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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Ethyl 2-amino-5-iodobenzoate Manufacturer/High quality/Best price/In stock

Cas:268568-11-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Benzoic acid, 2-amino-5-iodo-, ethyl ester

Cas:268568-11-2

Min.Order:1

Negotiable

Type:Other

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Factory Supply Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 268568-11-2 with best quality

Cas:268568-11-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Ethyl 2-amino-5-iodobenzoate 268568-11-2

Cas:268568-11-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

Ethyl 2-amino-5-iodobenzoate CAS:268568-11-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org

Ethyl 2-amino-5-iodobenzoate CAS:268568-11-2

Cas:268568-11-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:1 Kilogram

FOB Price: $40.0 / 60.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:Used as Pharmaceutical Intermediates Transp

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Ethyl 2-amino-5-iodobenzoate, 98+%; Ethyl 5-iodoanthranilate; Ethyl 2-amino-5-iodobenzoate; 2-Amino-5-iodobenzoic acid ethyl ester; Ethyl 5-iodoanthranilate, 2-(Ethoxycarbonyl)-4 -iodoaniline;2-amino-5-iodobenzoate CAS No.: 268568-11-2 Molecula

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: Ethyl 2-amino-5-iodobenzoate Synonyms: Ethyl 2-amino-5-iodobenzoate, 98+%;Ethyl 5-iodoanthranilate;Ethyl 2-amino-5-iodobenzoate;2-Amino-5-iodobenzoic acid ethyl ester;Ethyl 5-iodoanthranilate, 2-(Ethoxycarbonyl)-4-iodoaniline;2-am

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

SAGECHEM LIMITED

SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in

SAGECHEM/ Ethyl 2-amino-5-iodobenzoate /Manufacturer in China

Cas:268568-11-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis:

Benzoic acid,2-amino-5-iodo-, ethyl ester

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

Benzoic acid,2-amino-5-iodo-, ethyl ester

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

Ethyl 2-aMino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD

Our price is the lowest in China. We are the manufacturer of this product in China. Our price is the lowest in China. CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD., founded in 1984, engages in pharmaceutical research, development, prod

Ethyl 2-amino-5-iodobenzoate 268568-11-2;912575-12-3 low price manufacturer

Cas:268568-11-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ethyl 2-amino-5-iodobenzoateAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemic

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:Powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary and sec

Ethyl 2-amino-5-iodobenzoate

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

Ethyl 2-amino-5-iodobenzoate cas 268568-11-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Ethyl 2-amino-5-iodobenzoate cas 268568-11-2

Cas:268568-11-2

Min.Order:0

Negotiable

Type:Other

inquiry

Synthetic route

2-ethoxycarbonylaniline
87-25-2

2-ethoxycarbonylaniline

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

Conditions
ConditionsYield
With iodine; silver sulfate In ethanol at 20℃; for 1h;90%
ethanol
64-17-5

ethanol

2-amino-5-iodobenzoic acid
5326-47-6

2-amino-5-iodobenzoic acid

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

Conditions
ConditionsYield
With hydrogenchloride for 7h; Esterification; Heating;
With thionyl chloride for 18h; Reflux; Inert atmosphere; Cooling with ice;
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

2-amino-5-trimethylsilanylethynyl-benzoic acid ethyl ester
870621-97-9

2-amino-5-trimethylsilanylethynyl-benzoic acid ethyl ester

Conditions
ConditionsYield
With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) In triethylamine at 50℃; for 4h;90%
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

diisopropyl-carbodiimide
693-13-0

diisopropyl-carbodiimide

6-iodo-3-isopropyl-2-(isopropylamino)quinazolin-4(3H)-one

6-iodo-3-isopropyl-2-(isopropylamino)quinazolin-4(3H)-one

Conditions
ConditionsYield
With tris(bis(trimethylsilyl)amido)lanthanum(III) In neat (no solvent) at 100℃; for 24h; Schlenk technique; Inert atmosphere;86%
thiophene-2-carbonitrile
1003-31-2

thiophene-2-carbonitrile

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 2-amino-5-(5-cyanothiophen-2-yl)benzoate
1397709-67-9

ethyl 2-amino-5-(5-cyanothiophen-2-yl)benzoate

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 20h; Inert atmosphere;77%
tributyl-amine
102-82-9

tributyl-amine

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 2-amino-5-butyrylbenzoate
1290542-74-3

ethyl 2-amino-5-butyrylbenzoate

Conditions
ConditionsYield
With dichloro bis(acetonitrile) palladium(II); tetrabutylammomium bromide; water; zinc(II) oxide In dimethyl sulfoxide at 100℃; for 36h;76%
2-isobutylthiazole
18640-74-9

