CAS No.3221-15-6,EPITHIOCHLORHYDRIN Suppliers

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Thiirane,2-(chloromethyl)- cas 3221-15-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Thiirane,2-(chloromethyl)-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect

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Synthetic route

: 106-89-8
epichlorohydrin

: 3221-15-6
2-(chloromethyl)thiirane

Conditions

Conditions	Yield
With ammonium thiocyanate; bismuth(lll) trifluoromethanesulfonate In acetonitrile for 0.416667h; Heating;	99%
With tin(IV)tetraphenylporphyrinato trifluoromethanesulfonate; ammonium thiocyanate In acetonitrile for 0.416667h; Heating;	99%
With bismuth(III) chloride; ammonium thiocyanate In acetonitrile for 0.333333h; Heating;	98%

: N-(tert-butyl)-5-(chloromethyl)-1,3-oxathiolan-2-imine

A: 3221-15-6
2-(chloromethyl)thiirane

B: 1609-86-5
Tert-butyl isocyanate

Conditions

Conditions	Yield
In quinoline at 230℃;	A 12% B 81%

: 333-20-0
potassium thioacyanate

: 106-89-8
epichlorohydrin

: 3221-15-6
2-(chloromethyl)thiirane

Conditions

Conditions	Yield
With methanol
With methanol

: 17356-08-0
thiourea

: 106-89-8
epichlorohydrin

: 3221-15-6
2-(chloromethyl)thiirane

Conditions

Conditions	Yield
With methanol

: 102-08-9
N,N-diphenylthiourea

: 106-89-8
epichlorohydrin

: 3221-15-6
2-(chloromethyl)thiirane

Conditions

Conditions	Yield
With benzene

: 1147550-11-5
ammonium thiocyanate

: 106-89-8
epichlorohydrin

A: 3221-15-6
2-(chloromethyl)thiirane

B: 147194-24-9
3-chloro-2-hydroxypropyl thiocyanate

Conditions

Conditions	Yield
With 2,6-bis[2-(o-aminophenoxy)methyl]-4-bromo-1-methoxybenzene In dichloromethane; acetonitrile at 70℃; for 1.25h;	A n/a B 78 % Chromat.

...Expand

: 3221-15-6
2-(chloromethyl)thiirane

: 29027-25-6
chloromethylthiirane-S-monooxide

Conditions

Conditions	Yield
With water; fluorine; acetonitrile; propiononitrile In methanol at -78℃;	95%

: 3221-15-6
2-(chloromethyl)thiirane

: 93703-24-3
3-methyl-8-bromoxanthine

: 1005482-51-8
8-bromo-3-methyl-7-(thietan-3-yl)-3,7-dihydro-1H-pyrine-2,6-dione

Conditions

Conditions	Yield
With potassium hydroxide In water; N,N-dimethyl-formamide at 0 - 20℃;	94.3%

: 3221-15-6
2-(chloromethyl)thiirane

: chloromethylthiirane-S,S-dioxide

Conditions

Conditions	Yield
With water; fluorine; acetonitrile In dichloromethane at -15 - 0℃;	90%

: 3221-15-6
2-(chloromethyl)thiirane

: 75-36-5
acetyl chloride

: 16621-53-7
thioacetic acid S-(2-chloro-1-chloromethyl-ethyl) ester

Conditions

Conditions	Yield
With CoCl2 In dichloromethane at 20℃; for 4h;	81%

: 3221-15-6
2-(chloromethyl)thiirane

: 4857-06-1
2-chloro-1H-benzoimidazole

: 2-<1-(2-chlorobenzimidazolyl)>methyl-2,3-dihydrothiazolo<3,2-a>benzimidazole

Conditions

Conditions	Yield
With potassium carbonate In acetone for 3h; Heating;	80%

: 3221-15-6
2-(chloromethyl)thiirane

: 64-19-7
acetic acid

A: 61704-46-9
2,5-bis(chloromethyl)-1,4-dithiane

B: 136197-48-3
1-acetoxy-3-chloropropane-2-thiol

Conditions

Conditions	Yield
With lithium perchlorate In ethyl acetate Ambient temperature;	A 80% B 12%

