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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

2-Amino-1-(2,5-dimethoxyphenyl)ethanol Manufacturer/High quality/Best price/In stock

Cas:3600-87-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Desglymidodrine

Cas:3600-87-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 3600-87-1 with best quality

Cas:3600-87-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

2-Amino-1-(2,5-dimethoxyphenyl)ethanol CAS3600-87-1

Cas:3600-87-1

Min.Order:1 Kilogram

FOB Price: $289.0 / 499.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Benzenemethanol, a-(aminomethyl)-2,5-dimethoxy-

Cas:3600-87-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Superiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail bes

Factory wholesale 98% 2-Amino-1-(2,5-dimethoxyphenyl)ethanol CAS:3600-87-1

Cas:3600-87-1

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzenemethanol, a-(aminomethyl)-2,5-dimethoxy-

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:White Powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:A metabolite of Mid

Benzenemethanol, a-(aminomethyl)-2,5-dimethoxy-

Cas:3600-87-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benzenemethanol, a-(aminomethyl)-2,5-dimethoxy-

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h

Factory Supply 2,5-Dimethoxyphenyl-2-hydroxyethylamine

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and

TIANFUCHEM--3600-87-1--2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Desglymidodrine

Cas:3600-87-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

你好,亲爱的朋友! 我是中国的汉森和艾伦。欢迎来到我的lookchem商城!以下是我们公司产品和服务的简要介绍。如果您对我们的产品感兴趣,请及时通过电子邮件与我们联系 产品质量 √1,产品质量通过专业的生产工艺和质量检验,纯度达99%以上; √ 2. The products shall be packed in special standard barrels or according to the requirements of customers.

Desglymidodrine

Cas:3600-87-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:Active Pharmaceutical I

2-amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Midodrine Related Compound A (40 mg) (2-amino-1-(2,5-dimethoxyphenyl)ethanol)

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

2,5-Dimethoxyphenyl-2-hydroxyethylamine

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

2,5-Dimethoxyphenyl-2-hydroxyethylamine

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

DB BIOTECH CO., LTD

best seller Application:API

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Applicatio

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

2-Amino-1-(2,5-dimethoxyphenyl)ethanol cas 3600-87-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2-Amino-1-(2,5-dimethoxyphenyl)ethanol cas 3600-87-1

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

3600-87-1

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

2-Amino-(2,5-dimethoxyphenyl)ethanol (for Midodrin use)

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Falcon Life Sciences Pvt. Ltd

Pharma Grade Application:Pharmaceutical Intermediate

2-Amino-1-(2,5-dimethoxyphenyl)ethanol

Cas:3600-87-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

1-(2,5-dimethoxyphenyl)-2-nitroethanol
14438-63-2

1-(2,5-dimethoxyphenyl)-2-nitroethanol

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol at -10℃; for 2h; Solvent; Reagent/catalyst;83%
2-(2,5-dimethoxyphenyl)-2-trimethylsilyloxyacetonitrile
141367-35-3

2-(2,5-dimethoxyphenyl)-2-trimethylsilyloxyacetonitrile

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether for 1h; Heating;54%
1,2-epoxy-1-(2,5-dimethoxyphenyl)ethane
83436-65-1, 141303-39-1

1,2-epoxy-1-(2,5-dimethoxyphenyl)ethane

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With ammonia In ethanol for 120h; Ambient temperature;
2-amino-1-<2.5-dimethoxy-phenyl>-ethanone-(1)-hydrochloride

2-amino-1-<2.5-dimethoxy-phenyl>-ethanone-(1)-hydrochloride

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With ethanol; platinum Hydrogenation;
With water; platinum Hydrogenation;
5-<2.5-dimethoxy-phenyl>-oxazolidinone-(2)

5-<2.5-dimethoxy-phenyl>-oxazolidinone-(2)

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With hydrogenchloride
2-amino-1-(2,5-dimethoxyphenyl)ethanone hydrochloride

2-amino-1-(2,5-dimethoxyphenyl)ethanone hydrochloride

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With sodium tetrahydroborate In methanol at 0℃; for 0.5h;
2-bromo-2',5'-dimethoxyacetophenone
1204-21-3

2-bromo-2',5'-dimethoxyacetophenone

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaBH4 / dioxane; H2O / 1 h / Ambient temperature
2: KOH / diethyl ether; H2O / 0.5 h / Heating
3: NH3 / ethanol / 120 h / Ambient temperature
View Scheme
2-Bromo-1-(2,5-dimethoxy-phenyl)-ethanol

