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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:0 Metric Ton

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Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hot Sell Factory Supply Raw Material CAS 339549-67-6 ,cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:10 Kilogram

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Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph

Cyclopentyl-3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Cyclopentyl 3-methoxyphenyl ketone 339549-67-6

Cas:339549-67-6

Min.Order:1 Kilogram

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Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:1 Kilogram

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Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

High Purity Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Type:Trading Company

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:1 Gram

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Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:1 Kilogram

Negotiable

Type:Other

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

Cyclopentyl(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

Negotiable

Type:Manufacturers

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Wuhan Circle Star Chem-medical Technology co.,Ltd.

1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Cyclopentyl 3-Methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Qingdao Beluga Import and Export Co., LTD

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:0

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Hubei Langyou International Trading Co., Ltd

cyclopentyl-(3-methoxyphenyl)methanone Application:cyclopentyl-(3-methoxyphenyl)methanone

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:0

Negotiable

Type:Other

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DB BIOTECH CO., LTD

best seller Application:API

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

Negotiable

Type:Trading Company

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BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use

CYCLOPENTYL 3-METHOXYPHENYL KETONE

Cas:339549-67-6

Min.Order:0

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Type:Trading Company

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Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

339549-67-6

Cas:339549-67-6

Min.Order:0

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Type:Trading Company

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Hangzhou Fandachem Co.,Ltd

CYCLOPENTYL 3-METHOXYPHENYL KETONEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express

CYCLOPENTYL 3-METHOXYPHENYL KETONE

Cas:339549-67-6

Min.Order:0

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Type:Other

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Type:Lab/Research institutions

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Type:Lab/Research institutions

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Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

cyclopentyl-(3-methoxyphenyl)methanone

Cas:339549-67-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Changzhou Helios Biomedical Science and Technology Co.,LTD.

Changzhou Helios Biochemical Co., Ltd is a leading manufacturer and supplier for medical intermediates and pesticide intermediates . We specialize in custom synthesis of benzene ring, pyridine and pyrimidine derivatives to help customers to accelerat

Cyclopentyl 3-methoxyphenyl ketone

Cas:339549-67-6

Min.Order:0

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Synthetic route

3-methoxybenzonitrile
1527-89-5

3-methoxybenzonitrile

cyclopentylmagnesium bromide
33240-34-5

cyclopentylmagnesium bromide

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
In diethyl ether at 0 - 20℃; for 6h; Inert atmosphere;51%
Stage #1: 3-methoxybenzonitrile; cyclopentylmagnesium bromide In diethyl ether at 0℃; Inert atmosphere; Reflux;
Stage #2: With water In diethyl ether Acidic conditions;
C14H19BrO5S

C14H19BrO5S

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
With samarium diiodide In tetrahydrofuran at 23℃; Inert atmosphere;36%
Cyclopentyl bromide
137-43-9

Cyclopentyl bromide

3-methoxybenzonitrile
1527-89-5

3-methoxybenzonitrile

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
With magnesium In tetrahydrofuran
C13H17BrO3

C13H17BrO3

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: trimethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
2: samarium diiodide / tetrahydrofuran / 23 °C / Inert atmosphere
View Scheme
hexahydro-2H-oxepin-2-one
502-44-3

hexahydro-2H-oxepin-2-one

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: magnesium; iodine / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere
1.2: -15 - 20 °C / Inert atmosphere
2.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 23 °C / Inert atmosphere
3.1: trimethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
4.1: samarium diiodide / tetrahydrofuran / 23 °C / Inert atmosphere
View Scheme
C13H18O3

C13H18O3

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: phenyltrimethylammonium tribromide / tetrahydrofuran / 23 °C / Inert atmosphere
2: trimethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
3: samarium diiodide / tetrahydrofuran / 23 °C / Inert atmosphere
View Scheme
3-methoxyphenyl bromide
2398-37-0

3-methoxyphenyl bromide

(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: magnesium; iodine / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere
1.2: -15 - 20 °C / Inert atmosphere
2.1: phenyltrimethylammonium tribromide / tetrahydrofuran / 23 °C / Inert atmosphere
3.1: trimethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
4.1: samarium diiodide / tetrahydrofuran / 23 °C / Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

(-)-cyclopentyl(3-methoxyphenyl)methanol

(-)-cyclopentyl(3-methoxyphenyl)methanol

Conditions
ConditionsYield
With phenylsilane; copper(II) acetate monohydrate; (S)-2,2',6,6'-tetramethoxy-4,4'-bis(di(3,5-xylyl)phosphino)-3,3'-bipyridine In toluene at -20℃; for 36h; enantioselective reaction;96%
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