2-isobutylthiazole

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 2-amino-5-(2-isobutylthiazol-5-yl)-benzoate
1397709-71-5

ethyl 2-amino-5-(2-isobutylthiazol-5-yl)-benzoate

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 20h; Inert atmosphere;73%
ethyl 2-methylthiazole-4-carboxylate
6436-59-5

ethyl 2-methylthiazole-4-carboxylate

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 5-(4-amino-3-ethoxycarbonylphenyl)-2-methylthiazole-
1397709-72-6

ethyl 5-(4-amino-3-ethoxycarbonylphenyl)-2-methylthiazole-

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 20h; Inert atmosphere;72%
N-Methylpyrrole
96-54-8

N-Methylpyrrole

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 2-amino-5-(1-methylpyrrol-2-yl)benzoate
1397709-70-4

ethyl 2-amino-5-(1-methylpyrrol-2-yl)benzoate

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 20h; Inert atmosphere;64%
1-(4-chlorothiophen-2-yl)ethan-1-one
34730-20-6

1-(4-chlorothiophen-2-yl)ethan-1-one

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 5-(5-acetyl-3-chlorothiophen-2-yl)-2-aminobenzoate
1397709-68-0

ethyl 5-(5-acetyl-3-chlorothiophen-2-yl)-2-aminobenzoate

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 20h; Inert atmosphere;61%
methyl 2-methyl-3-furancarboxylate
6141-58-8

methyl 2-methyl-3-furancarboxylate

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

methyl 5-(4-amino-3-ethoxycarbonylphenyl)-2-methylfuran-3-carboxylate
1397709-69-1

methyl 5-(4-amino-3-ethoxycarbonylphenyl)-2-methylfuran-3-carboxylate

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 150℃; for 20h; Inert atmosphere;60%
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

3-amino-4-methyl-2-thiophenecarboxylic acid methyl ester
85006-31-1

3-amino-4-methyl-2-thiophenecarboxylic acid methyl ester

3-amino-5-(4-amino-3-ethoxycarbonyl-phenyl)-4-methylthiophene-2-carboxylic acid methyl ester
1393718-89-2

3-amino-5-(4-amino-3-ethoxycarbonyl-phenyl)-4-methylthiophene-2-carboxylic acid methyl ester

Conditions
ConditionsYield
With PdCl(C3H5)(dppb); potassium acetate In N,N-dimethyl acetamide at 120℃; for 20h; Inert atmosphere;42%
ethyl 3-(chloroformyl)propionate
14794-31-1

ethyl 3-(chloroformyl)propionate

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

2-(3-ethoxycarbonyl-propionylamino)-5-iodo-benzoic acid ethyl ester
268568-12-3

2-(3-ethoxycarbonyl-propionylamino)-5-iodo-benzoic acid ethyl ester

Conditions
ConditionsYield
With pyridine In toluene for 2h; Acylation; Heating;
pyrrolidine
123-75-1

pyrrolidine

ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

1-(2-carbethoxy-4-iodophenylazo)pyrrolidine

1-(2-carbethoxy-4-iodophenylazo)pyrrolidine

Conditions
ConditionsYield
Stage #1: ethyl 2-amino-5-iodobenzoate With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h;
Stage #2: pyrrolidine With potassium carbonate In water; acetonitrile at 0 - 20℃; Further stages.;
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

C14H17N3O3

C14H17N3O3

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: conc. HCl; sodium nitrite / H2O / 0.5 h / 0 °C
1.2: potassium carbonate / H2O; acetonitrile / 0 - 20 °C
2.1: i-PrMgCl*LiCl / tetrahydrofuran / 1 h / -40 °C
2.2: 85 percent / tetrahydrofuran / -40 - 20 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

ethyl 2-azido-5-formyl-benzoate

ethyl 2-azido-5-formyl-benzoate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: conc. HCl; sodium nitrite / H2O / 0.5 h / 0 °C
1.2: potassium carbonate / H2O; acetonitrile / 0 - 20 °C
2.1: i-PrMgCl*LiCl / tetrahydrofuran / 1 h / -40 °C
2.2: 85 percent / tetrahydrofuran / -40 - 20 °C
3.1: 94 percent / sodium azide; boron trifluoride diethyl etherate; trifluoroacetic acid / CH2Cl2 / 20 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

