2-Thioadenosine CAS No.:43157-50-2 Name: 2-Thioadenosine Synonyms: 2-Mercaptoadenosine Molecular Structure
Cas:43157-50-2
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Cas:43157-50-2
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:43157-50-2
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Cas:43157-50-2
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua
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NewCan Biotech Limited was established in 2021 and is primarily engaged in the research, development, production, and sales of sugars, nucleosides, nucleotides, phosphorylated monomers, as well as next-generation antiviral and antitumor drug intermed
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Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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Good price, high purity, mature production technology, in stock, accept custom synthesis per customer's requirements Storage:in stock Package:As per Customer‘ requirements Application:Pharmaceutical API
Stock products, own laboratoryAppearance:Off-white to light yellow solid powder Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
carbon disulfide
5-amino-1-(β-D-ribofuranosyl)imidazole-4-carboxamidoxime
2-Mercaptoadenosine
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol; dimethyl sulfoxide at 140 - 150℃; for 12h; Solvent; | 80% |
In methanol; water at 120℃; for 5h; Autoclave; | |
With diammonium sulfide In methanol; water at 120℃; for 5h; Inert atmosphere; Sealed tube; | 30.73 g |
carbon disulfide
adenosine 1-oxide
2-Mercaptoadenosine
Conditions | Yield |
---|---|
With sodium hydroxide 1.) reflux, 2.) MeOH, H2O, 120 deg C, 5 h; Multistep reaction; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 45 percent / m-chloroperbenzoic acid / acetic acid / 48 h / Ambient temperature 2: 1.) 5N aq. NaOH / 1.) reflux, 2.) MeOH, H2O, 120 deg C, 5 h View Scheme |
adenosine 1-oxide
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydroxide; water / 0.17 h / 140 °C 2: diammonium sulfide / methanol; water / 5 h / 120 °C / Inert atmosphere; Sealed tube View Scheme | |
Stage #1: adenosine 1-oxide With sodium hydroxide Stage #2: With carbon disulfide In methanol; water at 120℃; | |
Stage #1: adenosine 1-oxide With sodium hydroxide In water for 15h; Reflux; Stage #2: With carbon disulfide In methanol; water at 120℃; for 5h; Autoclave; |
adenosine
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Stage #1: adenosine With dihydrogen peroxide; acetic acid Stage #2: With sodium hydroxide In water Stage #3: With carbon disulfide In methanol; water at 120℃; for 5h; Autoclave; | |
Stage #1: adenosine With dihydrogen peroxide; acetic acid Stage #2: With sodium hydroxide In water Stage #3: With carbon disulfide In methanol; water at 120℃; for 5h; Autoclave; | |
Multi-step reaction with 3 steps 1: acetic acid; dihydrogen peroxide / 20 h / 50 °C 2: sodium hydroxide; water / 0.17 h / 140 °C 3: diammonium sulfide / methanol; water / 5 h / 120 °C / Inert atmosphere; Sealed tube View Scheme | |
Multi-step reaction with 2 steps 1.1: 3-chloro-benzenecarboperoxoic acid / methanol / 38 h 2.1: sodium hydroxide / water / 15 h / Reflux 2.2: 5 h / 120 °C / Autoclave View Scheme |
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium hydroxide In methanol at 20℃; for 1h; deprotonation; Stage #2: 1-bromo-butane In N,N-dimethyl-formamide at 20℃; for 4h; Alkylation; | 92% |
2-Mercaptoadenosine
1,1,1-trifluoro-3-iodopropane
2-[(3,3,3-trifluoropropyl)thio]adenosine
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium dithionite In N,N-dimethyl-formamide for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide In water; N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #3: 1,1,1-trifluoro-3-iodopropane In water; N,N-dimethyl-formamide at 20℃; Cooling with ice; | 92% |
