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inquirymeso-Tetra (p-bromophenyl) porphine CAS:29162-73-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qual
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirymeso-Tetra (p-bromophenyl) porphine Basic information Product Name: meso-Tetra (p-bromophenyl) porphine Synonyms: meso -Tetra (4-bromophenyl) porphine;meso-Tetra (p-bromophenyl) porphine;21H,23H-Porphine, 5,10,15,20-tetrakis(4-bromophenyl)-;5,
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquirySAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryTAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryBest Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
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inquirybest seller Application:API
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inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
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inquiryWuhan Sun-shine Bio-technology Corporation Limited is specializing in the anticancer, antitumor,heart head blood-vessel,pharmaceutical intermediates,fine Chemicals production and customization..Company has strong ability of research and development
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inquiryCerametek Materials (CMT) is your industrial and R&D supplier: 1. Semiconductor materials: Compounds of II, III, IV, V, VI groups such as Metal Sulfides, Selenides, Tellurides, Arsenide, Antimonide, Phosphide... 2. Advanced ceramic and crys
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inquiryShanghai Sunway Corporation Ltd., a high-tech enterprise specializing in R&D, synthesis, and sales of MOF/COF Ligands, fine chemicals and pharmaceutical intermediates. We have established long-term and good business relationship with suppliers
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inquirypyrrole
4-bromo-benzaldehyde
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With propionic acid In dichloromethane for 0.333333h; Reagent/catalyst; Sealed tube; Microwave irradiation; Inert atmosphere; Schlenk technique; | 78% |
With acetic acid; propionic acid at 130℃; for 0.75h; | 64.4% |
Stage #1: pyrrole; 4-bromo-benzaldehyde With boron trifluoride diethyl etherate In chloroform for 1h; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In chloroform for 1h; Further stages.; | 58% |
pyrrole
4-bromo-benzaldehyde
B
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: 2-[(4-bromophenyl)hydroxymethyl]-5-[(2-allyloxy-5-bromophenyl)hydroxymethyl]thiophene; pyrrole; 4-bromo-benzaldehyde With boron trifluoride diethyl etherate In dichloromethane for 3h; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane | A 15% B n/a |
pyrrole
4-bromo-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: pyrrole; 4-bromo-benzaldehyde With methanesulfonic acid In dichloromethane for 0.5h; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane for 0.166667h; | A n/a B 13% |
pyrrole
4-bromo-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: 4-bromo-benzaldehyde With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: 2-(2-nitro-1-(1H-pyrrol-2-yl)ethyl)-5-(phenyl(1H-pyrrol-2-yl)methyl)-1H-pyrrole In dichloromethane at 20℃; for 0.166667h; Inert atmosphere; Stage #3: pyrrole Further stages; | A 9% B 13% |
pyrrole
4-bromo-benzaldehyde
B
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: 2-[(4-bromophenyl)hydroxymethyl]-5-[(2-methoxy-5-bromophenyl)hydroxymethyl]thiophene; pyrrole; 4-bromo-benzaldehyde With boron trifluoride diethyl etherate In dichloromethane Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane | A 9% B n/a |
pyrrole
4-bromo-benzaldehyde
B
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: 2-[(4-bromophenyl)hydroxymethyl]-5-[(2-methoxyphenyl)hydroxymethyl]thiophene; pyrrole; 4-bromo-benzaldehyde With boron trifluoride diethyl etherate In dichloromethane for 3h; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane | A 3% B n/a |
pyrrole
4-methoxy-benzaldehyde
4-bromo-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
B
(5Z,10Z,14Z,19Z)-5,10,15-Tris-(4-bromo-phenyl)-20-(4-methoxy-phenyl)-porphyrin
C
5,15-di(4-bromophenyl)-10,20-di(4-methoxyphenyl)porphyrin
D
5-(4-bromophenyl)-10,15,20-tri(4-methoxyphenyl)porphyrin
Conditions | Yield |
---|---|
In propionic acid for 2h; Heating; cooling overnight; Further byproducts given. Yields of byproduct given; | A n/a B 75 mg C n/a D 20 mg |
pyrrole
4-methoxy-benzaldehyde
4-bromo-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
B
5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin
C
(5Z,10Z,14Z,19Z)-5,10,15-Tris-(4-bromo-phenyl)-20-(4-methoxy-phenyl)-porphyrin
D
5-(4-bromophenyl)-10,15,20-tri(4-methoxyphenyl)porphyrin
Conditions | Yield |
---|---|
In propionic acid for 2h; Heating; cooling overnight; Further byproducts given; | A n/a B n/a C 75 mg D 20 mg |
pyrrole
4-methoxy-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
B
5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin
C
(5Z,10Z,14Z,19Z)-5,10,15-Tris-(4-bromo-phenyl)-20-(4-methoxy-phenyl)-porphyrin
D
5-(4-bromophenyl)-10,15,20-tri(4-methoxyphenyl)porphyrin
Conditions | Yield |
---|---|
With 4-bromo-benzaldehyde In propionic acid for 2h; Heating; cooling overnight; Yield given. Further byproducts given. Yields of byproduct given; | A n/a B n/a C 75 mg D 20 mg |
pyrrole
4-bromo-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
B
5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin
C
(5Z,10Z,14Z,19Z)-5,10,15-Tris-(4-bromo-phenyl)-20-(4-methoxy-phenyl)-porphyrin
D
5-(4-bromophenyl)-10,15,20-tri(4-methoxyphenyl)porphyrin
Conditions | Yield |
---|---|
With 4-methoxy-benzaldehyde In propionic acid for 2h; Heating; cooling overnight; Yield given. Further byproducts given. Yields of byproduct given; | A n/a B n/a C 75 mg D 20 mg |
tetrakis(4-aminophenyl)porphyrin
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With hydrogen bromide; sodium nitrite 1)5 deg C, 2)100 deg. C; Yield given. Multistep reaction; | |
Stage #1: tetrakis(4-aminophenyl)porphyrin With hydrogenchloride; sodium nitrite In water for 0.166667h; Cooling with ice; Stage #2: With potassium bromide In water at 20℃; for 2.83333h; Cooling with ice; |
pyrrole
4-bromo-benzaldehyde
B
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
C
5-(4-bromophenyl)-10,15,20-triphenylporphyrin
Conditions | Yield |
---|---|
With benzaldehyde; propionic acid for 0.5h; Heating; Further byproducts given. Title compound not separated from byproducts; |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In dichloromethane; toluene Oxidation; | |
With air In dichloromethane at 39℃; for 4h; | |
With air In dichloromethane at 39℃; |
5-(4-bromophenyl)dipyrromethane
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With chloranil; trifluoroacetic acid 1.) CH2Cl2, 1 h 2.) CH2Cl2, 1 h, reflux; Yield given; Multistep reaction. Yields of byproduct given; |
4-bromo-benzaldehyde
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CF3SO2Cl / CH2Cl2 / 1 h / 20 °C 2: air / CH2Cl2 / 3 h / 39 °C View Scheme | |
Multi-step reaction with 2 steps 1: SiO2/SOCl2 / CH2Cl2 / 2 h / 20 °C 2: air / CH2Cl2 / 39 °C View Scheme | |
Multi-step reaction with 2 steps 1: PCl5 / CH2Cl2 / 1 h / 20 °C 2: air / CH2Cl2 / 4 h / 39 °C View Scheme | |
Multi-step reaction with 2 steps 1: / dichloromethane / 2 h / 20 °C / Green chemistry 2: ammonium cerium (IV) nitrate / dichloromethane / 0.33 h / 20 °C / Green chemistry View Scheme | |
Multi-step reaction with 2 steps 1: iodine / dichloromethane / 20 °C / Inert atmosphere 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.08 h / Inert atmosphere View Scheme |
4-bromo-benzaldehyde
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: BF3*OEt2; NaCl / CH2Cl2 / 0.25 h / 25 °C 2: DDQ / CH2Cl2; toluene View Scheme |
B
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With manganese(IV) oxide In 1,4-dioxane at 90℃; for 0.05h; Microwave irradiation; Sealed vessel; |
pyrrole
5-nitro-2-thiophenecarboxaldehyde
4-bromo-benzaldehyde
A
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: pyrrole; 5-nitro-2-thiophenecarboxaldehyde; 4-bromo-benzaldehyde With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With chloranil In dichloromethane for 0.5h; Inert atmosphere; Stage #3: With triethylamine In dichloromethane Inert atmosphere; |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
nickel(II) 5,10,15,20-tetrakis-(4’-bromophenyl)porphyrin
Conditions | Yield |
---|---|
In toluene at 140℃; for 1h; | 100% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With zinc diacetate In methanol; chloroform for 4h; Reflux; | 97% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
diethylaluminium chloride
Conditions | Yield |
---|---|
Stage #1: 5,10,15,20-tetrakis(p-bromophenyl)porphyrin In dichloromethane for 0.0833333h; Inert atmosphere; Cooling with ice; Stage #2: diethylaluminium chloride In dichloromethane at 20℃; for 1h; Inert atmosphere; | 97% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
(5,10,15,20-tetrakis(4-bromophenyl)porphyrinato)zinc(II)
Conditions | Yield |
---|---|
With zinc diacetate In methanol; dichloromethane at 20℃; for 3h; | 96% |
With zinc(II) acetate dihydrate In N,N-dimethyl-formamide for 5h; Inert atmosphere; Reflux; | 85% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
zinc diacetate
(5,10,15,20-tetrakis(4-bromophenyl)porphyrinato)zinc(II)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 180℃; for 0.5h; Microwave irradiation; | 96% |
In chloroform; N,N-dimethyl-formamide for 0.133333h; Reflux; | 80% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
phosphonic acid diethyl ester
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); triethylamine In toluene at 80℃; for 24h; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); triethylamine In tetrahydrofuran; toluene Reflux; | 26% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
phenylboronic acid
