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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
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inquiryfactory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryHigh Quality Best Price Storage:Store in dry, dark and ventilated place Application:Chemical Synthesis Intermediate
5-iodooctafluoro-3-oxapentanesulfonyl fluoride
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; iron(III) chloride In tetrahydrofuran at 80℃; for 6h; Temperature; Reagent/catalyst; Solvent; | 96% |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl chloride
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With potassium fluoride In acetonitrile at 20 - 34℃; for 24h; Product distribution / selectivity; | 92.7% |
With potassium fluoride In sulfolane at 60℃; for 3h; Product distribution / selectivity; | 91.5% |
With sodium fluoride In sulfolane at 73℃; Product distribution / selectivity; | 51.4% |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With Tetraethylene glycol dimethyl ether; hexafluoropropene-diethylamine adduct at 20 - 80℃; for 4h; Reagent/catalyst; | 86% |
With sulfur tetrafluoride; hydrogen fluoride at 0 - 20℃; for 16h; | 85% |
2-(1,2-dichloro-1,2,2-trifluoroethoxy)perfluorethanesulfonyl fluoride
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; bromine; zinc at 35 - 85℃; for 2h; Inert atmosphere; Cooling with ice; | 82% |
With 1-methyl-pyrrolidin-2-one; bromine; zinc at 35 - 85℃; for 2.5h; Autoclave; Inert atmosphere; | 82% |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonic acid
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With Tetraethylene glycol dimethyl ether; hexafluoropropene-diethylamine adduct at 20 - 80℃; for 4h; | 81% |
5-iodooctafluoro-3-oxapentanesulfonyl fluoride
methylmagnesium bromide
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
In tetrahydrofuran 155°C, 2 h; | 60% |
In tetrahydrofuran 155°C, 2 h; | 60% |
C7H3F7N2O3S
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With hydrogen fluoride at 60℃; for 0.5h; | 71 % Spectr. |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl chloride
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
FSO2CF2CF2OCF(CF2Cl)COONa
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
In diethylene glycol dimethyl ether at 140℃; |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
potassium tetrafluoro(2-fluorosulfonyl)-1-ethanolate
Conditions | Yield |
---|---|
With iodine In diethylene glycol dimethyl ether at 20℃; for 24h; | 96% |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With sulfuric acid In diethylene glycol dimethyl ether at 20℃; for 120h; | 73% |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With bromine at 0 - 20℃; | 65.6% |
With bromine at 0℃; |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
perfluorovinyl perfluoroiodoethyl ether
Conditions | Yield |
---|---|
With sodium iodide In dimethyl sulfoxide at 20 - 110℃; for 2h; Product distribution / selectivity; | 60% |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With potassium fluorosulfonate; bis(fluorosulfuryl) peroxide; fluorosulphonic acid at 28℃; Electrochemical reaction; |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
Stage #1: 1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride With potassium fluorosulfonate; bis(fluorosulfuryl) peroxide; fluorosulphonic acid at 28℃; Electrochemical reaction; Stage #2: With cesium fluoride In various solvent(s) Title compound not separated from byproducts; |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
2-(1,2-dichloro-1,2,2-trifluoroethoxy)perfluorethanesulfonyl fluoride
Conditions | Yield |
---|---|
With chlorine In HFC43-10mee at 20℃; |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With sodium azide; phosphorus pentoxide In acetonitrile at 20 - 40℃; for 51.3167h; Molecular sieve; Inert atmosphere; |
1,1,2,2-tetrafluoro-2-(trifluoroethenyloxy)ethanesulfonyl fluoride
Conditions | Yield |
---|---|
With potassium hydroxide In water; tert-butyl alcohol at 26 - 39℃; for 1.5h; Temperature; Solvent; |
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