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Cas:350-31-2
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryProduct name: 4-Chloro-3-Fluoronitrobenzene CAS No.:350-31-2 Molecule Formula:C6H3ClFNO2 Molecule Weight:175.54 Purity: 98.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TE
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inquiryProduct Name: 4-Chloro-3-fluoronitrobenzene Synonyms: 350-31-2;4-Chloro-3-fluoronitrobenzenen;3-FLUORO-4-CHLORONITROBENZENE;4-CHLORO-3-FLUORONITROBENZENE;1-chloro-2-fluoro-4-nitrobenzene;3-FLUORO-4-CHLORONITROBENZENE,99%;1-Chloro-2-fluoro-4-nit
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High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is
Cas:350-31-2
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Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
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Conditions | Yield |
---|---|
With para-tert-butylphenol; phosphorus pentachloride 1.) 130-140 deg C, 2 h, 2.) 230-240 deg C, 40 min; | 61% |
Conditions | Yield |
---|---|
With formic acid; fluorine at 10℃; for 1.75h; Fluorination; | 44% |
With sulfuric acid; fluorine |
1-chloro-2-fluorobenzene
A
3-chloro-4-fluoronitrobenzene
B
1-chloro-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
With nitric acid at 0℃; | |
With sulfuric acid; nitric acid at 0℃; for 0.5h; other reagent: nitric acid/acetic anhydride/zeolite H(1+)β; Yield given; Yields of byproduct given. Title compound not separated from byproducts; | |
With molecular sieve; nitric acid; acetic anhydride at 0℃; for 3h; other reagent: nitric acid/sulfuric acid; Yield given; Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
With sulfuric acid at -5℃; Diazotization.Behandeln der Diazoniumsalz-Loesung mit Natriumnitrit und Kupfer(I)-kupfer(II)-sulfit in Wasser; |
1-chloro-2-fluorobenzene
nitric acid
A
3-chloro-4-fluoronitrobenzene
B
1-chloro-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
at 0℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium dicarbonate; hydrochloric acid; calcium chloride. 2: hydrochloric acid / Bei Kochen mit 20prozentiger Saeure 3: diluted sulfuric acid / -5 °C / Diazotization.Behandeln der Diazoniumsalz-Loesung mit Natriumnitrit und Kupfer(I)-kupfer(II)-sulfit in Wasser View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrochloric acid / Bei Kochen mit 20prozentiger Saeure 2: diluted sulfuric acid / -5 °C / Diazotization.Behandeln der Diazoniumsalz-Loesung mit Natriumnitrit und Kupfer(I)-kupfer(II)-sulfit in Wasser View Scheme |
morpholine
1-chloro-2-fluoro-4-nitrobenzene
3-fluoro-4-(4-morpholinyl)nitrobenzene
Conditions | Yield |
---|---|
Neat (no solvent); | 100% |
1-chloro-2-fluoro-4-nitrobenzene
sodium thiophenolate
3-fluoro-4-(phenylthio)nitrobenzene
Conditions | Yield |
---|---|
In methanol for 5h; Ambient temperature; | 78% |
2-oxa-6-azaspiro[3.4]octane hemioxalate
1-chloro-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 24.25h; Inert atmosphere; | 76% |
1-chloro-2-fluoro-4-nitrobenzene
ethylene glycol
2-(2-fluoro-4-nitrophenoxy)ethan-1-ol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 12h; | 72.2% |
1-chloro-2-fluoro-4-nitrobenzene
phenylmethanethiol
1-(benzylsulfanyl)-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 12h; | 62% |
1-chloro-2-fluoro-4-nitrobenzene
8-oxa-3-azabicyclo[3.2.1]octane hydrochloride
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 24.25h; Inert atmosphere; Sealed tube; | 39% |
1-chloro-2-fluoro-4-nitrobenzene
sodium methylate
A
2-fluoro-1-methoxy-4-nitrobenzene
B
2-chloro-5-nitroanisole
Conditions | Yield |
---|---|
In methanol for 12h; Heating; | A 37% B 22% |
1-chloro-2-fluoro-4-nitrobenzene
sodium methylate
3,4-dimethoxynitrobenzene
Conditions | Yield |
---|---|
at 80℃; | |
at 80℃; |
o-hydroxymethyl thiophenol
1-chloro-2-fluoro-4-nitrobenzene
[2-(2-Fluoro-4-nitro-phenylsulfanyl)-phenyl]-methanol
Conditions | Yield |
---|---|
With copper; potassium carbonate at 160 - 170℃; |
1-chloro-2-fluoro-4-nitrobenzene
[2-(4-Chloro-2-fluoro-phenylsulfanyl)-phenyl]-methanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Cu, K2CO3 / 160 - 170 °C 2: aq. HCl, Fe / ethanol 3: (i) NaNO2, aq. HCl, (ii) CuCl View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