5,10,15,20-tetrakis((1,1′-biphenyl)-4-yl)porphyrin
Conditions | Yield |
---|---|
With potassium carbonate In 5,5-dimethyl-1,3-cyclohexadiene at 100℃; for 24h; Reagent/catalyst; Suzuki-Miyaura Coupling; | 94% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
diethylaluminium chloride
Conditions | Yield |
---|---|
In hexane; dichloromethane at 25℃; for 1h; Inert atmosphere; | 93.5% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With nickel diacetate; acetic acid In chloroform at 120℃; for 1h; | 93% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
zinc(II) acetate dihydrate
(5,10,15,20-tetrakis(4-bromophenyl)porphyrinato)zinc(II)
Conditions | Yield |
---|---|
In methanol; chloroform at 77℃; for 2h; Reflux; | 92% |
With acetic acid In chloroform at 120℃; for 1.5h; | 90% |
In chloroform at 120℃; for 2.5h; Sealed tube; Microwave irradiation; | 87% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
In diethylene glycol dimethyl ether for 12h; | 91% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
aniline
Conditions | Yield |
---|---|
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In tetrahydrofuran at 100℃; for 72h; | 91% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With Yb[N(SiMe3)2]3*x[LiCl(THF)3] In diethylene glycol dimethyl ether for 12h; | 90% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
zinc(II) acetate dihydrate
zinc(II) 5,10,15,20-tetrakis-(4'-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With acetic acid In chloroform at 120℃; for 1.5h; | 90% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
N-butylamine
Conditions | Yield |
---|---|
With racemic-2-(di-tert-butylphosphino)-1,1′-binaphthyl; palladium diacetate; sodium t-butanolate In tetrahydrofuran at 100℃; for 72h; | 86% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); chloro(dimethylsulfide) gold(I) In toluene for 14h; Inert atmosphere; Schlenk technique; Reflux; | 86% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
copper(II) acetate monohydrate
copper(II) 5,10,15,20-tetrakis-(4'-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With acetic acid In chloroform at 120℃; for 1.5h; | 85% |
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triphenylmethyl)-1H-pyrazole
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With potassium phosphate tribasic trihydrate; palladium diacetate; catacxium A In toluene for 8h; Inert atmosphere; Schlenk technique; Reflux; | 85% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
phenylacetylene
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; triphenylphosphine In tetrahydrofuran at 91℃; Sonogashira Cross-Coupling; Inert atmosphere; | 84% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
N-methylaniline
Conditions | Yield |
---|---|
With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate In tetrahydrofuran at 100℃; for 72h; | 82% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
cobalt(II) diacetate tetrahydrate
cobalt(II) 5,10,15,20-tetrakis-(4'-bromophenyl)porphyrin
Conditions | Yield |
---|---|
With acetic acid In chloroform at 120℃; for 1.5h; | 82% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
diphenylamine
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; 2-dicyclohexylphosphino-2',6'-dimethylbiphenyl In tetrahydrofuran at 100℃; for 72h; | 81% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
palladium(II) meso-tetrakis(4-bromophenyl)porphyrin
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 180℃; for 0.25h; Schlenk technique; Microwave irradiation; | 81% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
methyl vinyl ketone
Conditions | Yield |
---|---|
With palladium diacetate; sodium acetate; triphenylphosphine In N,N-dimethyl-formamide at 120℃; for 24h; Heck reaction; | 80% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
tin(II) chloride dihdyrate
Conditions | Yield |
---|---|
In pyridine at 120℃; for 4h; Darkness; | 80% |
With pyridine Reflux; |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
Stage #1: 5,10,15,20-tetrakis(p-bromophenyl)porphyrin In diethyl ether at 20℃; for 0.166667h; Schlenk technique; Inert atmosphere; Stage #2: N,N-dimethyl-formamide With n-butyllithium In diethyl ether at -50 - 20℃; for 3h; Schlenk technique; Inert atmosphere; | A 80% B 5% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
cobalt(II) acetate
5,10,15,20-tetrakis(4’-bromophenyl)porphyrinato cobalt (II)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 0.00833333h; Reflux; | 80% |
In methanol; chloroform for 1.5h; Reflux; | 62% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
(5,10,15,20-tetrakis(4-bromophenyl)porphyrinato)zinc(II)
Conditions | Yield |
---|---|
In methanol; dichloromethane at 20℃; for 5h; | 80% |
5,10,15,20-tetrakis(p-bromophenyl)porphyrin
cobalt(II) diacetate tetrahydrate
5,10,15,20-tetrakis(4’-bromophenyl)porphyrinato cobalt (II)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 150℃; Inert atmosphere; | 79% |
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