In ethyl acetate at 20℃; | 84% |
With sodium hydroxide In water |
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium dithionite In N,N-dimethyl-formamide for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide In water; N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #3: methyl iodide In water; N,N-dimethyl-formamide at 20℃; Cooling with ice; | 89% |
With sodium hydroxide In methanol at 0℃; for 3h; | |
With sodium hydride In N,N-dimethyl-formamide at 20℃; | |
With sodium hydroxide In methanol; water at 0℃; for 3h; | 2.1 g |
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine In methanol; sodium hydroxide at 20℃; for 1h; Stage #2: 1 ,6-dibromohexane In N,N-dimethyl-formamide at 20℃; for 4h; | 86% |
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium dithionite In N,N-dimethyl-formamide for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide In water; N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #3: ethyl iodide In water; N,N-dimethyl-formamide at 20℃; Cooling with ice; | 81% |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium methylate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: 8-(2-bromoethyl)-4,4-difluoro-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene In N,N-dimethyl-formamide at 20℃; for 16h; | 79% |
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium dithionite In N,N-dimethyl-formamide for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide In water; N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #3: 1-iodo-propane In water; N,N-dimethyl-formamide at 20℃; Cooling with ice; | 78% |
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium dithionite In N,N-dimethyl-formamide for 0.5h; Inert atmosphere; Stage #2: With sodium hydroxide In water; N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #3: amyl iodide In water; N,N-dimethyl-formamide at 20℃; Cooling with ice; | 64% |
Conditions | Yield |
---|---|
With sodium hydroxide for 3h; Ambient temperature; | 55% |
2-Mercaptoadenosine
2,2-dimethylpropyl bromide
Conditions | Yield |
---|---|
Stage #1: 2-Mercaptoadenosine With sodium hydroxide In methanol at 20℃; for 1.5h; Stage #2: 2,2-dimethylpropyl bromide In N,N-dimethyl-formamide at 80℃; for 48h; Further stages.; | 52% |
2-Mercaptoadenosine
1,7-dibromoheptane
2-<(7-bromoheptyl)thio>adenosine
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 3h; Ambient temperature; | 33% |
Conditions | Yield |
---|---|
With triethylamine 1.) DMF, 0.5 h, RT, 2.) DMF, 2.5 h; Multistep reaction; | |
Stage #1: 2-Mercaptoadenosine With sodium hydroxide In ethanol; water for 0.166667h; Stage #2: 1-bromocyclohexane In ethanol; water at 20℃; |
Conditions | Yield |
---|---|
With triethylamine 1.) DMF, 0.5 h, RT, 2.) DMF, 2.5 h; Multistep reaction; | |
Stage #1: 2-Mercaptoadenosine With sodium hydroxide In ethanol; water for 0.166667h; Stage #2: 1-bromo-hexane In ethanol; water at 20℃; |
2-Mercaptoadenosine
7-bromo-heptanonitrile
2-(6-cyanohexylthio)adenosine
Conditions | Yield |
---|---|
With triethylamine 1.) DMF, 0.5 h, RT, 2.) DMF, 2.5 h; Yield given. Multistep reaction; |
2-Mercaptoadenosine
(4-nitrophenyl)ethyl bromide
2-(6-amino-2-(p-nitrophenylethyl)sulfanyl-7H-purin-9-yl)-5-(hydroxymethyl)tetrahydrofuran-3,4-diol
Conditions | Yield |
---|---|
With triethylamine 1.) DMF, 0.5 h, RT, 2.) DMF, 2.5 h; Multistep reaction; |
2-Mercaptoadenosine
1-phenyl-2-bromoethane
2-<(phenylethyl)thio>adenosine
Conditions | Yield |
---|---|
With triethylamine 1.) DMF, 0.5 h, RT, 2.) DMF, 2.5 h; Multistep reaction; | |
Stage #1: 2-Mercaptoadenosine With sodium hydroxide In ethanol; water for 0.166667h; Stage #2: 1-phenyl-2-bromoethane In ethanol; water at 20℃; |
2-Mercaptoadenosine
3-chloro-1,1,1-trifluoropropane
2-[(3,3,3-trifluoropropyl)thio]adenosine
Conditions | Yield |
---|---|
