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Cas:3623-15-2
Min.Order:1 Kilogram
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inquiryProduct Name: 1-Phenyl-2-propyn-1-one Synonyms: 3-oxo-3-phenylpropyne;1-PHENYLPROP-2-YN-1-ONE;1-Phenyl-2-propyn-1-one;1-Oxo-2-propynylbenzene;Benzoylacetylene;Propinoylbenzene;Propiolophenone;2-PROPYN-1-ONE,1-PHENYL CAS: 3623-15-
Cas:3623-15-2
Min.Order:1 Kilogram
FOB Price: $8900.0
Type:Lab/Research institutions
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Cas:3623-15-2
Min.Order:1 Kilogram
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:3623-15-2
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Superior quality moderate price & quick delivery Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make other chemic
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:3623-15-2
Min.Order:1 bottle
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Type:Lab/Research institutions
inquiry1-Phenyl-2-propyn-1-oneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals a
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a
1-Phenyl-2-propyn-1-one cas 3623-15-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:3623-15-2
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryChangzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and
Cas:3623-15-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryhigh purity Application:Drug intermediates Materials intermediates and active molecules
Conditions | Yield |
---|---|
With Jones reagent In acetone at 0℃; Jones Oxidation; Inert atmosphere; | 100% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 20℃; for 5h; | 99% |
With sodium hypochlorite pentahydrate; 4-acetamido-2,2,6,6-tetramethylpiperidine-N-hydroxyammonium tetrafluoroborate In water; acetonitrile at 20℃; for 0.75h; | 99% |
(E)-1-methoxy-4-(4-phenylbut-1-en-3-yn-1-yl)benzene
A
4-methoxy-benzaldehyde
B
phenyl propargyl ketone
Conditions | Yield |
---|---|
With oxygen; 5,15,10,20-tetraphenylporphyrin In chloroform Irradiation; | A 83% B 85% |
(E)-1,4-Diphenylbut-1-en-3-yne
A
benzaldehyde
B
phenyl propargyl ketone
Conditions | Yield |
---|---|
With oxygen; 5,15,10,20-tetraphenylporphyrin In chloroform for 75h; Irradiation; | A 80% B 84% |
propargyl benzene
phenyl propargyl ketone
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; [copper(II)(salqu)] In acetonitrile at 70℃; for 4h; | 77% |
With tetrachloromethane; di-tert-butyl chromate; acetic acid Reagens 4: Acetanhydrid; | |
With selenium(IV) oxide; ethanol |
bis(p-chlorophenyl) diselenide
1-Phenyl-2-propyn-1-ol
A
(Z)-2-(4-Chloro-phenylselanyl)-3-phenyl-propenal
B
phenyl propargyl ketone
Conditions | Yield |
---|---|
With sulfuric acid; tetraethylammonium perchlorate In water; acetonitrile at 65℃; for 14h; electrochemical oxidation; | A 74% B 12% |
1,1-dichloro-3-ethoxy-3-phenylpropene
A
1-phenyl-propynone-diethylacetal
B
(Z)-β-chloro-1-phenyl propenone
C
phenyl propargyl ketone
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 80℃; for 18h; | A 72% B n/a C 18% D 9% |
Conditions | Yield |
---|---|
Stage #1: benzaldehyde; acetylenemagnesium bromide In tetrahydrofuran at -78 - 20℃; for 1h; Inert atmosphere; Stage #2: With chromium(VI) oxide; sulfuric acid In acetone at 0℃; for 3h; Inert atmosphere; | 69% |
Stage #1: benzaldehyde; acetylenemagnesium bromide Inert atmosphere; Stage #2: With Jones reagent Inert atmosphere; |
ethanol
1,1,1,3-tetrachloro-3-phenylpropane
A
1,1-dichloro-3-ethoxy-3-phenylpropene
B
1-phenyl-propynone-diethylacetal
C
(Z)-β-chloro-1-phenyl propenone
D
phenyl propargyl ketone
Conditions | Yield |
---|---|
