CAS No.2970-95-8,1-(3,4-Dimethoxy-phenyl)-2-dimethylamino-ethanol Suppliers

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1-(3,4-DIMETHOXYPHENYL)-2-(DIMETHYLAMINO)ETHANOL

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1-(3,4-Dimethoxy-phenyl)-2-dimethylamino-ethanol CAS：2970-95-8

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1-(3,4-Dimethoxy-phenyl)-2-dimethylamino-ethanol CAS:2970-95-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing

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Synthetic route

: 127901-47-7
N,N-dimethyl-3,4-dimethoxyphenylglyoxamide

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In tetrahydrofuran for 1h; Heating;	88%

: 33061-24-4
1-(3,4-dimethoxyphenyl)-2-(dimethylamino)ethanone

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
With sodium tetrahydroborate In methanol at 20℃; for 3.25h;	80%

: 33061-25-5
1-(3,4-dimethoxyphenyl)-2-(dimethylamino)ethanone hydrochloride

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
With ethanol; platinum Hydrogenation;

: 91-16-7
1,2-dimethoxybenzene

: 3976-11-2
N,N-dimethyl-glycine nitrile; hydrochloride

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
(i), (ii) NaBH4; Multistep reaction;

: 26285-62-1
dimethylaminomethyltributyltin

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
With n-butyllithium 1.) hexane, THF, -78 deg C, 15 min, 2.) -78 deg C, 2 h; Yield given. Multistep reaction;

: 91-16-7
1,2-dimethoxybenzene

ClO2: ClO2

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 42 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 1 h / Heating 2: sodium metaperiodate / H2O; methanol / 15 h / Ambient temperature 3: acetic anhydride / 0.5 h / Heating 4: 88 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme

: 127901-45-5
2-(3,4-Dimethoxy-phenyl)-2-methanesulfinyl-N,N-dimethyl-acetamide

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: acetic anhydride / 0.5 h / Heating 2: 88 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme

: 127901-39-7
2-(3,4-Dimethoxy-phenyl)-N,N-dimethyl-2-methylsulfanyl-acetamide

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: sodium metaperiodate / H2O; methanol / 15 h / Ambient temperature 2: acetic anhydride / 0.5 h / Heating 3: 88 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating View Scheme

: 90-05-1
2-methoxy-phenol

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1.1: 55 °C 2.1: aluminum (III) chloride / dichloromethane / 0.58 h / -5 - 0 °C 2.2: 1 h / -5 - 0 °C 3.1: bromine / chloroform / 3 h / 20 °C 4.1: ethanol / 0.67 h / 0 - 5 °C 5.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C View Scheme

: 91-16-7
1,2-dimethoxybenzene

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1.1: aluminum (III) chloride / dichloromethane / 0.58 h / -5 - 0 °C 1.2: 1 h / -5 - 0 °C 2.1: bromine / chloroform / 3 h / 20 °C 3.1: ethanol / 0.67 h / 0 - 5 °C 4.1: sodium tetrahydroborate / methanol / 3.25 h / 20 °C View Scheme

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: bromine / chloroform / 3 h / 20 °C 2: ethanol / 0.67 h / 0 - 5 °C 3: sodium tetrahydroborate / methanol / 3.25 h / 20 °C View Scheme

: 1835-02-5
2-Bromo-1-(3,4-dimethoxyphenyl)ethanone

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: ethanol / 0.67 h / 0 - 5 °C 2: sodium tetrahydroborate / methanol / 3.25 h / 20 °C View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 19611-17-7
2-(3',4'-dimethoxyphenyl)-6,7-dimethoxynaphthalene

Conditions

Conditions	Yield
With hydrogenchloride

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 571-91-5
dimethyl-(2,3,7,8-tetramethoxy-5H-dibenzo[a,d]cyclohepten-5-ylmethyl)-amine

Conditions

Conditions	Yield
With hydrogenchloride

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: C12H18NO3(1-)*K(1+)

