Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:27650-86-8
Min.Order:1 Kilogram
FOB Price: $20.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:27650-86-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
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Cas:27650-86-8
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:27650-86-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
Cas:27650-86-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
3-(Naphth-1-yl)propan-1-ol
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
With carbon tetrabromide; TOP Ambient temperature; | 95% |
With phosphorus tribromide In dichloromethane at 0 - 20℃; | 81% |
With sulfuric acid; hydrogen bromide; acetic acid |
1-(3-bromo-n-propyl)-1,2,3,4-tetrahydronaphthalene
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 4h; Heating; | 70% |
sodium diethylmalonate
1-Chloromethylnaphthalene
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multistep reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: BuLi; N,N,N',N'-tetramethylethylendiamine (TMEDA) / diethyl ether 2: TsOH (p-toluenesulphonic acid) / methanol 3: Ph3PBr2 View Scheme |
2-(3-naphthalen-1-yl-propoxy)-tetrahydro-pyran
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: TsOH (p-toluenesulphonic acid) / methanol 2: Ph3PBr2 View Scheme |
1-Naphthalenepropanoic acid
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 97 percent / LiAlH4 / tetrahydrofuran 2: 95 percent / CBr4, tri-n-octylphosphine / Ambient temperature View Scheme |
1-(2-bromo)ethylnaphthalene
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 72 percent / ethanol; H2O / 21 h / Heating 2: 94 percent / 40percent aq. H2SO4 / 20 h / Heating 3: 97 percent / LiAlH4 / tetrahydrofuran 4: 95 percent / CBr4, tri-n-octylphosphine / Ambient temperature View Scheme |
3-(naphthalen-1-yl)propanenitrile
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 94 percent / 40percent aq. H2SO4 / 20 h / Heating 2: 97 percent / LiAlH4 / tetrahydrofuran 3: 95 percent / CBr4, tri-n-octylphosphine / Ambient temperature View Scheme |
3-(naphthalen-1-yl)propionic acid methyl ester
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4; diethyl ether 2: red phosphorus; H2SO4; aqueous HBr View Scheme |
1-naphthylmagnesiumbromide
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether; benzene 2: H2SO4; acetic acid; aqueous HBr View Scheme |
diethyl (1-naphthylmethyl)malonate
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ethanol; water; sodium hydroxide / Reflux 1.2: pH Ca. 1 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 3.1: phosphorus tribromide / dichloromethane / 0 - 20 °C View Scheme |
1-Chloromethylnaphthalene
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium ethanolate / ethanol / Inert atmosphere 1.2: 24 h / 20 °C / Inert atmosphere 2.1: ethanol; water; sodium hydroxide / Reflux 2.2: pH Ca. 1 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 4.1: phosphorus tribromide / dichloromethane / 0 - 20 °C View Scheme |
Conditions | Yield |
---|---|
In dimethyl sulfoxide | 100% |
1-(3-bromopropyl)naphthalene
sodium cyanide
4-(1-naphthalenyl)butanenitrile
Conditions | Yield |
---|---|
In ethanol; water for 5h; Heating; | 84% |
1-(3-bromopropyl)naphthalene
4-hydroxy-1-[2-(4-morpholinyl)ethyl]-1H-indole
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 105℃; for 1.5h; | 44% |
10-dimethylamino-3,7-dimethyl-deca-2,6-dien-1-ol
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; Williamson reaction; | 35% |
(4S,5R)-5-[3,5-bis(trifluoromethyl)phenyl]-4-methyl-1,3-oxazolidin-2-one
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Stage #1: (4S,5R)-5-[3,5-bis(trifluoromethyl)phenyl]-4-methyl-1,3-oxazolidin-2-one With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Stage #2: 1-(3-bromopropyl)naphthalene In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 1.8% |
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
With water; sodium sulfite |
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane Heating; |
1-(3-bromopropyl)naphthalene
3-(1-naphthyl)propylmagnesium bromide
Conditions | Yield |
---|---|
With magnesium Grignard reaction; |
1-(3-bromopropyl)naphthalene
[3-(naphthalen-1-yl)propyl]phosphonous dichloride
Conditions | Yield |
---|---|
Stage #1: 1-(3-bromopropyl)naphthalene With magnesium In diethyl ether for 12h; Heating; Stage #2: With cadmium(II) chloride at 0℃; for 2h; Stage #3: With phosphorus trichloride In diethyl ether at 20℃; for 2.5h; | 34 % Spectr. |
cyclohexylpiperazine
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile Heating; |
1-(3-bromopropyl)naphthalene
N,N-diisopropyl-P-[3-(naphthalen-1-yl)propyl]phosphonamidous chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: Mg / diethyl ether / 12 h / Heating 1.2: CdCl2 / 2 h / 0 °C 1.3: 34 percent Spectr. / PCl3 / diethyl ether / 2.5 h / 20 °C 2.1: 70 percent Spectr. / CH2Cl2 / 2 h / 20 °C View Scheme |
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Mg / diethyl ether / 12 h / Heating 1.2: CdCl2 / 2 h / 0 °C 1.3: 34 percent Spectr. / PCl3 / diethyl ether / 2.5 h / 20 °C 2.1: 70 percent Spectr. / CH2Cl2 / 2 h / 20 °C 3.1: 31 percent / iPr2EtN / CH2Cl2 / 2 h / 20 °C View Scheme |
1-(3-bromopropyl)naphthalene
4-(naphthalen-1-yl)butanal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 84 percent / ethanol; H2O / 5 h / Heating 2: Dibal / diethyl ether; toluene / 1.) -78 deg C, 1 h, 2.) RT, 3 h View Scheme |
1-(3-bromopropyl)naphthalene
1-cyclopropyl-naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NBS, (PhCO)2O2 / CCl4 / Heating 2: Zn-Cu View Scheme |
phenylacetic acid
n-butyllithium
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane | 75%. |
{2,2-dimethyl-5-[2-(4-hydroxy-3-trifluoromethylphenyl)ethyl]-1,3-dioxan-5-yl}carbamic acid t-butyl ester
1-(3-bromopropyl)naphthalene
[2,2-dimethyl-5-(2-{4-[3-(1-naphthyl)propoxy]-3-trifluoromethylphenyl}ethyl)-1,3-dioxan-5-yl]carbamic acid t-butyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 1.5h; |
1-(3-bromopropyl)naphthalene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetonitrile / Reflux 2: hydrogenchloride; water / Reflux View Scheme |
1-(3-bromopropyl)naphthalene
1,5,9-triazatricyclo[7.3.1.05,13 ]tridecane
Conditions | Yield |
---|---|
In acetonitrile Reflux; |
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