
(S)-2-{4-[(2,4-Dimethoxy-quinazolin-6-ylmethyl)-methyl-amino]-benzoylamino}-pentanedioic acid diethyl ester
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In N,N-dimethyl-formamide at 70℃; | 51% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
4(3H)-oxo-6-(bromomethyl)-2-methyl quinazoline
diethyl N-<4--N-methylamino>benzoyl>-L-glutamate
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In N,N-dimethyl-formamide at 80℃; for 18h; | 41% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
3-Amino-6-bromomethyl-2-carbamoylpyrazine 4-Oxide
Diethyl N-<4-<<(5-Amino-6-carbamoylpyrazinyl)methyl>methylamino>benzoyl>-L-glutamate N-Oxide
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide for 144h; Ambient temperature; | 40% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
1,2,5,6-tetrahydro-3-methyl-1-oxobenzo[f]-quinazolin-9-sulfonyl chloride
diethyl N-<4-quinazolin-9-yl)sulfonyl>amino>benzoyl>-L-glutamate
Conditions | Yield |
---|---|
In pyridine Ambient temperature; | 40% |
40% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
5-Bromomethyl-7H-pyrrolo[2,3-d]pyrimidine-2,4-diamine
(S)-2-{4-[(2,4-Diamino-7H-pyrrolo[2,3-d]pyrimidin-5-ylmethyl)-methyl-amino]-benzoylamino}-pentanedioic acid diethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 5h; Ambient temperature; | 38% |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
2-bromomethyl-3-phenyl-7-trifluoromethylquinoxaline
diethyl N-[4-(3-phenyl-7-trifluoromethylquinoxalin-2-yl)methyl]-N-methyl-benzoyl-L-glutamate
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide at 20℃; for 72h; | 22% |
oxirane
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
diethyl N-<4-benzoyl>-L-glutamate
Conditions | Yield |
---|---|
In acetic acid 1.) 0 deg C, 2.) room temperature, 17 h; Yield given; |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Acetic acid 6-bromomethyl-4-oxo-3,4-dihydro-quinazolin-2-ylmethyl ester
Conditions | Yield |
---|---|
With calcium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
2-Amino-6-bromomethyl-3H-pyrido[3,2-d]pyrimidin-4-one
Diethyl 8-Deaza-N10-methylfolic Acid
Conditions | Yield |
---|---|
In N,N-dimethyl acetamide for 6h; Heating; Yield given; |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
6-(bromomethyl)-4-chloro-2-methylquinoline
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In N,N-dimethyl-formamide at 70℃; for 18h; |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
2-amino-6-(bromomethyl)-4-hydroxy-5,6,7,8-tetrahydroquinazoline hydrobromide
Conditions | Yield |
---|---|
With magnesium oxide In N,N-dimethyl acetamide at 120 - 135℃; for 18h; |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 53 percent / dimethylformamide / 100 - 110 °C 2: 94 percent / aq. NaOH / ethanol / Ambient temperature View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 40 percent / pyridine / Ambient temperature 2: 99 percent / 1N aq. NaOH / Ambient temperature View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
N-(4-(N-((3,4-dihydro-4-oxo-6-quinazolinyl)methyl) methylamino)benzoyl)-L-glutamic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 89.3 percent / CaCO3 / dimethylamine / 24 h / 50 °C 2: 62.1 percent / 1.00 N aq. NaOH / H2O; ethanol / 24 h / 22 °C View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
N - p-[ N-(3,4-dihydro-2-methoxy-4-oxoquinazolin-6-ylmethyl)-N-methylamino]benzoyl-L-glutamic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 51 percent / 2,6-lutidine / dimethylformamide / 70 °C 2: 83 percent / 1 N aq. NaOH / ethanol; H2O / 14.5 h / 60 °C View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
diethyl N-<4-ethyl>-N-methylamino>benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h 2: 80 percent / pyridine / 1 h / Ambient temperature 3: 20 percent / dimethylformamide / 24 h / 90 - 100 °C View Scheme | |
Multi-step reaction with 3 steps 1: 86 percent / various solvent(s) / 5 h / 100 °C 2: 80 percent / pyridine / 1 h / Ambient temperature 3: 20 percent / dimethylformamide / 24 h / 90 - 100 °C View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
diethyl N-<4-benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h 2: 80 percent / pyridine / 1 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: 86 percent / various solvent(s) / 5 h / 100 °C 2: 80 percent / pyridine / 1 h / Ambient temperature View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamic acid 5'-monophosphate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h 2: 80 percent / pyridine / 1 h / Ambient temperature 3: 20 percent / dimethylformamide / 24 h / 90 - 100 °C 4: 42 percent / NaHCO3 / dimethylformamide / 2 h / Ambient temperature 5: 1.) Zn, Cu, acetylacetone, 2.) NaOH / 1.) DMF, 50 deg C to 55 deg C, 1.5 h, 2.) ethanol, 48 h View Scheme | |
Multi-step reaction with 5 steps 1: 86 percent / various solvent(s) / 5 h / 100 °C 2: 80 percent / pyridine / 1 h / Ambient temperature 3: 20 percent / dimethylformamide / 24 h / 90 - 100 °C 4: 42 percent / NaHCO3 / dimethylformamide / 2 h / Ambient temperature 5: 1.) Zn, Cu, acetylacetone, 2.) NaOH / 1.) DMF, 50 deg C to 55 deg C, 1.5 h, 2.) ethanol, 48 h View Scheme |
diethyl <4-(N-methylamino)benzoyl>-L-glutamate
diethyl N-<4-amino>ethyl>-N-methylamino>benzoyl>-L-glutamate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: aq. acetic acid / 1.) 0 deg C, 2.) room temperature, 17 h 2: 80 percent / pyridine / 1 h / Ambient temperature 3: 20 percent / dimethylformamide / 24 h / 90 - 100 °C 4: 42 percent / NaHCO3 / dimethylformamide / 2 h / Ambient temperature View Scheme | |
Multi-step reaction with 4 steps 1: 86 percent / various solvent(s) / 5 h / 100 °C 2: 80 percent / pyridine / 1 h / Ambient temperature 3: 20 percent / dimethylformamide / 24 h / 90 - 100 °C 4: 42 percent / NaHCO3 / dimethylformamide / 2 h / Ambient temperature View Scheme |
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