[2-(4-Amino-2-fluoro-phenylsulfanyl)-phenyl]-methanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Cu, K2CO3 / 160 - 170 °C 2: aq. HCl, Fe / ethanol View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / o-xylene / Reflux 4.2: 15 h / 90 °C / Inert atmosphere 5.1: 15 h / 20 °C View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
linezolid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / o-xylene / 1 h / Reflux 5.1: hydrogenchloride; water / 0.25 h / 20 °C 5.2: pH 8 - 9 6.1: dichloromethane; water / 1 h / 20 °C 6.2: pH 9 / cooling with ice View Scheme | |
Multi-step reaction with 4 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: sodium hydrogencarbonate / water 4: n-butyllithium View Scheme | |
Multi-step reaction with 4 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: toluene / -20 °C / Inert atmosphere; Reflux 4: Tributylphosphine oxide; lithium bromide / o-xylene View Scheme | |
Multi-step reaction with 6 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / toluene / 1 h / Inert atmosphere; Reflux 5.1: hydrogenchloride / dichloromethane; water / 1 h / 20 °C 5.2: pH 7 / cooling with ice 6.1: dichloromethane; water / 1 h / 20 °C 6.2: pH 9 / cooling with ice View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
(S)-N-[[3-[3-fluoro-4-[4-morpholinyl]phenyl]-2-oxo-5-oxazolidinyl]methyl]amine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / o-xylene / 1 h / Reflux 5.1: hydrogenchloride; water / 0.25 h / 20 °C 5.2: pH 8 - 9 View Scheme | |
Multi-step reaction with 5 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / toluene / 1 h / Inert atmosphere; Reflux 5.1: hydrogenchloride / dichloromethane; water / 1 h / 20 °C 5.2: pH 7 / cooling with ice View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: sodium hydrogencarbonate / water View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
3-fluoro-4-(morpholin-4-yl)-phenyl isocyanate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: toluene / -20 °C / Inert atmosphere; Reflux View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
3-fluoro-4-(morpholinyl)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: toluene / -20 °C / Inert atmosphere; Reflux 4: Tributylphosphine oxide; lithium bromide / o-xylene / 1 h / Reflux 5: hydrogenchloride; ethanol / ethyl acetate / 45 °C View Scheme | |
Multi-step reaction with 5 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / toluene / 1 h / Inert atmosphere; Reflux 5.1: hydrogenchloride; water / dichloromethane / 0.5 h / 20 °C 5.2: pH 8 - 9 View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
(S)-(E,Z)-5-((benzylideneamino)methyl)-3-(3-fluoro-4-morpholinophenyl)oxazolidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: toluene / -20 °C / Inert atmosphere; Reflux 4: Tributylphosphine oxide; lithium bromide / o-xylene / 1 h / Reflux View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
(S)-(E,Z)-5-((4-chlorobenzylideneamino)methyl)-3-(3-fluoro-4-morpholinophenyl)oxazolidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: toluene / -20 °C / Inert atmosphere; Reflux 4: Tributylphosphine oxide; lithium bromide / toluene / 1 h / Inert atmosphere; Reflux View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
B
(S)-5-(chloromethyl)-3-[3-fluoro-4-(4-morpholinyl)phenyl]-2-oxazolid-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Neat (no solvent) 2: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3: toluene / -20 °C / Inert atmosphere; Reflux 4: Tributylphosphine oxide; lithium bromide / o-xylene / Reflux View Scheme |
1-chloro-2-fluoro-4-nitrobenzene
(S)-5-(azidomethyl)-3-[3-fluoro-4-(4-morpholinyl)phenyl]-2-oxazolin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: Neat (no solvent) 2.1: ammonium formate / palladium 10% on activated carbon / tetrahydrofuran; methanol / 20 °C / Inert atmosphere; cooling with ice 3.1: toluene / -20 °C / Inert atmosphere; Reflux 4.1: Tributylphosphine oxide; lithium bromide / o-xylene / Reflux 4.2: 15 h / 90 °C / Inert atmosphere View Scheme |
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