C42H48N2O8

C42H48N2O8

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 90 percent / CuI / Pd(PPh3)4 / triethylamine / 4 h / 50 °C
2: 86 percent / triethylamine / CHCl3 / 2 h / Heating
3: 96 percent / K2CO3 / CH2Cl2; methanol / 3 h / 20 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

C48H64N2O8Si2
870621-98-0

C48H64N2O8Si2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 percent / CuI / Pd(PPh3)4 / triethylamine / 4 h / 50 °C
2: 86 percent / triethylamine / CHCl3 / 2 h / Heating
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

7-iodo-3,4-dihydro-1H-1-benzazepine-2,5-dione
252894-39-6

7-iodo-3,4-dihydro-1H-1-benzazepine-2,5-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine / toluene / 2 h / Heating
2: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3: aq. DMSO / 3 h / 150 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

5-hydroxy-7-iodo-2-oxo-2,3-dihydro-1H-benzo[b]azepine-4-carboxylic acid ethyl ester
268568-13-4

5-hydroxy-7-iodo-2-oxo-2,3-dihydro-1H-benzo[b]azepine-4-carboxylic acid ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / toluene / 2 h / Heating
2: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

2-iodo,9-trifluoromethyl-7,12-dihydro-indolo[3,2-d][1]benzazepin-6(5H)-one
252894-28-3

2-iodo,9-trifluoromethyl-7,12-dihydro-indolo[3,2-d][1]benzazepin-6(5H)-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

3-(6-oxo-9-trifluoromethyl-5,6,7,12-tetrahydro-indolo[3,2-d][1]benzazepin-2-yl)-acrylonitrile
309967-45-1

3-(6-oxo-9-trifluoromethyl-5,6,7,12-tetrahydro-indolo[3,2-d][1]benzazepin-2-yl)-acrylonitrile

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
5.1: Pd(OAc)2; P(C6H5)3; TEA / dimethylformamide / Heating
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

3-(6-oxo-9-trifluoromethyl-5,6,7,12-tetrahydro-benzo[2,3]azepino[4,5-b]indol-2-yl)-acrylic acid methyl ester

3-(6-oxo-9-trifluoromethyl-5,6,7,12-tetrahydro-benzo[2,3]azepino[4,5-b]indol-2-yl)-acrylic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
5.1: Pd(OAc)2; P(C6H5)3; TEA / dimethylformamide / Heating
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

2-(3-hydroxy-prop-1-ynyl)-9-trifluoromethyl-5,12-dihydro-7H-benzo[2,3]azepino[4,5-b]indol-6-one

2-(3-hydroxy-prop-1-ynyl)-9-trifluoromethyl-5,12-dihydro-7H-benzo[2,3]azepino[4,5-b]indol-6-one

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
5.1: PdCl2[P(C6H5)3]2; CuI; TEA / 50 °C
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

2-(3-oxo-1-butenyl)-9-trifluoromethyl-7,12-dihydro-indolo[3, 2-d][1]benzazepin-6(5H)-one

2-(3-oxo-1-butenyl)-9-trifluoromethyl-7,12-dihydro-indolo[3, 2-d][1]benzazepin-6(5H)-one

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
5.1: Pd(OAc)2; P(C6H5)3; TEA / dimethylformamide / Heating
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

3-(6-oxo-9-trifluoromethyl-5,6,7,12-tetrahydro-indolo[3,2-d][1]benzazepin-2-yl)-propionitrile

3-(6-oxo-9-trifluoromethyl-5,6,7,12-tetrahydro-indolo[3,2-d][1]benzazepin-2-yl)-propionitrile

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
5.1: Pd(OAc)2; P(C6H5)3; TEA / dimethylformamide / Heating
6.1: Mg; MeOH / 1 h / Heating
View Scheme
ethyl 2-amino-5-iodobenzoate
268568-11-2

ethyl 2-amino-5-iodobenzoate

98 N 349

98 N 349

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine / toluene / 2 h / Heating
2.1: KH / dimethylformamide; toluene / 3 h / 0 - 80 °C
3.1: aq. DMSO / 3 h / 150 °C
4.1: AcOH / 1 h / 70 °C
4.2: H2SO4; AcOH / 1 h / 70 °C
5.1: PdCl2[P(C6H5)3]2; CuI; TEA / 50 °C
View Scheme

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