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Henan Kanbei Chemical Co.,LTD

1. Well-equipped, stable and high-quality raw material supply chain, to provide customers with the best quality products. 2.Strict quality inspection process and professional certificate testing to ensure the quality level of the final product. 3.E

99% Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Diethylaminosulfur trifluoride Manufacturer/High quality/Best price/In stock

Cas:38078-09-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Acceptance criteria Result Appearance Light yellow liquid Light yellow liquid Boiling point

Top purity Diethylaminosulfur trifluoride with high quality and best price cas:38078-09-0

Cas:38078-09-0

Min.Order:1 Gram

FOB Price: $2.0 / 5.0

Type:Manufacturers

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Diethylaminosulfur Trifluoride with high purity

Cas:38078-09-0

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

High quality Diethylaminosulfur trifluoride CAS 38078-09-0 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, F

High quality Diethylaminosulfur trifluoride CAS 38078-09-0 with factory price

Cas:38078-09-0

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

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Jinan Finer Chemical Co., Ltd

Product description: Product name Diethylaminosulfur trifluoride CAS number 38078-09-0 Assay ≥99% Appearance Yellowish liquid Capacity 200mt/year Application Fluorinated reag

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

Diethylaminosulfur trifluoride, 95%

Cas:38078-09-0

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Diethylaminosulfur Trifluoride

Cas:38078-09-0

Min.Order:1

Negotiable

Type:Other

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Tengzhou Runlong Fragrance Co., Ltd.

1、Our factory passed ISO 9001, ISO 14001, ISO 22000 system certification; HALAL 、KOSHER、FCC AND FDA certificate are available. We can provide customers with better prices, and the supply is stable. 2、We founded in 2004,10% of the staff have more tha

CAS 38078-09-0 DAST / Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company

TIANFU-CHEM -Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Dast Diethylaminosulfur Trifluoride CAS: 38078-09-0

Cas:38078-09-0

Min.Order:1 Kilogram

FOB Price: $32.0 / 65.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Standard CAS 38078-09-0 with competitive price

Cas:38078-09-0

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Diethylaminosulfur trifluoride 38078-09-0

Cas:38078-09-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:1 Kilogram

FOB Price: $89.0 / 100.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply High quality Diethylaminosulfur trifluoride CAS 38078-09-0 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2

High quality Diethylaminosulfur trifluoride CAS 38078-09-0

Cas:38078-09-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:38078-09-0

Cas:38078-09-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Diethylaminosulfur trifluoride;DAST CAS:38078-09-0, Please contact us by email freely. We are leading exporter in China. If you rea

Diethylaminosulfur trifluoride;DAST CAS:38078-09-0 from fandachem

Cas:38078-09-0

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Sulfur diethylamine trifluoride

Cas:38078-09-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

DAST

Cas:38078-09-0

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

DIETHYLAMINOSULFUR TRIFLUORIDE

Cas:38078-09-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Lingrui Chemical Co.,Ltd.

High quality 38078-09-0 Diethylaminosulfur trifluoride factory in China Diethylamino sulfur trifluoride, commonly used abbreviation DAST, is a fluorination reagent widely used in organic synthesis. It is (dihydrocarbyl amino) A member of the sulfur

High quality 38078-09-0 Diethylaminosulfur trifluoride factory in China

Cas:38078-09-0

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:100 Gram

Negotiable

Type:Other

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Diethylaminosulfur trifluoride

Cas:38078-09-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Synthetic route

N,N-diethyl-1,1,1-trimethylsilanamine
996-50-9

N,N-diethyl-1,1,1-trimethylsilanamine

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

Conditions
ConditionsYield
With sulfur tetrafluoride
With sulfur tetrafluoride In trichlorofluoromethane at -78 - -60℃;
With sulfur tetrafluoride In diethyl ether
C9H13F10NOS
80027-80-1

