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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

(9H-Fluoren-9-yl)-methyldecyl-(2-oxoethyl)-carbamate

Cas:239088-22-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL

Cas:239088-22-3

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

9H-FLUOREN-9-YLMETHYL DECYL(2-OXOETHYL)CARBAMATE

Cas:239088-22-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

(9H-Fluoren-9-yl)methyldecyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Hangzhou Think Chemical Co. Ltd

HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Other

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Carbamic acid,decyl(2-oxoethyl)-, 9H-fluoren-9-ylmethyl ester (9CI)

Cas:239088-22-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

Product Name: (9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate Synonyms: (9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate;2-[N-(9-FluorenylMethox…Appearance:Solid powder Storage:Sealed,light and oxygen resistant Package:aluminum foil bag,carton

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Other

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratoryAppearance:White to light yellow solid Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

9H-fluoren-9-ylmethyl N-decyl-N-(2-oxoethyl)carbamate cas no. 239088-22-3 98%

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Huarong Pharm Co., Ltd.

High qualityAppearance:White powder Storage:Room temperature Package:Aluminum bag Application:Used in producing API Transportation:By air Port:Beijing

2-[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

Carbamic acid,decyl(2-oxoethyl)-, 9H-fluoren-9-ylmethyl ester (9CI)

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Guangdong Juda Chemical Industrial Co.,Limited

Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate CAS No.239088-22-3

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:yellow to light brown crystals Storage:Room temperature with sealed well Package:according to the clients requirement Applicatio

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

(9H-FLUOREN-9-YL)METHYL?ECYL(2-OXOETHYL)CARBAMATEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

(9H-FLUOREN-9-YL)METHYL?ECYL(2-OXOETHYL)CARBAMATE

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:100mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any po

2-[N-(9-Fluorenylmethoxycarbonyl)-N-decylamino]ethanal

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

9H-fluoren-9-ylmethyl N-decyl-N-(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

The factory supplies Application:manufacturing supplies

Carbamicacid,decyl(2-oxoethyl)-,9H-fluoren-9-ylmethylester(9CI)

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

239088-22-3

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

home-produced Application:medicine

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

suzhou BetterBioChem Co., Ltd.

Betterbiochem is specialized in APIs, pharmaceutical intermediates & fine chemicals. 1. The best quality, competitive price. 2. The best service before or after shipment. 3. Rich experience in export operation. 4. Rich experience in

[N-(9-FLUORENYLMETHOXYCARBONYL)-N-DECYLAMINO]ETHANAL

Cas:239088-22-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wising Chem Co., Ltd

Henan Wising Chem specialize in sourcing the chemicals in China. We are associated with many trusted manufacturers each having different area of expertise required for meeting the needs of our local as well as overseas buyers . We have access to cu

N-BUTYL (S)-2-HYDROXYBUTYRATE supplier

Cas:239088-22-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Other

inquiry

Wuhan MoonZY Biological Technology Co.,Ltd

instock with good quality and wholesale price Storage:Keep in a cool & dry place Package:Packing material and QTY as your request Application:Pharma;Industry;other application Transportation:Express or as your request Port:Any port of China

(9H-Fluoren-9-yl)methyl decyl(2-oxoethyl)carbamate,239088-22-3

Cas:239088-22-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

C41H49N3O2

C41H49N3O2

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran at 15 - 20℃; for 0.5h;95%
N-(9-fluorenylmethoxycarbonyl)-N-n-decylaminoethanol
239088-19-8

N-(9-fluorenylmethoxycarbonyl)-N-n-decylaminoethanol

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
With sodium hypochlorite solution; 2,2,6,6-tetramethylpiperidin-1-ol; sodium hydrogencarbonate; potassium bromide In dichloromethane; water at -5℃; pH=8.5;92.4%
Stage #1: N-(9-fluorenylmethoxycarbonyl)-N-n-decylaminoethanol With N-ethyl-N,N-diisopropylamine In dichloromethane at -5℃; for 0.25h;
Stage #2: With sulfur trioxide pyridine complex; dimethyl sulfoxide In dichloromethane at -5℃; for 0.5h;
90%
Stage #1: N-(9-fluorenylmethoxycarbonyl)-N-n-decylaminoethanol With N-ethyl-N,N-diisopropylamine In dichloromethane at -5℃; for 0.0833333h;
Stage #2: With pyridine; sulfur trioxide In dichloromethane; dimethyl sulfoxide at -5℃; for 0.5h;
C29H41NO4
1260529-12-1

C29H41NO4

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
With hydrogenchloride In dichloromethane at -10 - 30℃;82.2%
With formic acid at 20℃; for 4h;
Multi-step reaction with 2 steps
1.1: formic acid / toluene / 4 h / 20 °C
1.2: 1 h
2.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
N-FMOC-N-allyldecylamine