(methoxymethyl)triphenylphosphonium chloride
4009-98-7

(methoxymethyl)triphenylphosphonium chloride

C15H20O2

C15H20O2

Conditions
ConditionsYield
Stage #1: (methoxymethyl)triphenylphosphonium chloride With n-butyllithium; phenyllithium In diethyl ether; hexane at -78 - 0℃;
Stage #2: (m-methoxyphenyl)cyclopentyl ketone In diethyl ether; hexane at -78 - 0℃; Wittig reaction;
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

1-bromocyclopentyl (m-methoxyphenyl) ketone

1-bromocyclopentyl (m-methoxyphenyl) ketone

Conditions
ConditionsYield
With bromine In tetrachloromethane at 0 - 20℃; for 1h;30.1 g
With bromine In tetrachloromethane
With copper(ll) bromide In ethyl acetate for 4h; Reflux;274.6 g
With copper(ll) bromide In ethyl acetate for 4h; Reflux;
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

1-(alpha-benzylimino-m-methoxybenzyl)cyclopentanol

1-(alpha-benzylimino-m-methoxybenzyl)cyclopentanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bromine / tetrachloromethane / 1 h / 0 - 20 °C
2: benzene / 120 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: toluene / 120 h
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

2-(benzylamino)-2-(m-methoxyphenyl)cyclohexanone

2-(benzylamino)-2-(m-methoxyphenyl)cyclohexanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: bromine / tetrachloromethane / 1 h / 0 - 20 °C
2: benzene / 120 h / 20 °C
3: Dowtherm TM / 7 h / 20 - 200 °C
View Scheme
Multi-step reaction with 3 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: toluene / 120 h
3: 2-methyl-propan-1-ol / 2 h / 150 °C / Microwave irradiation
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

2-[N-benzyl-N-(6-ethoxy-6-oxohexyl)]-2-(m-methoxyphenyl)cyclohexanone

2-[N-benzyl-N-(6-ethoxy-6-oxohexyl)]-2-(m-methoxyphenyl)cyclohexanone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: bromine / tetrachloromethane / 1 h / 0 - 20 °C
2.1: benzene / 120 h / 20 °C
3.1: Dowtherm TM / 7 h / 20 - 200 °C
4.1: 1,2-dichloro-ethane / 0.17 h / 20 °C
4.2: 20 °C
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C26H33NO4

C26H33NO4

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: bromine / tetrachloromethane / 1 h / 0 - 20 °C
2.1: benzene / 120 h / 20 °C
3.1: Dowtherm TM / 7 h / 20 - 200 °C
4.1: 1,2-dichloro-ethane / 0.17 h / 20 °C
4.2: 20 °C
5.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

N-(5-carboxypentyl)-N-desethylmethoxetamine

N-(5-carboxypentyl)-N-desethylmethoxetamine

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: bromine / tetrachloromethane / 1 h / 0 - 20 °C
2.1: benzene / 120 h / 20 °C
3.1: Dowtherm TM / 7 h / 20 - 200 °C
4.1: 1,2-dichloro-ethane / 0.17 h / 20 °C
4.2: 20 °C
5.1: lithium hydroxide monohydrate; water / tetrahydrofuran / 20 °C
6.1: 5%-palladium/activated carbon; hydrogen / ethanol / 20 °C
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

(±)-2-(3-methoxyphenyl)-2-(ethylamino)cyclohexanone

(±)-2-(3-methoxyphenyl)-2-(ethylamino)cyclohexanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: bromine / tetrachloromethane
2: 0 °C
3: decalin / 190 °C / Microwave irradiation
View Scheme
Multi-step reaction with 3 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: 18 h / -40 - 20 °C / Sealed tube; Inert atmosphere
3: palladium dichloride / decalin / 10 h / Sealed tube; Heating
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

1-((Ethylimino)(3-methoxyphenyl) methyl)cyclopentan-1-ol

1-((Ethylimino)(3-methoxyphenyl) methyl)cyclopentan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bromine / tetrachloromethane
2: 0 °C
View Scheme
Multi-step reaction with 2 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: 18 h / -40 - 20 °C / Sealed tube; Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C15H23NO2

C15H23NO2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: bromine / tetrachloromethane
2: 0 °C
3: decalin / 190 °C / Microwave irradiation
4: sodium tetrahydroborate; methanol
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C14H19NO2

C14H19NO2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: bromine / tetrachloromethane
2: 0 °C
3: decalin / 190 °C / Microwave irradiation
4: hydrogen bromide / water / Reflux
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C14H21NO2

C14H21NO2

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: bromine / tetrachloromethane
2: 0 °C
3: decalin / 190 °C / Microwave irradiation
4: hydrogen bromide / water / Reflux
5: sodium tetrahydroborate; methanol
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C18H25NO4