With sodium ethanolate for 18h; Heating; Further byproducts given; | A 22% B 2% C 2% D 59% |
1-phenyl-2-(1H-tetrazol-5-yl)ethanone
phenyl propargyl ketone
Conditions | Yield |
---|---|
With lead(IV) acetate In 1,4-dioxane at 0℃; for 0.5h; | 53% |
benzaldehyde
trimethylsilylacetylene
A
3-(trimethylsilyl)-1-phenyl-2-propyn-1-one
B
phenyl propargyl ketone
Conditions | Yield |
---|---|
Stage #1: trimethylsilylacetylene With indium(III) bromide; triethylamine In diethyl ether at 20℃; for 1h; Inert atmosphere; Sealed tube; Stage #2: benzaldehyde In diethyl ether at 40℃; for 24h; Inert atmosphere; Sealed tube; | A 40% B 10% |
ethanol
1,1,1,3-tetrachloro-3-phenylpropane
A
ethyl 3-phenyl-2-propenoate
B
1-phenyl-propynone-diethylacetal
C
(Z)-β-chloro-1-phenyl propenone
D
phenyl propargyl ketone
Conditions | Yield |
---|---|
With potassium hydroxide for 18h; Heating; Further byproducts given; | A 2% B 33% C 5% D 14% |
ethanol
1,1,1,3-tetrachloro-3-phenylpropane
A
3-Oxo-3-phenylpropanal 1-(diethylacetal)
B
1-phenyl-propynone-diethylacetal
C
(Z)-β-chloro-1-phenyl propenone
D
phenyl propargyl ketone
Conditions | Yield |
---|---|
With potassium hydroxide for 18h; Heating; Further byproducts given; | A 2% B 33% C 5% D 14% |
ethanol
1,1,1,3-tetrachloro-3-phenylpropane
A
phenylpropargyl aldehyde diethyl acetal
B
1-phenyl-propynone-diethylacetal
C
(Z)-β-chloro-1-phenyl propenone
D
phenyl propargyl ketone
Conditions | Yield |
---|---|
With potassium hydroxide for 18h; Heating; Further byproducts given; | A 8% B 33% C 5% D 14% |
ethanol
1,1,1,3-tetrachloro-3-phenylpropane
A
3-ethoxy-3-phenyl-2-propenal
B
1-phenyl-propynone-diethylacetal
C
(Z)-β-chloro-1-phenyl propenone
D
phenyl propargyl ketone
Conditions | Yield |
---|---|
With potassium hydroxide for 18h; Heating; Further byproducts given; | A 2% B 33% C 5% D 14% |
ethanol
1,1,1,3-tetrachloro-3-phenylpropane
A
1-phenyl-propynone-diethylacetal
B
(Z)-β-chloro-1-phenyl propenone
C
phenyl propargyl ketone
Conditions | Yield |
---|---|
With potassium hydroxide for 18h; Heating; Further byproducts given; | A 33% B 5% C 14% D 3% |
1,1,1,3-tetrachloro-3-phenylpropane
A
1-phenyl-propynone-diethylacetal
B
(Z)-β-chloro-1-phenyl propenone
C
phenyl propargyl ketone
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 18h; Heating; Further byproducts given; | A 33% B 5% C 14% D 3% |
1-Phenyl-2-propyn-1-ol
A
3-phenyl-3-keto-propanol-di(1-phenyl-2-propyn-1-yl) acetal
B
phenyl propargyl ketone
Conditions | Yield |
---|---|
at 5℃; electrolysis: nickel net anode, cylindrical stainless steel cathode; electrolyte: 0.1M KOH/t-butanol - water (1:1); | A 28% B 4% |
at 5℃; electrolysis: nickel net anode, cylindrical stainless steel cathode; electrolyte: KOH/t-butanol - water (1:1); | A 28% B 4% |
tetrachloromethane
propargyl benzene
di-tert-butyl chromate
acetic anhydride
acetic acid
phenyl propargyl ketone
3-(trimethylsilyl)-1-phenyl-2-propyn-1-one
phenyl propargyl ketone
Conditions | Yield |
---|---|
With borax | |
With borax In methanol | |
Multi-step reaction with 2 steps 1: potassium carbonate / methanol / 2 h 2: chromium(VI) oxide; sulfuric acid / acetone; water / 0.33 h / 0 °C View Scheme |
ethyl [2]alcohol
1,1-dichloro-3-ethoxy-3-phenylpropene
A
1-phenyl-propynone-diethylacetal
B
1-phenyl-3-deuterioprop-2-yn-1-one
C
phenyl propargyl ketone
Conditions | Yield |
---|---|
With sodium ethanolate for 8h; Mechanism; Heating; |
C9H5(3)HO
phenyl propargyl ketone
Conditions | Yield |
---|---|
With water; hydrogenphosphate In tetrahydrofuran at 25℃; Rate constant; |
phenyl propargyl ketone
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; hexane Ambient temperature; Yield given; |