...Expand

: 3221-15-6
2-(chloromethyl)thiirane

A: 61704-46-9
2,5-bis(chloromethyl)-1,4-dithiane

B: 136197-48-3
1-acetoxy-3-chloropropane-2-thiol

Conditions

Conditions	Yield
With lithium perchlorate; acetic acid In ethyl acetate Ambient temperature;	A 80% B 12%

: 3221-15-6
2-(chloromethyl)thiirane

: 536-74-3
phenylacetylene

: 1-chloro-3-(5-phenyl-1H-1,2,3-triazol-1-yl)propane-2-thiol

Conditions

Conditions	Yield
With sodium azide In water at 60℃; for 2.5h; Green chemistry; regioselective reaction;	80%

: 3221-15-6
2-(chloromethyl)thiirane

: 13463-94-0
N-(4-chlorophenyl)cyanamide

: C10H9ClN2S

Conditions

Conditions	Yield
With potassium hydroxide In water at 20℃; for 48h;	76%

: 3221-15-6
2-(chloromethyl)thiirane

: 14213-18-4
3-fluorophenylcyanamide

: N-(3-fluorophenyl)-N-(thietan-3-yl)cyanamide

Conditions

Conditions	Yield
With potassium hydroxide In water at 20℃; for 48h;	74%

: 3221-15-6
2-(chloromethyl)thiirane

: 4857-06-1
2-chloro-1H-benzoimidazole

: 136265-52-6
1-(thietan-3-yl)-2-chlorobenzimidazole

Conditions

Conditions	Yield
With potassium hydroxide In water at 60℃; for 3h;	73%

: 3221-15-6
2-(chloromethyl)thiirane

: 121-92-6
3-nitrobenzoic acid

: 3-Nitro-benzoic acid thietan-3-yl ester

Conditions

Conditions	Yield
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In water at 60 - 70℃;	73%

: 3221-15-6
2-(chloromethyl)thiirane

: 622-34-4
1-phenylcyanamide

: N-phenyl-N-(thietan-3-yl)cyanamide

Conditions

Conditions	Yield
With potassium hydroxide In water at 20℃; for 48h;	72%

: 3221-15-6
2-(chloromethyl)thiirane

: 7411-23-6
3,5-dibromotriazole

: 2-bromo-5-(3,5-dibromo-1H-1,2,4-triazol-1-yl-methyl)-5,6-dihydro-1,3-thiazolo[3,2-b][1,2,4]triazole

Conditions

Conditions	Yield
With potassium carbonate In acetone for 3h; Heating;	71%

: 3221-15-6
2-(chloromethyl)thiirane

: 445-29-4
o-fluoro-benzoic acid

: 2-Fluoro-benzoic acid thietan-3-yl ester

Conditions

Conditions	Yield
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In water at 60 - 70℃;	70%

: 3221-15-6
2-(chloromethyl)thiirane

: 89-52-1
o-acetylamino-benzoic acid

: 2-Acetylamino-benzoic acid thietan-3-yl ester

Conditions

Conditions	Yield
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In water at 60 - 70℃;	69%

: 3221-15-6
2-(chloromethyl)thiirane

: 22666-84-8
4-hydroxybenzaldehyde sodium salt

: 4-(thietan-3-yloxy)benzaldehyde

Conditions

Conditions	Yield
In methanol; water at 45 - 55℃; for 2h;	69%

: 3221-15-6
2-(chloromethyl)thiirane

: 873-83-6
4-Amino-2,6-dihydroxypyrimidine

: 6-(thietan-3-ylamino)pyrimidine-2,4(1H,3H)-dione

Conditions

Conditions	Yield
With potassium hydroxide In water at 50 - 55℃; for 2h;	69%

: 3221-15-6
2-(chloromethyl)thiirane

: 60592-84-9
N-(4-bromophenyl)cyanamide

: C10H9BrN2S

Conditions

Conditions	Yield
With potassium hydroxide In water at 20℃; for 48h;	69%

: 3221-15-6
2-(chloromethyl)thiirane

: 67-56-1
methanol

: 130258-47-8
1-Chloro-2-(1-chloromethyl-2-methoxy-ethyldisulfanyl)-3-methoxy-propane