C9H13F10NOS

A

diethylamidosulfurous fluoride
1550-61-4

diethylamidosulfurous fluoride

B

1,1,2,2,3,3,4,4,5-nonafluoropentane
678-73-9

1,1,2,2,3,3,4,4,5-nonafluoropentane

C

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

D

2,2,3,3,4,4,5,5-octafluoropentyl diethylamidosulfite
80032-41-3

2,2,3,3,4,4,5,5-octafluoropentyl diethylamidosulfite

E

bis(2,2,3,3,4,4,5,5-octafluoropentyloxy)diethylaminofluorosulfurane
80027-87-8

bis(2,2,3,3,4,4,5,5-octafluoropentyloxy)diethylaminofluorosulfurane

Conditions
ConditionsYield
under 0.05 - 0.08 Torr; Product distribution; the bath temperature gradually raised to 90 deg C;A 1.12 g
B 2.88 g
C 1.6 g
D 1.5 g
E 3.05 g
C9H13F10NOS
80027-80-1

C9H13F10NOS

A

1,1,2,2,3,3,4,4,5-nonafluoropentane
678-73-9

1,1,2,2,3,3,4,4,5-nonafluoropentane

B

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

C

2,2,3,3,4,4,5,5-octafluoropentyl diethylamidosulfite
80032-41-3

2,2,3,3,4,4,5,5-octafluoropentyl diethylamidosulfite

D

bis(2,2,3,3,4,4,5,5-octafluoropentyloxy)diethylaminofluorosulfurane
80027-87-8

bis(2,2,3,3,4,4,5,5-octafluoropentyloxy)diethylaminofluorosulfurane

Conditions
ConditionsYield
under 0.05 - 0.08 Torr; the bath temperature gradually raised to 90 deg C; Further byproducts given;A 2.88 g
B 1.6 g
C 1.5 g
D 3.05 g
C11H13F14NOS
80027-81-2

C11H13F14NOS

A

diethylamidosulfurous fluoride
1550-61-4

diethylamidosulfurous fluoride

B

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

C

1,1,2,2,3,3,4,4,5,5,6,6,7-tridecafluoroheptane
2708-11-4

1,1,2,2,3,3,4,4,5,5,6,6,7-tridecafluoroheptane

D

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite
80032-43-5

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

E

bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane
80027-88-9

bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane

Conditions
ConditionsYield
under 0.05 - 0.08 Torr; Product distribution; the bath temperature gradually raised to 90 deg C;A 0.5 g
B 3 g
C 4.45 g
D 4.2 g
E 4.8 g
C11H13F14NOS
80027-81-2

C11H13F14NOS

A

diethylamidosulfurous fluoride
1550-61-4

diethylamidosulfurous fluoride

B

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

C

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite
80032-43-5

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

D

bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane
80027-88-9

bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane

Conditions
ConditionsYield
under 0.05 - 0.08 Torr; the bath temperature gradually raised to 90 deg C; Further byproducts given;A 0.5 g
B 3 g
C 4.2 g
D 4.8 g
C11H13F14NOS
80027-81-2

C11H13F14NOS

A

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

B

1,1,2,2,3,3,4,4,5,5,6,6,7-tridecafluoroheptane
2708-11-4

1,1,2,2,3,3,4,4,5,5,6,6,7-tridecafluoroheptane

C

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite
80032-43-5

2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyl diethylamidosulfite

D

bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane
80027-88-9

bis(2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)diethylaminofluorosulfurane

Conditions
ConditionsYield
under 0.05 - 0.08 Torr; the bath temperature gradually raised to 90 deg C; Further byproducts given;A 3 g
B 4.45 g
C 4.2 g
D 4.8 g
triethylamine tris(hydrogen fluoride)
73602-61-6

triethylamine tris(hydrogen fluoride)

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

A

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

B

C6H15N*2FH*H(1+)*BF4(1-)

C6H15N*2FH*H(1+)*BF4(1-)

Conditions
ConditionsYield
In [D3]acetonitrile at 20℃; for 0.166667h; Inert atmosphere; Molecular sieve;
ethyl 5-bromo-6-formyl-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylate

ethyl 5-bromo-6-formyl-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylate

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

ethyl 5-bromo-6-(difluoromethyl)-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylate

ethyl 5-bromo-6-(difluoromethyl)-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylate

Conditions
ConditionsYield
In dichloromethane100%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

trimethyl-(1H,1H,7H-dodecafluoroheptyloxy)silane
56002-71-2

trimethyl-(1H,1H,7H-dodecafluoroheptyloxy)silane

C11H13F14NOS
80027-81-2

C11H13F14NOS

Conditions
ConditionsYield
In diethyl ether 1.) 0 deg C - 5 deg C, 10 min; 2.) 20 deg C, 30 min.;99%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

trimethyl-(1H,1H,5H-octafluoropentyloxy)silane
56002-63-2

trimethyl-(1H,1H,5H-octafluoropentyloxy)silane

C9H13F10NOS
80027-80-1

C9H13F10NOS

Conditions
ConditionsYield
In diethyl ether 1.) 0 deg C - 5 deg C, 10 min; 2.) 20 deg C, 30 min.;99%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

4-fluoro-7-methylsulfinyl-indan-1-one

4-fluoro-7-methylsulfinyl-indan-1-one

4-fluoro-7-(fluoromethylsulfanyl)indan-1-one

4-fluoro-7-(fluoromethylsulfanyl)indan-1-one

Conditions
ConditionsYield
With antimony(III) chloride In dichloromethane at 20℃; for 3h; Cooling with ice;99%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

(S)-tert-butyl 3-((4-(2-((5-((2-(hydroxymethyl)phenyl)methylsulfonamido)-2-methylnaphthalen-1-yl)oxy)pyridin-3-yl)pyrimidin-2-yl)amino)piperidine-1-carboxylate

(S)-tert-butyl 3-((4-(2-((5-((2-(hydroxymethyl)phenyl)methylsulfonamido)-2-methylnaphthalen-1-yl)oxy)pyridin-3-yl)pyrimidin-2-yl)amino)piperidine-1-carboxylate

(S)-tert-butyl 3-((4-(2-((5-((2-(fluoromethyl)phenyl)methylsulfonamido)-2-methylnaphthalen-1-yl)oxy)pyridin-3-yl)pyrimidin-2-yl)amino)piperidine-1-carboxylate

(S)-tert-butyl 3-((4-(2-((5-((2-(fluoromethyl)phenyl)methylsulfonamido)-2-methylnaphthalen-1-yl)oxy)pyridin-3-yl)pyrimidin-2-yl)amino)piperidine-1-carboxylate

Conditions
ConditionsYield
In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran at -78℃; for 0.5h;99%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

ethyl 2-(2-bromophenyl)-2-hydroxyacetate

ethyl 2-(2-bromophenyl)-2-hydroxyacetate

ethyl 2-bromophenyl-fluoroacetate
1214911-36-0

ethyl 2-bromophenyl-fluoroacetate

Conditions
ConditionsYield
In dichloromethane at -78 - 20℃; Inert atmosphere;98%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

Conditions
ConditionsYield
With tetrafluoroboric acid; diethyl ether at 20 - 30℃; Inert atmosphere;96%
With tetrafluoroboric acid diethyl ether In diethyl ether at 20 - 30℃; for 0.833333h; Product distribution / selectivity; Inert atmosphere;96%
With boron trifluoride diethyl etherate In diethyl ether at 5 - 20℃; Inert atmosphere;92%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

5-(2,3-dichloroindol-1-yl)-4-methoxy-1-methyl-6-oxo-pyridazine-3-carbaldehyde

5-(2,3-dichloroindol-1-yl)-4-methoxy-1-methyl-6-oxo-pyridazine-3-carbaldehyde

4-(2,3-dichloroindol-1-yl)-6-(difluoromethyl)-5-methoxy-2-methyl-pyridazin-3-one

4-(2,3-dichloroindol-1-yl)-6-(difluoromethyl)-5-methoxy-2-methyl-pyridazin-3-one

Conditions
ConditionsYield
In dichloromethane96%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