3,5,6,6-tetramethyl-3-(1-phenyl-3-methylsilanyl-1-trimethylsilanyloxyprop-2-ynyl)-3,6-dihydro[1,4]oxazin-2-one
A
phenyl propargyl ketone
B
3,5,6,6-tetramethyl-3,6-dihydro-[1,4]oxazin-2-one
Conditions | Yield |
---|---|
With water; pyridinium p-toluenesulfonate Hydrolysis; |
selenium(IV) oxide
ethanol
propargyl benzene
phenyl propargyl ketone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrahydrofuran / 0 - 20 °C 2: IBX / ethyl acetate; tetrahydrofuran / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: tetrahydrofuran / 0 - 20 °C 2: IBX / ethyl acetate / 80 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / 0 °C 2: MnO2 / CH2Cl2 / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 72 percent / NaH / tetrahydrofuran / Heating 2: 86 percent / NaN3; AlCl3 / tetrahydrofuran / 5 h / Heating 3: 53 percent / Pb(OAc)4 / dioxane / 0.5 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 86 percent / NaN3; AlCl3 / tetrahydrofuran / 5 h / Heating 2: 53 percent / Pb(OAc)4 / dioxane / 0.5 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C 2: 3N HCl / tetrahydrofuran; hexane / Ambient temperature View Scheme |
((S)-1-carbamimidoyl-2-phenyl-ethyl)-carbamic acid tert-butyl ester
phenyl propargyl ketone
[(S)-2-phenyl-1-(4-phenyl-pyrimidin-2-yl)-ethyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile at 120℃; for 0.666667h; Microwave irradiation; | 100% |
Conditions | Yield |
---|---|
In methanol at 65℃; | 100% |
phenyl propargyl ketone
Conditions | Yield |
---|---|
With copper In dichloromethane at 20℃; stereoselective reaction; | 100% |
Conditions | Yield |
---|---|
With N-benzyl-trimethylammonium hydroxide In tetrahydrofuran; water at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In tetrahydrofuran at 80℃; Inert atmosphere; | 80% |
phenylmethanethiol
phenyl propargyl ketone
3,3-bis(benzylmercapto)propiophenone
Conditions | Yield |
---|---|
With tributylphosphine In tetrahydrofuran | 99% |
With 1-butyl-3-methylimidazolium hydroxide; 1-n-butyl-3-methylimidazolim bromide for 0.333333h; | 95% |
benzamidine monohydrochloride
phenyl propargyl ketone
2,4-diphenylpyrimidine
Conditions | Yield |
---|---|
With sodium carbonate In acetonitrile at 120℃; for 0.666667h; microwave irradiation; | 99% |
With sodium carbonate In acetonitrile at 120℃; for 0.666667h; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With hexafluorophosphoric acid In acetic acid at 20℃; for 48h; | 99% |
With hexafluorophosphoric acid In acetic acid at 20℃; | 99% |
Conditions | Yield |
---|---|
With triphenylphosphine In toluene at 20℃; Inert atmosphere; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With triphenylphosphine In acetonitrile at 20℃; Inert atmosphere; regioselective reaction; | 99% |
2-benzoyl-3-(2-furyl)prop-2-enenitrile
phenyl propargyl ketone
C23H15NO3
Conditions | Yield |
---|---|
With triphenylphosphine In toluene at 20℃; Inert atmosphere; regioselective reaction; | 99% |
phenyl propargyl ketone
C25H16BrNO2
Conditions | Yield |
---|---|
With triphenylphosphine In toluene at 20℃; Inert atmosphere; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With C35H52N4O4; scandium tris(trifluoromethanesulfonate) In tetrahydrofuran; dichloromethane at 30℃; for 5h; Michael Addition; Molecular sieve; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With C35H52N4O4; scandium tris(trifluoromethanesulfonate) In tetrahydrofuran; dichloromethane at 30℃; for 3h; Michael Addition; Molecular sieve; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With C35H52N4O4; scandium tris(trifluoromethanesulfonate) In tetrahydrofuran; dichloromethane at 30℃; for 5h; Michael Addition; Molecular sieve; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With C35H52N4O4; scandium tris(trifluoromethanesulfonate) In tetrahydrofuran; dichloromethane at 30℃; for 5h; Michael Addition; Molecular sieve; enantioselective reaction; | 99% |