Conditions

Conditions	Yield
With potassium hydroxide In dimethyl sulfoxide at 85℃; for 0.75h;

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 1616788-82-9
[2-(3, 4-dimethoxyphenyl)-2-phenoxyethyl]dimethylamine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 1616788-83-0
[2-(3, 4-dimethoxyphenyl)-2-phenoxyethyl]methylcarbamic acid ethyl ester

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 4-(3,4-dimethoxyphenyl)-4-(4-hydroxyphenyl)-2-methylbutyric acid ethyl ester

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: boron trifluoride diethyl etherate / ethyl acetate / 3.25 h / 0 - 20 °C View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: [2-(3,4-dimethoxyphenyl)-2-(4-methoxyphenyl)ethyl]methylcarbamic acid ethyl ester

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: boron trifluoride diethyl etherate / ethyl acetate / 3.25 h / 0 - 20 °C 5: potassium carbonate / acetone / 1 h / 20 - 45 °C View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: [2-(3,4-dimethoxyphenyl)-2-(4-methoxyphenyl)ethyl]methylamine

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: boron trifluoride diethyl etherate / ethyl acetate / 3.25 h / 0 - 20 °C 5: potassium carbonate / acetone / 1 h / 20 - 45 °C 6: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C View Scheme

Yield

Multi-step reaction with 6 steps
1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C
2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C
3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C
4: boron trifluoride diethyl etherate / ethyl acetate / 3.25 h / 0 - 20 °C
5: potassium carbonate / acetone / 1 h / 20 - 45 °C
6: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C
View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 23330-76-9, 23367-60-4, 66395-91-3, 110841-21-9
6,7-dimethoxy-4-(4-methoxyphenyl)-2-methyl-1, 2, 3, 4-tetrahydroisoquinoline

Conditions

Conditions	Yield
Multi-step reaction with 7 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: boron trifluoride diethyl etherate / ethyl acetate / 3.25 h / 0 - 20 °C 5: potassium carbonate / acetone / 1 h / 20 - 45 °C 6: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C 7: formaldehyd / acetic acid / 2 h / 90 °C / Inert atmosphere View Scheme

Yield

Multi-step reaction with 7 steps
1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C
2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C
3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C
4: boron trifluoride diethyl etherate / ethyl acetate / 3.25 h / 0 - 20 °C
5: potassium carbonate / acetone / 1 h / 20 - 45 °C
6: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C
7: formaldehyd / acetic acid / 2 h / 90 °C / Inert atmosphere
View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 1616788-86-3
[2-(3,4-dimethoxyphenyl)-2-phenoxyethyl]methylamine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 1616788-87-4
[2-(3,4-dimethoxyphenyl)-2-phenoxyethyl]methylamine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C 5: formaldehyd / acetic acid / 1 h / 90 °C / Inert atmosphere View Scheme

: 2970-95-8
1-(3, 4-dimethoxyphenyl)-2-dimethylaminoethanol

: 1616781-25-9
4-(6,7-dimethoxy-2-methyl-1, 2, 3, 4-tetrahydroisoquinolin-4-yl)phenol

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C 2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C 3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C 4: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C 5: formaldehyd / acetic acid / 1 h / 90 °C / Inert atmosphere 6: boron trifluoride diethyl etherate / ethyl acetate / 2.25 h / 0 - 20 °C View Scheme

Yield

Multi-step reaction with 6 steps
1: potassium hydroxide / dimethyl sulfoxide / 0.75 h / 85 °C
2: potassium hydroxide / dimethyl sulfoxide / 2 h / 20 - 120 °C
3: sodium hydrogencarbonate / toluene / 2.5 h / 120 °C
4: sodium hydroxide / dimethyl sulfoxide / 6 h / 125 °C
5: formaldehyd / acetic acid / 1 h / 90 °C / Inert atmosphere
6: boron trifluoride diethyl etherate / ethyl acetate / 2.25 h / 0 - 20 °C
View Scheme

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