N-FMOC-N-allyldecylamine

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Stage #1: N-FMOC-N-allyldecylamine With ozone In methanol; dichloromethane; oxygen at -65 - -55℃; for 2.5h;
Stage #2: With triethylamine In methanol; dichloromethane at -55 - 21℃; for 3h;
Stage #3: With hydrogenchloride; water In methanol; dichloromethane
61%
oxalyl dichloride
79-37-8

oxalyl dichloride

N-(9-fluorenylmethoxycarbonyl)-N-n-decylaminoethanol
239088-19-8

N-(9-fluorenylmethoxycarbonyl)-N-n-decylaminoethanol

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
With sulfuric acid; triethylamine In n-heptane; dichloromethane; water; dimethyl sulfoxide
With sulfuric acid; triethylamine In n-heptane; dichloromethane; water; dimethyl sulfoxide
caprinaldehyde
112-31-2

caprinaldehyde

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: butan-1-ol / 60 °C
2.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
3.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
3.2: 0.92 h / 0 - 5 °C
4.1: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 5 steps
1.1: butan-1-ol / 60 °C
2.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
3.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
3.2: 0.92 h / 0 - 5 °C
4.1: formic acid / toluene / 4 h / 20 °C
4.2: 1 h
5.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
Multi-step reaction with 5 steps
1: butan-1-ol / 60 °C
2: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
3: toluene / 40 - 50 °C
4: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
5: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 6 steps
1.1: butan-1-ol / 60 °C
2.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
3.1: toluene / 40 - 50 °C
4.1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
5.1: formic acid / toluene / 4 h / 20 °C
5.2: 1 h
6.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
Multi-step reaction with 3 steps
1: 5%-palladium/activated carbon; hydrogen / methanol / 20 - 100 °C / 3750.38 Torr
2: N-ethyl-N,N-diisopropylamine / dichloromethane / -20 - 30 °C
3: hydrogenchloride / dichloromethane / -10 - 30 °C
View Scheme
1-aminodecane
2016-57-1

1-aminodecane

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: butan-1-ol; water / 60 °C
2.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C
3.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
3.2: 0.92 h / 0 - 5 °C
4.1: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 3.5 h / 50 °C / 3750.38 Torr
2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
2.2: 0.92 h / 0 - 5 °C
3.1: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: hydrogen / 5% Pd(II)/C(eggshell) / methanol / 3.5 h / 50 °C / 3750.38 Torr
2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
2.2: 0.92 h / 0 - 5 °C
3.1: formic acid / toluene / 4 h / 20 °C
3.2: 1 h
4.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
C7H8O3S*C14H31NO2
1260529-14-3

C7H8O3S*C14H31NO2

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
2: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
2.1: formic acid / toluene / 4 h / 20 °C
2.2: 1 h
3.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
C14H29NO2

C14H29NO2

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
2.2: 0.92 h / 0 - 5 °C
3.1: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
2.2: 0.92 h / 0 - 5 °C
3.1: formic acid / toluene / 4 h / 20 °C
3.2: 1 h
4.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
Multi-step reaction with 4 steps
1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
2: toluene / 40 - 50 °C
3: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
4: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 5 steps
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr
2.1: toluene / 40 - 50 °C
3.1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
4.1: formic acid / toluene / 4 h / 20 °C
4.2: 1 h
5.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
decylaminoethanal dimethylacetal
72816-68-3

decylaminoethanal dimethylacetal

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
1.2: 0.92 h / 0 - 5 °C
2.1: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
1.2: 0.92 h / 0 - 5 °C
2.1: formic acid / toluene / 4 h / 20 °C
2.2: 1 h
3.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
Multi-step reaction with 3 steps
1: toluene / 40 - 50 °C
2: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
3: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: toluene / 40 - 50 °C
2.1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
3.1: formic acid / toluene / 4 h / 20 °C
3.2: 1 h
4.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
decylimminoethanolacetal
1260529-09-6

decylimminoethanolacetal

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C
2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
2.2: 0.92 h / 0 - 5 °C
3.1: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C
2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C
2.2: 0.92 h / 0 - 5 °C
3.1: formic acid / toluene / 4 h / 20 °C
3.2: 1 h
4.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
Multi-step reaction with 4 steps
1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C
2: toluene / 40 - 50 °C
3: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
4: formic acid / 4 h / 20 °C
View Scheme
Multi-step reaction with 5 steps
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C
2.1: toluene / 40 - 50 °C
3.1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C
4.1: formic acid / toluene / 4 h / 20 °C
4.2: 1 h
5.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.5 h / 15 - 20 °C
View Scheme
1-Decanol
112-30-1