aminomalonic acid diethyl ester
1-benzyl-7-fluoroindoline-2,3-dione
phenyl propargyl ketone
Conditions | Yield |
---|---|
With (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In toluene at 25℃; for 36h; Molecular sieve; enantioselective reaction; | 99% |
N-hydroxyphthalimide
phenyl propargyl ketone
3-benzoyl-3a-hydroxy-3aH-1-oxa-8a-azacyclopenta[a]indene-8-one
Conditions | Yield |
---|---|
With triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; | 99% |
With triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 1h; | 99% |
phenyl propargyl ketone
diethyl 4-benzoyl-5-(3,4-dichlorophenyl)-1H-pyrrole-2,2(5H)-dicarboxylate
Conditions | Yield |
---|---|
With (S,Sp)-R-Phosferrox; copper(II) acetate monohydrate; triethylamine In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Molecular sieve; enantioselective reaction; | 99% |
phenyl propargyl ketone
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 72h; Inert atmosphere; Darkness; enantioselective reaction; | 99% |
phenyl propargyl ketone
Conditions | Yield |
---|---|
In acetonitrile at 60℃; for 48h; Inert atmosphere; Darkness; enantioselective reaction; | 99% |
phenyl propargyl ketone
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 72h; Inert atmosphere; Darkness; enantioselective reaction; | 99% |
thiophenol
phenyl propargyl ketone
1-phenyl-3,3-bis(phenylthio)propan-1-one
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium hydroxide; 1-n-butyl-3-methylimidazolim bromide for 0.25h; | 98% |
With lithium tert-butoxide In ethanol at 20℃; for 0.166667h; | 88% |
With sodium acetate In tetrahydrofuran; water at 70℃; for 2.5h; | 80% |
With N-benzyl-trimethylammonium hydroxide In methanol |
phenyl propargyl ketone
3-phenyl-4-amino-5-mercapto-1,2,4-triazole
4-amino-3-(benzoylvinylthio)-5-phenyl-1,2,4-triazole
Conditions | Yield |
---|---|
In methanol at 20℃; for 3h; | 98% |
In methanol at 65℃; for 5h; | 84% |
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium hydroxide; 1-n-butyl-3-methylimidazolim bromide for 0.333333h; | 98% |
In ammonia for 1h; | 96% |
With sodium acetate In tetrahydrofuran; water at 70℃; for 3h; | 75% |
phenyl propargyl ketone
1,3,5-tribenzoylbenzene
Conditions | Yield |
---|---|
dmap; acetylacetone In dichloromethane at 20℃; for 2h; | 98% |
With t-butyl azide In 1,4-dioxane at 100℃; for 30h; | 64.3% |
In N,N-dimethyl-formamide for 3h; Heating; | 57% |
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl acetamide at 55℃; for 0.666667h; microwave irradiation; | 98% |
With sodium azide In N,N-dimethyl acetamide at 100℃; for 2h; Cycloaddition; | 95% |
With sodium azide In N,N-dimethyl acetamide at 20 - 100℃; for 14h; Cycloaddition; | 95% |
ethyl 3-aminobut-2-enoate
phenyl propargyl ketone
ethyl 2-methyl-6-phenylnicotinate
Conditions | Yield |
---|---|
In acetic acid; toluene at 170℃; for 0.166667h; Product distribution; Further Variations:; Solvents; microwave irradiation; Bohlmann-Rahtz synthesis; | 98% |
Conditions | Yield |
---|---|
With ammonium acetate In ethanol for 24h; Bohlmann-Rahtz reaction; Heating; | 98% |
With ammonium acetate In ethanol for 24h; Heating; | 98% |
ethane-1,2-dithiol
phenyl propargyl ketone
2-(1,3-dithiolan-2-yl)-1-phenylethan-1-one
Conditions | Yield |
---|---|
With 1-butyl-3-methylimidazolium hydroxide; 1-n-butyl-3-methylimidazolim bromide for 0.25h; | 98% |
With sodium acetate In tetrahydrofuran; water at 70℃; for 3.5h; | 74% |
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