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Cas:475-31-0
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inquiryGlycocholic Acid CAS:475-31-0 / 1192657-83-2 Name Glycocholic acid Synonyms 3a,7a,12a-Trihydroxy-5b-cholan-24-oic acid N-(carboxymethyl)amide; Cholylglycine; N-(3-alpha,7-alpha,12-alpha-Trihydroxy
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inquiryProduct Name: Glycocholic acid Synonyms: GLYCOCHOLIC ACID;GLYCOCHOLIC ACID HYDRATE;GLYCOCHOLIC;cholylglycine;CHOLYLGLYCINE HYDRATE;5-BETA-CHOLANIC ACID-3-ALPHA, 7-ALPHA, 12-ALPHA-TRIOL N-(CARB
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Min.Order:1 Gram
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryglycocholic acid ethyl ester
glycocholic acid
Conditions | Yield |
---|---|
Stage #1: glycocholic acid ethyl ester With water; sodium hydroxide at 20 - 28℃; Stage #2: With hydrogenchloride In water pH=7 - 7.5; | 92.3% |
Conditions | Yield |
---|---|
Stage #1: cholic acid With triethylamine In tetrahydrofuran at 25℃; for 2h; Inert atmosphere; Stage #2: glycine ethyl ester hydrochloride With pivaloyl chloride In tetrahydrofuran; water at 0 - 10℃; Reagent/catalyst; | 78.3% |
Conditions | Yield |
---|---|
With 1,4-dioxane; tributyl-amine anschliessend Behandeln mit Glycin und wss. NaOH; |
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With sodium hydroxide |
cholic acid hydrazide
glycocholic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous hydrochloric acid; aqueous sodium nitrite solution 2: aq. NaOH solution View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h 2: triethylamine; glycine / dimethyl sulfoxide / 4 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 30 °C 2: potassium hydroxide / tetrahydrofuran; water / 10 h / 35 - 40 °C View Scheme |
cholic acid N-succinimidyl ester
glycocholic acid
Conditions | Yield |
---|---|
With triethylamine; glycine In dimethyl sulfoxide at 20℃; for 4h; |
glycocholic acid
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran; water at 35 - 40℃; for 10h; | 0.8 g |
Conditions | Yield |
---|---|
With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate at 20℃; for 24h; | 90% |
Conditions | Yield |
---|---|
With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran at 20℃; for 24h; Reagent/catalyst; | 89% |
Conditions | Yield |
---|---|
With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran at 20℃; for 24h; | 88% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 60 - 70℃; pH=7 - 8; | 87% |
Conditions | Yield |
---|---|
With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran at 20℃; for 24h; | 87% |
Conditions | Yield |
---|---|
With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran at 20℃; for 24h; | 85% |
Conditions | Yield |
---|---|
With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In tetrahydrofuran at 20℃; for 24h; | 85% |
glycocholic acid
N-nitrosoglycocholic acid
Conditions | Yield |
---|---|
With sodium acetate; acetic acid; nitrosylchloride at 10 - 15℃; for 0.5h; | 75% |
Conditions | Yield |
---|---|
Stage #1: glycocholic acid With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: α-amino,ω-azido,α,ω-dideoxy-hexaethyleneglycol With triethylamine In N,N-dimethyl-formamide at 20℃; | 55.56% |
glycocholic acid
Conditions | Yield |
---|---|
Stage #1: glycocholic acid With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: 2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-ethylamine With triethylamine In N,N-dimethyl-formamide at 20℃; | 55% |
ethanol
glycocholic acid
A
cinnamamide
B
ethyl N-[3-phenyl-1-oxo-2-propen-1-yl] glycinate
Conditions | Yield |
---|---|
With 1.) KO2; phase-transfer catalyst 1.) ether, 40 deg C, 8 h; Yield given. Multistep reaction; | A 48% B n/a |
Conditions | Yield |
---|---|
With triethylamine; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; | 38.7% |
glycocholic acid
A
carbon dioxide
B
(3α,5β,7α,12α)-3,7,12-trihydroxycholan-24-amide
C
oxalic acid
Conditions | Yield |
---|---|
With KO2; phase-transfer catalyst In tetrahydrofuran at 40℃; for 8h; Mechanism; | A n/a B 27% C n/a |
Conditions | Yield |
---|---|
Stage #1: glycocholic acid With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline In ethanol at 60℃; for 4h; Stage #2: metformin hydrochloride In ethanol for 24h; Heating; Further stages.; | 20% |
Conditions | Yield |
---|---|
With barium dihydroxide | |
With mineral acid |
glycocholic acid
7-ketodeoxycholic acid glycine-conjugate
Conditions | Yield |
---|---|
With potassium phosphate; NAD; 2-oxo-propionic acid; diothiothreitol In water Ambient temperature; lactic dehydrogenase, 7α-hydroxysteroid dehydrogenase; Yield given; |
glycocholic acid
glycoursodeoxycholic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium phosphate, pyruvate, dithiothreitol, NAD / H2O / Ambient temperature; lactic dehydrogenase, 7α-hydroxysteroid dehydrogenase 2: potassium phosphate, glucose, dithiothreitol, NADP / H2O / glucose dehydrogenase, 7β-hydroxysteroid dehydrogenase View Scheme |
Conditions | Yield |
---|---|
In ethanol at 40℃; for 3h; |
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