1-Decanol

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate / dichloromethane / -10 - 50 °C
2: 5%-palladium/activated carbon; hydrogen / methanol / 20 - 100 °C / 3750.38 Torr
3: N-ethyl-N,N-diisopropylamine / dichloromethane / -20 - 30 °C
4: hydrogenchloride / dichloromethane / -10 - 30 °C
View Scheme
Multi-step reaction with 4 steps
1.1: pyridine / dichloromethane / 24 h / 20 °C
2.1: ethanol / 5 h / 90 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / -5 °C
4.2: 0.5 h / -5 °C
View Scheme
Multi-step reaction with 4 steps
1.1: dichloromethane / 0.08 h / 0 °C
1.2: 24 h / 20 - 25 °C
2.1: ethanol / 24 h / 90 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / -5 °C
4.2: 0.5 h / -5 °C
View Scheme
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 12 h / 0 - 20 °C
2: ethanol / 12 h / 90 °C
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C
4: sodium hydrogencarbonate; potassium bromide; 2,2,6,6-tetramethylpiperidin-1-ol; sodium hypochlorite solution / dichloromethane; water / -5 °C / pH 8.5
View Scheme
methanesulfonic acid decyl ester
41233-29-8

methanesulfonic acid decyl ester

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: ethanol / 5 h / 90 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / -5 °C
3.2: 0.5 h / -5 °C
View Scheme
Multi-step reaction with 3 steps
1.1: ethanol / 24 h / 90 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / -5 °C
3.2: 0.5 h / -5 °C
View Scheme
Multi-step reaction with 3 steps
1: ethanol / 12 h / 90 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C
3: sodium hydrogencarbonate; potassium bromide; 2,2,6,6-tetramethylpiperidin-1-ol; sodium hypochlorite solution / dichloromethane; water / -5 °C / pH 8.5
View Scheme
(fluorenylmethoxy)carbonyl chloride
28920-43-6

(fluorenylmethoxy)carbonyl chloride

2-(n-Decylamino)ethanol
15196-28-8

2-(n-Decylamino)ethanol

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.08 h / -5 °C
2.2: 0.5 h / -5 °C
View Scheme
N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

vancomycin hydrochloride

vancomycin hydrochloride

Nvan-2-(n-decylamino)ethyl vancomycin hydrochloride

Nvan-2-(n-decylamino)ethyl vancomycin hydrochloride

Conditions
ConditionsYield
Stage #1: N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester; vancomycin hydrochloride With N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 20℃; for 15h;
Stage #2: With methanol; trifluoroacetic acid In DMF (N,N-dimethyl-formamide) at 0℃; for 1h;
Stage #3: With hydrogenchloride; borane pyridine; water; methylamine more than 3 stages;
N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

LY264826

LY264826

C100H121Cl2N11O28

C100H121Cl2N11O28

Conditions
ConditionsYield
In methanol; N,N-dimethyl-formamide at 65℃; for 2h;
N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

vancomycin hydrochloride
1404-93-9

vancomycin hydrochloride

C93H108Cl2N10O26

C93H108Cl2N10O26

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 55℃; for 4h;
Stage #1: vancomycin hydrochloride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 55 - 60℃;
Stage #2: N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester In N,N-dimethyl-formamide at 25℃; for 18h;
Stage #3: With trifluoroacetic acid In methanol; N,N-dimethyl-formamide at 25℃; for 2h; Temperature; Reagent/catalyst;
N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

vancomycin hydrochloride
1404-93-9

vancomycin hydrochloride

N3-decylaminoethylvancomycin

N3-decylaminoethylvancomycin

Conditions
ConditionsYield
Stage #1: N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester; vancomycin hydrochloride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25 - 65℃; for 18h;
Stage #2: With sodium cyanoborohydride; trifluoroacetic acid In methanol; N,N-dimethyl-formamide at 20℃; for 3h;
Stage #3: With piperidine for 1h; Temperature; Reagent/catalyst;
N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

L-Lactic acid
79-33-4

L-Lactic acid

vancomycin hydrochloride
1404-93-9

vancomycin hydrochloride

C78H100Cl2N10O24*C3H6O3

C78H100Cl2N10O24*C3H6O3

Conditions
ConditionsYield
Stage #1: N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester; vancomycin hydrochloride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 55 - 60℃;
Stage #2: With trifluoroacetic acid In methanol; N,N-dimethyl-formamide at 2℃;
Stage #3: L-Lactic acid Further stages;
N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester
239088-22-3

N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester

vancomycin
1404-90-6

vancomycin

N-decyl-N-Fmoc-aminoethylvancomycin

N-decyl-N-Fmoc-aminoethylvancomycin

Conditions
ConditionsYield
Stage #1: N-decyl-N-(2-oxoethyl)carbamic acid 9H-fluoren-9-ylmethyl ester; vancomycin With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20 - 25℃; for 2h;
Stage #2: With sodium cyanoborohydride; trifluoroacetic acid In methanol; N,N-dimethyl-formamide at 20 - 25℃; for 1h;
700 mg

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