2-Bromo-1-(2,5-dimethoxy-phenyl)-ethanol

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / diethyl ether; H2O / 0.5 h / Heating
2: NH3 / ethanol / 120 h / Ambient temperature
View Scheme
2,5-dimethoxybenzaldehyde
93-02-7

2,5-dimethoxybenzaldehyde

alkaline permanganate

alkaline permanganate

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 percent / zinc iodide / 1 h / Ambient temperature
2: 54 percent / lithium aluminum hydride / diethyl ether / 1 h / Heating
View Scheme
2-(2,5-dimethoxyphenyl)-2-hydroxyacetonitrile
56979-58-9

2-(2,5-dimethoxyphenyl)-2-hydroxyacetonitrile

desglymidodrine
3600-87-1

desglymidodrine

Conditions
ConditionsYield
With hydrogenchloride; borane In tetrahydrofuran1.5 g (52%)
BOC-glycine
4530-20-5

BOC-glycine

desglymidodrine
3600-87-1

desglymidodrine

midodrine hydrochloride

midodrine hydrochloride

Conditions
ConditionsYield
Stage #1: BOC-glycine With 1,1'-carbonyldiimidazole In ethyl acetate for 1h;
Stage #2: desglymidodrine In ethyl acetate at 20℃; for 1h;
Stage #3: With hydrogenchloride In water; ethyl acetate at 20℃; for 4.25h;
87%
desglymidodrine
3600-87-1

desglymidodrine

2-{[(tert-butoxy)carbonyl]amino}acetate ester

2-{[(tert-butoxy)carbonyl]amino}acetate ester

N-(2-(2,5-Dimethoxyphenyl)-2-hydroxyethyl)-2-((1,1-dimethylethoxy)carbonylamino)essigsaeureamid
176851-43-7

N-(2-(2,5-Dimethoxyphenyl)-2-hydroxyethyl)-2-((1,1-dimethylethoxy)carbonylamino)essigsaeureamid

Conditions
ConditionsYield
With 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine In acetonitrile at 40℃; for 15h; Schlenk technique; Inert atmosphere;75%
N-(tert-butoxycarbonyl)glycine methyl ester
31954-27-5

N-(tert-butoxycarbonyl)glycine methyl ester

desglymidodrine
3600-87-1

desglymidodrine

N-(2-(2,5-Dimethoxyphenyl)-2-hydroxyethyl)-2-((1,1-dimethylethoxy)carbonylamino)essigsaeureamid
176851-43-7

N-(2-(2,5-Dimethoxyphenyl)-2-hydroxyethyl)-2-((1,1-dimethylethoxy)carbonylamino)essigsaeureamid

Conditions
ConditionsYield
With 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine In acetonitrile at 40℃; for 15h; Temperature; Schlenk technique; Inert atmosphere;70%
desglymidodrine
3600-87-1

desglymidodrine

chloroacetyl chloride
79-04-9

chloroacetyl chloride

2-chloro-N-[2-(2,5-dimethoxyphenyl)-2-hydroxyethyl]acetamide
60681-99-4

2-chloro-N-[2-(2,5-dimethoxyphenyl)-2-hydroxyethyl]acetamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane; water for 4h; Ambient temperature;50%
desglymidodrine
3600-87-1

desglymidodrine

phenyl chloroformate
1885-14-9

phenyl chloroformate

5-(2,5-dimethoxyphenyl)oxazolidin-2-one
141367-36-4

5-(2,5-dimethoxyphenyl)oxazolidin-2-one

Conditions
ConditionsYield
With pyridine; sodium hydride 1.) RT, 3 h, 2.) THF, RT, 12 h; Yield given. Multistep reaction;
desglymidodrine
3600-87-1

desglymidodrine

trifluoroacetic anhydride
407-25-0

trifluoroacetic anhydride

A

(R)-N-[2-(2,5-dimethoxyphenyl)-2-hydroxyethyl]-2,2,2-trifluoroacetamide

(R)-N-[2-(2,5-dimethoxyphenyl)-2-hydroxyethyl]-2,2,2-trifluoroacetamide

B

(S)-N-[2-(2,5-dimethoxyphenyl)-2-hydroxyethyl]-2,2,2-trifluoroacetamide

(S)-N-[2-(2,5-dimethoxyphenyl)-2-hydroxyethyl]-2,2,2-trifluoroacetamide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.166667h;
desglymidodrine
3600-87-1

desglymidodrine

6-(2,5-Dimethoxy-phenyl)-morpholin-3-one
83436-68-4

6-(2,5-Dimethoxy-phenyl)-morpholin-3-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 50 percent / NaOH / CH2Cl2; H2O / 4 h / Ambient temperature
2: KOH / ethanol / 24 h / Ambient temperature
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