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate for 0.66h; Heating;	68%
With 2,3-dicyano-5,6-dichloro-p-benzoquinone for 3.5h; Heating;	45%

: 3221-15-6
2-(chloromethyl)thiirane

: 5026-62-0
sodium methylparaben

: methyl 4-(thietane-3-yloxy)benzoate

Conditions

Conditions	Yield
In methanol; water at 45 - 55℃; for 2h;	68%

: 3221-15-6
2-(chloromethyl)thiirane

: sodium n-hexyl xanthogenate

: Dithiocarbonic acid O-hexyl ester S-thiiranylmethyl ester

Conditions

Conditions	Yield
In benzene at 70 - 80℃; for 3h;	67%

: 3221-15-6
2-(chloromethyl)thiirane

: 123-99-9
azelaic acid

A: 122976-45-8
Nonanedioic acid mono-thietan-3-yl ester

B: 122976-44-7
Nonanedioic acid dithietan-3-yl ester

Conditions

Conditions	Yield
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In water 1.) 1 h, 70 deg C, 2.) 8 h, 70 deg C;	A 6% B 65%
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In water 1.) 1 h, 70 deg C, 2.) 8 h, 70 deg C;	A 6% B 65%

...Expand

: 3221-15-6
2-(chloromethyl)thiirane

: 64-17-5
ethanol

: 130258-48-9
1-Chloro-2-(1-chloromethyl-2-ethoxy-ethyldisulfanyl)-3-ethoxy-propane

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate for 0.66h; Heating;	65%
With 2,3-dicyano-5,6-dichloro-p-benzoquinone for 5h; Heating;	60%

: 3221-15-6
2-(chloromethyl)thiirane

: 140-93-2
sodium isopropylxanthate

: S-(1,2-epithiopropyl) isopropylxanthate

Conditions

Conditions	Yield
In benzene at 70 - 80℃; for 3h;	65%

: 3221-15-6
2-(chloromethyl)thiirane

: 45765-25-1
(2-chlorophenyl)cyanamide

: N-(2-chlorophenyl)-N-(thietan-3-yl)cyanamide

Conditions

Conditions	Yield
With potassium hydroxide In water at 20℃; for 48h;	63%

: 3221-15-6
2-(chloromethyl)thiirane

: 7471-26-3
N-(4-methoxyphenyl)benzenesulphonamide

: N-(4-methoxyphenyl)-N-(thietan-3-yl)benzenesulfonamide

Conditions

Conditions	Yield
With potassium hydroxide In water at 20℃; for 10h;	62%

: 2875-23-2, 127089-57-0
(E)-3-(2-furanyl)-1-(2'-hydroxyphenyl)-2-propen-1-one

: 3221-15-6
2-(chloromethyl)thiirane

: (E)-3-(furan-2-yl)-1-(2-(thiiran-2-ylmethoxy)phenyl)prop-2-en-1-one

Conditions

Conditions	Yield
With potassium carbonate In N,N-dimethyl-formamide; acetone at 70 - 80℃; for 20h;	61.8%

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Hazard Codes	T
Risk Statements	43-34-23/24/25
Safety Statements	45-38-36/37/39-28A-26-24

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Henan Tianfu Chemical Co., Ltd.

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Henan Wentao Chemical Product Co., Ltd.

Hangzhou J&H Chemical Co., Ltd.

KAISA GROUP INC

Antimex Chemical Limied

HANGZHOU TIANYE CHEMICALS CO., LTD.

Changchun Artel lmport and Export trade company

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LEAP CHEM Co., Ltd.

Jilin haofei import and export trade Co.,Ltd

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Finetech Industry Limited

Nanjing Raymon Biotech Co., Ltd.

RennoTech Co., Ltd.

Wuxi D-Stone International Co., Ltd.

Chemical Co.Ltd

Synthetic route

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