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inquiryBenzenemethanol,4-hydroxy-3-methoxy-a-methyl-Appearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceut
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inquiryConditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol for 3h; Ambient temperature; | 74% |
With iron(III) chloride; C6H13BN2 In dichloromethane at 20℃; | 65% |
With sodium hydroxide; sodium tetrahydroborate |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | 63% |
In diethyl ether; toluene at 20℃; Grignard reaction; | 54% |
In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; |
1-(4-hydroxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)ethanol
A
Apocynol
B
2-methoxy-phenol
C
1-(3-methoxy-4-hydroxyphenyl)ethanone
D
phenol
Conditions | Yield |
---|---|
With sodium hydroxide; nickel at 25℃; Product distribution; Further Variations:; Temperatures; other substrates, other current densities; Catalytic hydrogenation; Electrochemical reaction; | A 41% B 43% C 1.3% D 2% |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium tetrahydroborate Hydrieren des Reaktionsprodukts an Palladium/Kohle in Aethanol; |
Conditions | Yield |
---|---|
In diethyl ether for 1h; Heating; |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium cyanoborohydride In methanol for 18h; Product distribution; | A 95 % Spectr. B 5 % Spectr. |
Apocynol
Conditions | Yield |
---|---|
With potassium hydroxide; water |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: BF3 2: NaBH4; aqueous NaOH View Scheme |
1-(3-methoxy-4-hydroxyphenyl)ethanone
A
Apocynol
B
4-(1-aminoethyl)-2-methoxyphenol
Conditions | Yield |
---|---|
With ammonium formate In methanol at 70℃; for 4.5h; Inert atmosphere; | |
With ammonium formate In methanol at 70℃; for 4.5h; Inert atmosphere; |
3-methoxy-4-hydroxystyrene
A
Apocynol
B
1-(3-methoxy-4-hydroxyphenyl)ethanone
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical at 40℃; for 12h; pH=2; Kinetics; |
Conditions | Yield |
---|---|
Stage #1: methyl bromide With magnesium In diethyl ether for 1h; Inert atmosphere; Reflux; Stage #2: vanillin In tetrahydrofuran; diethyl ether at 0 - 20℃; for 2h; |
A
p-cresol
B
2-Methoxy-4-methylphenol
C
4-hydroxymethyl-2-methoxyphenol
D
Apocynol
E
Syringenin
F
vanillin
G
phenol
Conditions | Yield |
---|---|
Stage #1: lignin With titanium(IV) oxide In water for 5h; UV-irradiation; Stage #2: With hydrogen In methanol at 20℃; under 7498.84 Torr; for 24h; |
A
4-hydroxymethyl-2-methoxyphenol
B
coniferol
C
Apocynol
E
vanillin
F
2-methoxy-phenol
Conditions | Yield |
---|---|
Stage #1: lignin With titanium(IV) oxide In water for 5h; UV-irradiation; Stage #2: With hydrogen In methanol at 20℃; under 7498.84 Torr; for 24h; |
1-(3-methoxy-4-hydroxyphenyl)ethanone
A
3-methoxy-4-hydroxystyrene
B
4-Ethylguaiacol
C
Apocynol
Conditions | Yield |
---|---|
With hydrogen In 1,3,5-trimethyl-benzene at 120℃; under 37503.8 Torr; for 2h; Autoclave; |
Conditions | Yield |
---|---|
96% |
9,10-dihydro-9,10-dihydroxyanthracene
Apocynol
10-hydroxy-10-(4-hydroxy-3-methoxy-α-methylbenzyl)-9(10H)-anthracenone
Conditions | Yield |
---|---|
In water at 45℃; | 95% |
Conditions | Yield |
---|---|
95% | |
(i) HCl, CH2Cl2, (ii) Na2CO3, PE, (iii) /BRN= 1098229/; Multistep reaction; |
1,2,3-Benzotriazole
Apocynol
4-[1-(1H-1,2,3-benzotriazol-1-yl)ethyl]-2-methoxyphenol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 2h; Reflux; | 78% |
Apocynol
4-(1-bromoethyl)-2-methoxyphenol
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; sodium bromide In dichloromethane; N,N-dimethyl-formamide at 20℃; for 24h; chemoselective reaction; | 61% |
Conditions | Yield |
---|---|