2-(2,5-dimethoxyphenyl)morpholine
83436-71-9

2-(2,5-dimethoxyphenyl)morpholine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 50 percent / NaOH / CH2Cl2; H2O / 4 h / Ambient temperature
2: KOH / ethanol / 24 h / Ambient temperature
3: 70 percent / LiAlH4 / diethyl ether / 8 h / Heating
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

C12H15(2)H2NO3
83436-76-4

C12H15(2)H2NO3

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 50 percent / NaOH / CH2Cl2; H2O / 4 h / Ambient temperature
2: KOH / ethanol / 24 h / Ambient temperature
3: 65 percent / LiAlD4 / diethyl ether / 8 h / Heating
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

5,5'-bis(2,5-dimethoxyphenyl)-3,3'-tetramethylenedi(oxazolidin-2-one)
141367-38-6

5,5'-bis(2,5-dimethoxyphenyl)-3,3'-tetramethylenedi(oxazolidin-2-one)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) pyridine, 2.) sodium hydride / 1.) RT, 3 h, 2.) THF, RT, 12 h
2: 77 percent / butyl lithium / hexane; hexamethylphosphoric acid triamide; tetrahydrofuran / 3 h / Heating
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

5,5'-bis(2,5-dimethoxyphenyl)-3,3'-hexamethylenedi(oxazolidin-2-one)
141367-37-5

5,5'-bis(2,5-dimethoxyphenyl)-3,3'-hexamethylenedi(oxazolidin-2-one)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) pyridine, 2.) sodium hydride / 1.) RT, 3 h, 2.) THF, RT, 12 h
2: 80 percent / butyl lithium / hexane; hexamethylphosphoric acid triamide; tetrahydrofuran / 3 h / Heating
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

N,N'-bis<2-hydroxy-2-(2,5-dimethoxyphenyl)ethyl>-tetramethylenediamine
141367-31-9

N,N'-bis<2-hydroxy-2-(2,5-dimethoxyphenyl)ethyl>-tetramethylenediamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) pyridine, 2.) sodium hydride / 1.) RT, 3 h, 2.) THF, RT, 12 h
2: 77 percent / butyl lithium / hexane; hexamethylphosphoric acid triamide; tetrahydrofuran / 3 h / Heating
3: 85percent potassium hydroxide, H2O / ethanol / 12 h / Heating
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

N,N'-bis<2-hydroxy-2-(2,5-dimethoxyphenyl)ethyl>-hexamethylenediamine
141381-40-0

N,N'-bis<2-hydroxy-2-(2,5-dimethoxyphenyl)ethyl>-hexamethylenediamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) pyridine, 2.) sodium hydride / 1.) RT, 3 h, 2.) THF, RT, 12 h
2: 80 percent / butyl lithium / hexane; hexamethylphosphoric acid triamide; tetrahydrofuran / 3 h / Heating
3: 85percent potassium hydroxide, H2O / ethanol / 12 h / Heating
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

1-methyl-4-oxo-4,5,6,7-tetrahydro-1H-indazole
85302-16-5

1-methyl-4-oxo-4,5,6,7-tetrahydro-1H-indazole

1-(2,5-dimethoxyphenyl)-2-(1-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ylamino)ethanol

1-(2,5-dimethoxyphenyl)-2-(1-methyl-4,5,6,7-tetrahydro-1H-indazol-4-ylamino)ethanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: titanium(IV) isopropylate; N-trimethylsilyl-pyrrolidin-2-one / 6 h / 70 °C / Sealed tube
2: N-trimethylsilyl-pyrrolidin-2-one; sodium tetrahydroborate / ethanol / 20 °C
View Scheme
desglymidodrine
3600-87-1

desglymidodrine

1-methyl-4-oxo-4,5,6,7-tetrahydro-1H-indazole
85302-16-5

1-methyl-4-oxo-4,5,6,7-tetrahydro-1H-indazole

C18H23N3O3

C18H23N3O3

Conditions
ConditionsYield
With titanium(IV) isopropylate; N-trimethylsilyl-pyrrolidin-2-one at 70℃; for 6h; Sealed tube;

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