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inquirytrans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
With methanol; barium dihydroxide |
trans-2-(4-acetamidocyclohexyl)acetic acid
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
With sulfuric acid | |
With sodium hydroxide In butan-1-ol at 25 - 120℃; for 16.25h; |
ethyl 2‐[(1r,4r)‐4‐aminocyclohexyl]acetate
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
With water for 12h; Heating; | 1.46 g |
trans-(4-Amino-cyclohexyl)-acetic acid ethyl ester
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chloroform; aq. NaOH solution 2: barium hydroxide; aqueous methanol View Scheme |
4-acetamidophenylacetic acid
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2 / PtO2 / acetic acid 2: aq. H2SO4 View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide; hydrogen; nickel In water at 125 - 130℃; under 86258.6 - 97509.8 Torr; for 168h; | |
With palladium 10% on activated carbon; hydrogen In water at 20℃; under 3102.97 Torr; for 72h; | |
With palladium 10% on activated carbon; hydrogen at 20℃; under 3102.97 Torr; for 72h; | |
With 5%-palladium/activated carbon; hydrogen In 2-methyl-propan-1-ol at 25 - 55℃; under 3750.38 Torr; for 6.25h; Autoclave; | 2.5 g |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 5%-palladium/activated carbon; hydrogen / methanol / 3 h / 25 - 30 °C / 1500.15 - 2250.23 Torr 2: sodium hydroxide / water / 5 h / 25 - 30 °C 3: sodium hydroxide / butan-1-ol / 16.25 h / 25 - 120 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydroxide / water / 5 h / 25 - 30 °C 2: sodium hydroxide / butan-1-ol / 16.25 h / 25 - 120 °C View Scheme |
N-(4-oxocyclohexyl)acetamide
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium tert-butylate / methanol / 1 h / 0 - 5 °C 1.2: 1 h / 0 - 5 °C 2.1: 5%-palladium/activated carbon; hydrogen / methanol / 3 h / 25 - 30 °C / 1500.15 - 2250.23 Torr 3.1: sodium hydroxide / water / 5 h / 25 - 30 °C 4.1: sodium hydroxide / butan-1-ol / 16.25 h / 25 - 120 °C View Scheme |
but-3-enoyl chloride
trans-2-(4-aminocyclohexyl)acetic acid
(4-But-3-enoylamino-cyclohexyl)-acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water 1.) 0 deg C to 5 deg C, 2.) room temp., 20 min; | 72% |
2-chloroethyl isothiocyanate
trans-2-(4-aminocyclohexyl)acetic acid
{4-[3-(2-Chloro-ethyl)-ureido]-cyclohexyl}-acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 72 percent / NaOH / H2O / 1.) 0 deg C to 5 deg C, 2.) room temp., 20 min 2: CCl4 / -30 - -20 °C 3: nitromethane / 24 h / 60 - 70 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 72 percent / NaOH / H2O / 1.) 0 deg C to 5 deg C, 2.) room temp., 20 min 2: CCl4 / -30 - -20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
C11H18ClN3O4
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH 2: NaNO2, HCO2H / formic acid View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
trans-4-aminocyclohexylacetic acid hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water pH=5; |
trans-2-(4-aminocyclohexyl)acetic acid
trans 2-{1-[4-(N-(tert-butoxycarbonyl))amino]cyclohexyl}ethyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 2 h / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
trans-2-(1-(4-(N-tert-butoxycarbonyl)amino)cyclohexyl)acetaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 2 h / 20 °C 3: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Cariprazine
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C 6: dichloromethane / 18 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: dichloromethane / 14 h / 5 - 30 °C 2: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran / 4 h / 25 - 30 °C / Inert atmosphere 3: boron trifluoride diethyl etherate; sodium tetrahydroborate / tetrahydrofuran / 1.75 h / -20 - 30 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: dichloromethane / 14 h / 5 - 30 °C 2.1: 1,1'-carbonyldiimidazole / 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran / 2 h / 25 - 30 °C / Inert atmosphere 2.2: 4 h / 25 - 30 °C / Inert atmosphere 3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran / 2 h / 0 - 5 °C / Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / 20 h / 25 - 30 °C View Scheme | |
Multi-step reaction with 6 steps 1.1: sodium hydroxide / 1,4-dioxane / 0.17 h / 0 - 5 °C 1.2: 3.16 h / 0 - 30 °C 2.1: 4-methyl-morpholine / dichloromethane / 4 h / -20 - -15 °C 3.1: hydrogenchloride / ethyl acetate / 12 h / 25 - 30 °C 4.1: triethylamine / dichloromethane / 0.17 h / 25 - 30 °C 4.2: 12 h / 25 - 30 °C 5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran / 2 h / 0 - 5 °C / Inert atmosphere 6.1: sodium tris(acetoxy)borohydride / 20 h / 25 - 30 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
trans-2-(2-(1-4-(N-tert-butyloxycarbonyl)amino)cyclohexyl)ethyl-7-cyano-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 2 h / 20 °C 3: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 2 h / 20 °C 3: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C 4: sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 20 °C / Inert atmosphere View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 2 h / 20 °C 3: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere 5: trifluoroacetic acid / 1,2-dichloro-ethane / 16 h / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C 6: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C 6: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C 6: triethylamine / dichloromethane / 14 h / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: hydrogenchloride / water / 2 h / Reflux 2.1: triethylamine / dichloromethane / 20 °C 3.1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5.1: trifluoroacetic acid / dichloromethane / 20 °C 6.1: 1,1'-carbonyldiimidazole / acetonitrile; dichloromethane / 16 h / 20 °C / Inert atmosphere 6.2: Inert atmosphere; Reflux View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C 6: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 2 h / 20 °C 3: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogenchloride / water / 2 h / Reflux 2: triethylamine / dichloromethane / 20 °C 3: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5: trifluoroacetic acid / dichloromethane / 20 °C 6: N-ethyl-N,N-diisopropylamine / dichloromethane / 14 h / 20 °C View Scheme |
trans-2-(4-aminocyclohexyl)acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: hydrogenchloride / water / 2 h / Reflux 2.1: triethylamine / dichloromethane / 20 °C 3.1: diisobutylaluminium hydride / toluene / -78 °C / Inert atmosphere 4.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C 5.1: trifluoroacetic acid / dichloromethane / 20 °C 6.1: N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 6.2: 16 h / 20 °C / Inert atmosphere View Scheme |
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