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inquiryProduct Name: 1-butyl-3-methylimidazole bisulfate synonyms:1-butyl-3-methylimidazoliumhydrogensulfate;3-butyl-1-methyl-1H-imidazol-3-ium hydrogensulfate;[BMIm][HSO4];BASIONIC AC 28; 1-Butyl-3-methylimidazolium hydrogensulfate;Basionics(R) AC 28
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inquiry1-methyl-3-(n-butyl)imidazolium iodide
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
With Amberlyst A-26 (HSO4- form) In methanol | 100% |
With Amberlist A-26 HSO4(-) form In methanol Ionic liquid; |
1-butyl-3-methylimidazolium chloride
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
With sulfuric acid In dichloromethane for 48h; Reflux; Cooling with ice; | 99.4% |
With sodium hydrogen sulfate In acetonitrile at 25℃; for 96h; Inert atmosphere; | 97% |
With sulfuric acid In dichloromethane for 24h; Reflux; | 95% |
1-butyl-3-methylimidazolium methylsulfate
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
With water for 24h; Reagent/catalyst; Reflux; | 99% |
With water at 149.84℃; for 18h; Autoclave; High pressure; | |
With sulfuric acid; water at 165℃; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
In water at 170 - 215℃; for 4h; Inert atmosphere; | 98% |
1-n-butyl-3-methylimidazolim bromide
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
With 1-hexene; sulfuric acid; dihydrogen peroxide at 25℃; for 3h; | 97% |
With sulfuric acid; silver sulfate In ethanol at 50℃; for 2h; | 75% |
With sulfuric acid; silver sulfate In ethanol; water at 50℃; for 2h; | 75% |
1-methyl-1H-imidazole
n-Butyl chloride
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
Stage #1: 1-methyl-1H-imidazole; n-Butyl chloride In toluene for 48h; Reflux; Stage #2: With potassium hydrogensulfate In toluene | 94% |
Stage #1: 1-methyl-1H-imidazole; n-Butyl chloride In dichloromethane at 49.84 - 59.84℃; Stage #2: With potassium hydrogensulfate In dichloromethane at 69.84℃; |
1-Butylimidazole
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene / 4 h / 20 °C / Inert atmosphere; Cooling with ice 2: water / 18 h / 149.84 °C / Autoclave; High pressure View Scheme |
sulfuric acid
sodium sulfate
1-butyl-3-methylimidazolium chloride
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
Ionic liquid; Inert atmosphere; |
1-methyl-1H-imidazole
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
Stage #1: 1-methyl-1H-imidazole at 69.84℃; for 12h; Stage #2: With sulfuric acid In acetonitrile at 69.84℃; |
1-methyl-1H-imidazole
1-bromo-butane
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
Stage #1: 1-methyl-1H-imidazole; 1-bromo-butane for 48h; Stage #2: With sulfuric acid In ethyl acetate at 70℃; for 48h; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
With sulfuric acid In water |
Conditions | Yield |
---|---|
at 83℃; for 8h; Ionic liquid; | 83.5% |
1-butyl-3-methylimidazolium hydrogen sulfate
1-butyl-3-methylimidazolium propioanate
Conditions | Yield |
---|---|
With barium dihydroxide; acetic acid In water at 20 - 76℃; for 14.5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
sulfur trioxide
Conditions | Yield |
---|---|
at 60℃; for 96h; Schlenk technique; |
1-butyl-3-methylimidazolium hydrogen sulfate
1-butyl-3-methylimidazolium peroxymonosulphate
Conditions | Yield |
---|---|
With Oxone; oxone In acetone for 2h; Sonication; Inert atmosphere; |
1-butyl-3-methylimidazolium hydrogen sulfate
sulfur trioxide pyridine complex
Conditions | Yield |
---|---|
With germaniumtetrachloride at 50℃; for 24h; Sealed tube; |
1-butyl-3-methylimidazolium hydrogen sulfate
pyridine
sulfur trioxide pyridine complex
Conditions | Yield |
---|---|
With europium(III) oxide at 25 - 60℃; for 168h; Sealed tube; |
1-butyl-3-methylimidazolium hydrogen sulfate
zinc(II) chloride
Conditions | Yield |
---|---|
at 26.84℃; for 5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
at 26.84℃; for 5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
at 26.84℃; for 5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
at 26.84℃; for 5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
at 26.84℃; for 5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
cobalt(II) chloride
Conditions | Yield |
---|---|
at 26.84℃; for 5h; |
1-butyl-3-methylimidazolium hydrogen sulfate
Conditions | Yield |
---|---|
With strontium(II) hydroxide octahydrate; water Large scale; |
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