With 1-hexyl-3-methyl-1-imidazolium bromide at 140℃; for 0.133333h; Microwave irradiation; Combinatorial reaction / High throughput screening (HTS); chemoselective reaction; | 56% |
With silica gel In 1,4-dioxane for 0.2h; microwave irradiation; | 43% |
para-diiodobenzene
Apocynol
4,4'-((1E,1'E)-(1,4-phenylene)bis(ethene-2,1-diyl))bis(2-methoxyphenol)
Conditions | Yield |
---|---|
With piperidine; sodium formate; 1-hexyl-3-methyl-1-imidazolium bromide; lithium chloride; bis(dibenzylideneacetone)-palladium(0); tricyclohexylphosphine at 150℃; for 0.666667h; Heck Reaction; Microwave irradiation; stereoselective reaction; | 42% |
Apocynol
dehydrodiapocynol
Conditions | Yield |
---|---|
With horseradish peroxidase (EC 1.11.1.7); dihydrogen peroxide; citric acid In phosphate buffer; acetone for 0.5h; pH=3.5; Dimerization; | 34% |
Conditions | Yield |
---|---|
With cerium(III) chloride In tetrahydrofuran | 28% |
Conditions | Yield |
---|---|
With cerium(III) chloride In tetrahydrofuran | 27% |
Apocynol
A
2-methoxy-1,4-benzoquinone
B
vanillin
C
1-(3-methoxy-4-hydroxyphenyl)ethanone
Conditions | Yield |
---|---|
With dihydrogen peroxide In water; acetonitrile for 0.5h; Microwave irradiation; | A 23% B 5% C 18% |
Apocynol
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water for 1h; Heating; | 20.5% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In water; acetonitrile for 0.5h; Reagent/catalyst; Microwave irradiation; | 18% |
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene for 4h; | |
With sodium phosphate buffer; DH-I and DH-II of Pseudomonas sp. TMY 1009; NAD; acetaldehyde; yeast alcohol dehydrogenase In water |
1,4-dibromo-2,5-dimethoxybenzene
Apocynol
(E,E)-1,4-dimethoxy-2,5-bis((4-hydroxy-3-methoxy)styryl)benzene
Conditions | Yield |
---|---|
With piperidine; sodium formate; 1-hexyl-3-methyl-1-imidazolium bromide; lithium chloride; bis(dibenzylideneacetone)-palladium(0); tricyclohexylphosphine at 150℃; for 0.666667h; Heck Reaction; Microwave irradiation; stereoselective reaction; | 14% |
Apocynol
A
2-methoxy-1,4-benzoquinone
B
1-(3-methoxy-4-hydroxyphenyl)ethanone
Conditions | Yield |
---|---|
With dihydrogen peroxide In water; acetonitrile for 0.5h; Microwave irradiation; | A 11% B 10% |
With dihydrogen peroxide In water; acetonitrile at 39.84℃; for 0.25h; Reagent/catalyst; | A 43 %Chromat. B 52 %Chromat. |
With dihydrogen peroxide In water; acetonitrile at 39.84℃; for 0.25h; Reagent/catalyst; Time; | A 65 %Chromat. B 19 %Chromat. |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
Apocynol
4-Ethyliden-2-methoxy-2,5-cyclohexadienon
Conditions | Yield |
---|---|
(i) HCl, CH2Cl2, (ii) Et3N; Multistep reaction; | |
(i) HCl, CH2Cl2, (ii) Na2CO3, PE; Multistep reaction; |
Apocynol
sodium benzenesulfonate
<1-(4-Hydroxy-3-methoxy-phenyl)-aethyl>-phenyl-sulfon
Conditions | Yield |
---|---|
In acetic acid | |
With acetic acid |
Conditions | Yield |
---|---|
With potassium hydroxide; potassium borohydride | |
Multi-step reaction with 2 steps 1: acetic acid 2: KBH4, aq. KOH View Scheme |
Apocynol
C18H22O4
Conditions | Yield |
---|---|
With potassium hydroxide; potassium borohydride | |
Multi-step reaction with 2 steps 1: acetic acid 2: KBH4, aq. KOH View Scheme |
Apocynol
1-(4-hydroxy-3-methoxybenzyl)-1'-(4-ethyl-3-methoxy-2-phenyl)ethane
Conditions | Yield |
---|---|
With potassium hydroxide; potassium borohydride | |
Multi-step reaction with 2 steps 1: acetic acid 2: KBH4, aq. KOH View Scheme |
Apocynol
Conditions | Yield |
---|---|
With potassium hydroxide; potassium borohydride |
Apocynol
4-Hydroxy-3-methoxy-1-(1-chlor-ethyl)-benzol
Conditions | Yield |
---|---|
With hydrogenchloride In dichloromethane |
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