(trifluoromethyl)trimethylsilane
81290-20-2

(trifluoromethyl)trimethylsilane

toluene-4-sulfonamide
70-55-3

toluene-4-sulfonamide

N-[(diethylamino)(trifluoromethyl)-λ4-sulfanylidene]-4-methylbenzenesulfonamide

N-[(diethylamino)(trifluoromethyl)-λ4-sulfanylidene]-4-methylbenzenesulfonamide

Conditions
ConditionsYield
Stage #1: diethylamino-sulfur trifluoride; (trifluoromethyl)trimethylsilane With N-ethyl-N,N-diisopropylamine In dichloromethane at -20℃; for 1h; Inert atmosphere;
Stage #2: toluene-4-sulfonamide In dichloromethane at 0 - 20℃; Inert atmosphere;
95%
Trifluoromethanesulfonamide
421-85-2

Trifluoromethanesulfonamide

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

(trifluoromethyl)trimethylsilane
81290-20-2

(trifluoromethyl)trimethylsilane

N-[(diethylamino)(trifluoromethyl)-λ4-sulfanylidene]-1,1,1-trifluoromethanesulfonamide

N-[(diethylamino)(trifluoromethyl)-λ4-sulfanylidene]-1,1,1-trifluoromethanesulfonamide

Conditions
ConditionsYield
Stage #1: diethylamino-sulfur trifluoride; (trifluoromethyl)trimethylsilane With N-ethyl-N,N-diisopropylamine In dichloromethane at -20℃; for 1h; Inert atmosphere;
Stage #2: Trifluoromethanesulfonamide In dichloromethane at 0 - 20℃; Inert atmosphere;
94%
Mn4O3(O2CCH3)4(C6H5COCHCOC6H5)3

Mn4O3(O2CCH3)4(C6H5COCHCOC6H5)3

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

Mn4O3F(CH3COO)3(C6H5COCHCOC6H5)3

Mn4O3F(CH3COO)3(C6H5COCHCOC6H5)3

Conditions
ConditionsYield
In dichloromethane pptn. (hexanes); elem. anal.;93%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

1-(4-methyl-3-nitro-phenyl)-ethanone
5333-27-7

1-(4-methyl-3-nitro-phenyl)-ethanone

4-(1,1-difluoro)ethyl-2-nitrotoluene

4-(1,1-difluoro)ethyl-2-nitrotoluene

Conditions
ConditionsYield
In dichloromethane at -40 - 60℃; for 24h; Inert atmosphere;93%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

boron trifluoride diethyl etherate
109-63-7

boron trifluoride diethyl etherate

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

ethanaminium,N-(difluoro-λ4-sulfanylidene)-N-ethyl-,tetrafluoroborate

Conditions
ConditionsYield
In diethyl ether at 20 - 30℃; Inert atmosphere; Heating; Reflux;89%
diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

4-Chlorophenylboronic acid
1679-18-1

4-Chlorophenylboronic acid

N-(4-chlorophenylsulfinyl)-N,N-diethylamine
1017238-74-2

N-(4-chlorophenylsulfinyl)-N,N-diethylamine

Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.0833333h; Schlenk technique;88%
3-Oxo-2,3,4,5,6,7-tetrahydrobenzofuran
52762-36-4

3-Oxo-2,3,4,5,6,7-tetrahydrobenzofuran

diethylamino-sulfur trifluoride
38078-09-0

diethylamino-sulfur trifluoride

2-(N,N-Diethyl-aminosulfanyl)-2-fluoro-4,5,6,7-tetrahydro-benzofuran-3-one
144104-37-0

2-(N,N-Diethyl-aminosulfanyl)-2-fluoro-4,5,6,7-tetrahydro-benzofuran-3-one

Conditions
ConditionsYield
87%

Raw Materials

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