C18H25NO4

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: ammonia / ethyl acetate / 4 h
3.1: tetrahydrofuran; 2-methyl-propan-1-ol / 18 h / Reflux
4.1: L-Pyroglutamic acid / methanol / 20 °C
5.1: L-Pyroglutamic acid; triethylamine / tetrahydrofuran / 0.01 h / Inert atmosphere
5.2: 18 h / 70 °C / Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C21H33NO4Si

C21H33NO4Si

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: ammonia / ethyl acetate / 4 h
3.1: tetrahydrofuran; 2-methyl-propan-1-ol / 18 h / Reflux
4.1: L-Pyroglutamic acid / methanol / 20 °C
5.1: L-Pyroglutamic acid; triethylamine / tetrahydrofuran / 0.01 h / Inert atmosphere
5.2: 18 h / 70 °C / Inert atmosphere
6.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.45 h / -78 °C / Inert atmosphere
6.2: 1.25 h / -78 - 0 °C
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C18H25NO5

C18H25NO5

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: ammonia / ethyl acetate / 4 h
3.1: tetrahydrofuran; 2-methyl-propan-1-ol / 18 h / Reflux
4.1: L-Pyroglutamic acid / methanol / 20 °C
5.1: L-Pyroglutamic acid; triethylamine / tetrahydrofuran / 0.01 h / Inert atmosphere
5.2: 18 h / 70 °C / Inert atmosphere
6.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.45 h / -78 °C / Inert atmosphere
6.2: 1.25 h / -78 - 0 °C
7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -15 - 20 °C / Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

(2R,6R)-2-amino-6-hydroxy-2-(3-methoxyphenyl)cyclohexan-1-one hydrochloride

(2R,6R)-2-amino-6-hydroxy-2-(3-methoxyphenyl)cyclohexan-1-one hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: ammonia / ethyl acetate / 4 h
3.1: tetrahydrofuran; 2-methyl-propan-1-ol / 18 h / Reflux
4.1: L-Pyroglutamic acid / methanol / 20 °C
5.1: L-Pyroglutamic acid; triethylamine / tetrahydrofuran / 0.01 h / Inert atmosphere
5.2: 18 h / 70 °C / Inert atmosphere
6.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.45 h / -78 °C / Inert atmosphere
6.2: 1.25 h / -78 - 0 °C
7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -15 - 20 °C / Inert atmosphere
8.1: 3-chloro-benzenecarboperoxoic acid; hydrogenchloride / 18 h / Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C23H33NO2Si

C23H33NO2Si

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: toluene / 120 h
3.1: 2-methyl-propan-1-ol / 2 h / 150 °C / Microwave irradiation
4.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.45 h / -78 °C / Inert atmosphere
4.2: 1.25 h / -78 - 0 °C
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C20H23NO3

C20H23NO3

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: toluene / 120 h
3.1: 2-methyl-propan-1-ol / 2 h / 150 °C / Microwave irradiation
4.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.45 h / -78 °C / Inert atmosphere
4.2: 1.25 h / -78 - 0 °C
5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -15 - 20 °C / Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

(2R,6R)-2-amino-6-hydroxy-2-(3-methoxyphenyl)cyclohexan-1-one

(2R,6R)-2-amino-6-hydroxy-2-(3-methoxyphenyl)cyclohexan-1-one

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2.1: toluene / 120 h
3.1: 2-methyl-propan-1-ol / 2 h / 150 °C / Microwave irradiation
4.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 0.45 h / -78 °C / Inert atmosphere
4.2: 1.25 h / -78 - 0 °C
5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -15 - 20 °C / Inert atmosphere
6.1: 3-chloro-benzenecarboperoxoic acid; hydrogenchloride / 18 h / Inert atmosphere
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C13H17NO2

C13H17NO2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: ammonia / ethyl acetate / 4 h
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

2-amino-2-(3-methoxyphenyl)cyclohexan-1-one

2-amino-2-(3-methoxyphenyl)cyclohexan-1-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: ammonia / ethyl acetate / 4 h
3: tetrahydrofuran; 2-methyl-propan-1-ol / 18 h / Reflux
View Scheme
(m-methoxyphenyl)cyclopentyl ketone
339549-67-6

(m-methoxyphenyl)cyclopentyl ketone

C13H17NO2*H(1+)

C13H17NO2*H(1+)

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: copper(ll) bromide / ethyl acetate / 4 h / Reflux
2: ammonia / ethyl acetate / 4 h
3: tetrahydrofuran; 2-methyl-propan-1-ol / 18 h / Reflux
4: L-Pyroglutamic acid / methanol / 20 °C
View Scheme

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