With sodium hydride 1.) DMF, 2.) DMF, 36 h; Yield given; Multistep reaction; |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: methanol; aq. NaOH / 1 h / 20 °C 1.2: 86 percent / dimethylformamide / 4 h / 20 °C 2.1: proton sponge; trimethyl phosphate; phosphorous oxychloride / 2.33 h / 0 °C 2.2: (Bu3NH(1+))2P2O7H2; Bu3N; tetraethylammonium bromide / dimethylformamide / 0.75 h / 20 °C View Scheme |
2-Mercaptoadenosine
C11H14Cl2N5O4PS2
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: aq. NaOH / methanol / 3 h / 0 °C 2.1: proton sponge; pyridine / 0.25 h / 0 °C 2.2: PSCl3 / 0.25 h / 0 °C View Scheme |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: aq. NaOH / methanol / 3 h / 0 °C 2.1: proton sponge; pyridine / 0.25 h / 0 °C 2.2: PSCl3 / 0.25 h / 0 °C 3.1: H2P2O7(2-)*[(Bu3NH)(1+)]2; Bu3N / 0.05 h / 20 °C 3.2: aq. TEAB / 0.67 h / 20 °C 3.3: Sephadex-CM C-25 View Scheme |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: aq. NaOH / methanol / 3 h / 0 °C 2.1: proton sponge; pyridine / 0.25 h / 0 °C 2.2: PSCl3 / 0.25 h / 0 °C 3.1: H2P2O7(2-)*[(Bu3NH)(1+)]2; Bu3N / 0.05 h / 20 °C 3.2: aq. TEAB / 0.67 h / 20 °C 3.3: Sephadex-CM C-25 View Scheme |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: NaOH / methanol / 1.5 h / 20 °C 1.2: 52 percent / dimethylformamide / 48 h / 80 °C 2.1: POCl3; PO(OCH3)3 2.2: (Bu3NH(1+))2H2P2O7(2-) 2.3: 71 percent / H2O View Scheme |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 0.25 M aq. NaOH / methanol / 1 h / 20 °C 1.2: 92 percent / dimethylformamide / 4 h / 20 °C 2.1: proton sponge / various solvent(s) / 0.33 h / 0 °C 2.2: POCl3 / various solvent(s) / 2 h / 0 °C View Scheme |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 0.25 M aq. NaOH / methanol / 1 h / 20 °C 1.2: 92 percent / dimethylformamide / 4 h / 20 °C 2.1: proton sponge / various solvent(s) / 0.33 h / 0 °C 2.2: POCl3 / various solvent(s) / 2 h / 0 °C 3.1: 60 percent / (Bu3NH+)2P2O7H2; Bu3N / dimethylformamide / 0.02 h View Scheme |
2-Mercaptoadenosine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 0.25 M aq. NaOH / methanol / 1 h / 20 °C 1.2: 92 percent / dimethylformamide / 4 h / 20 °C 2.1: proton sponge / various solvent(s) / 0.33 h / 0 °C 2.2: POCl3 / various solvent(s) / 2 h / 0 °C 3.1: 30 percent / (Bu3NH+)2P2O7H2; Bu3N / dimethylformamide / 0.02 h View Scheme |
2-Mercaptoadenosine
N6-(2-methoxyethyl)-2-(3,3,3-trifluoropropylthio)adenosine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1.) NaH / 1.) DMF, 2.) DMF, 36 h 2: 73 percent / AcONa / 7 h / 80 °C 3: NaH / dimethylformamide / 24 h / 60 °C 4: 0.1 M NaOH / methanol / 0.5 h / Heating View Scheme |
2-Mercaptoadenosine
(2R,3S,4R,5R)-2-(hydroxymethyl)-5-(6-((2-(methylthio)ethyl)amino)-2-((3,3,3-trifluoropropyl)thio)-9H-purin-9-yl)tetrahydrofuran-3,4-diol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1.) NaH / 1.) DMF, 2.) DMF, 36 h 2: 73 percent / AcONa / 7 h / 80 °C 3: NaH / dimethylformamide / 24 h / 60 °C 4: 0.1 M NaOH / methanol / 0.5 h / Heating View Scheme | |
Multi-step reaction with 5 steps 1: ethyl acetate / 20 °C 2: triethylamine; dmap / acetonitrile / 0.5 h / 20 - 25 °C 3: copper(ll) bromide; isopentyl nitrite / tetrahydrofuran / 2 h / 30 - 50 °C 4: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C 5: sodium hydroxide; methanol / 0.25 h / 5 °C / Cooling View Scheme | |
Multi-step reaction with 5 steps 1: ethyl acetate / 20 °C 2: triethylamine; dmap / acetonitrile / 0.5 h / 20 - 25 °C 3: isopentyl nitrite; copper dichloride / tetrahydrofuran / 2 h / 30 - 50 °C 4: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C 5: sodium hydroxide; methanol / 0.25 h / 5 °C / Cooling View Scheme | |
Multi-step reaction with 4 steps 1: sodium hydroxide / water 2: sodium acetate / 80 °C 3: sodium hydride / N,N-dimethyl-formamide 4: sodium hydroxide / methanol / Reflux View Scheme |
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