CAS No.485-64-3,(8alpha,9R)-10,11-dihydrocinchonan-9-ol Suppliers

Dayang Chem (Hangzhou) Co.,Ltd.

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(8alpha,9R)-10,11-dihydrocinchonan-9-ol

Cas:485-64-3

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Shanghai Upbio Tech Co.,Ltd

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Cinchonan-9-ol,10,11-dihydro-, (8a,9R)-

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Xiamen Jenny Chemical Technology Co., Ltd.

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(8alpha,9R)-10,11-dihydrocinchonan-9-ol

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Cinchonan-9-ol,10,11-dihydro-, (8a,9R)-

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Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for fluorhe synthesis of various pesticides, medicines, surfactants, polymer monomers, nd ntifungal agents

Cinchonan-9-ol,10,11-dihydro-, (8a,9R)-

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Zibo Hangyu Biotechnology Development Co., Ltd

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(8alpha,9R)-10,11-dihydrocinchonan-9-ol

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

(8alpha,9R)-10,11-dihydrocinchonan-9-ol

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Shanghai Goyic Pharmaceutical&Chemical Co,. Ltd

Dihydrocinchonidine; (R)-((1S,2S,4S,5R)-5-ethylquinuclidin-2-yl)(6-methoxyquinolin-4-yl)methanol CAS No. 485-64-3 Product Name: (8alpha,9R)-10,11-dihydrocinchonan-9-ol Chemical Name：(R)-((1S,2S,4S,5R)-5-ethylquinuclidin-2-yl)(6-meth

(R)-((1S,2S,4S,5R)-5-ethylquinuclidin-2-yl)(6-methoxyquinolin-4-yl)methanol CAS No. 485-64-3

Cas:485-64-3

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Simson Pharma Limited

The system can just identify the products information in first sheet, it is not be permitted to add or edit new sheet by userself.Our products are required in MG to Gram only. · Pharmaceutical Reference Standards· Traceable workin

10,11-Dihydrocinchonidine (Cinchamidine)

Cas:485-64-3

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Finetech Industry Limited

High Quality Best Price Storage:Store in dry, dark and ventilated place Application:Chemical Synthesis Intermediate

FT-0700733

Cas:485-64-3

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Synthetic route

: 485-71-2
Cinchonidin

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 10h;	92%
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 12h;	86%
With triethylsilane; 1% Pd on activated carbon In water at 45℃; for 24h; Reagent/catalyst; Green chemistry; chemoselective reaction;	83%

: 5962-19-6
(8α,9R)-10,11-dihydro-cinchonan-6',9-diol

: 485-64-3
(-)-hydrocinchonidine

: 109922-61-4, 109959-06-0
1-[(3R,4S)-3-Ethyl-4-(3-quinolin-4-yl-oxiranylmethyl)-piperidin-1-yl]-2,2,2-trifluoro-ethanone

A: 485-65-4
dihydrocinchonine

B: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
With potassium carbonate 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h; Yield given. Multistep reaction. Yields of byproduct given;

dihydrocinchoninone: dihydrocinchoninone

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
With sodium ethanolate; aluminium
With sodium ethanolate; zinc
With sodium ethanolate; aluminium
With sodium ethanolate; zinc

hydrocinchoninone: hydrocinchoninone

A: 485-65-4
dihydrocinchonine

B: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
With ethanol; palladium Hydrogenation;

: 71-41-0
pentan-1-ol

: 485-65-4
dihydrocinchonine

KOH: KOH

A: 73522-74-4
hydrocinchonine

B: 485-64-3
(-)-hydrocinchonidine

C: 73522-73-3
hydrocinchonidine

...Expand

: 485-65-4
dihydrocinchonine

A: 485-64-3
(-)-hydrocinchonidine

B (9R)-10,11-dihydro-cinchonan-9-ol, epihydrocinchonidine: (9R)-10,11-dihydro-cinchonan-9-ol, epihydrocinchonidine

Conditions

Conditions	Yield
With potassium hydroxide; pentan-1-ol

: 491-35-0
C6H4NCH2CHCCH2

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: lithium diisopropylamide, pyridine hydrochloride 2: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature 3: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h 4: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min 5: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 6: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

Yield

Multi-step reaction with 6 steps
1: lithium diisopropylamide, pyridine hydrochloride
2: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature
3: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h
4: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min
5: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h
6: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h
View Scheme

: 109922-57-8
[4]quinolyl-acetic acid

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature 2: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h 3: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min 4: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 5: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

Yield

Multi-step reaction with 5 steps
1: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature
2: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h
3: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min
4: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h
5: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h
View Scheme

: 109922-60-3
4-[(E)-3-((3R,4R)-3-Ethyl-piperidin-4-yl)-propenyl]-quinoline

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 2: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

: 109922-59-0
(4S,5R)-5-Ethyl-4-((E)-3-quinolin-4-yl-allyl)-1,4,5,6-tetrahydro-pyridine-3-carboxylic acid methyl ester

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min 2: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 3: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

: 52530-99-1
dihydrosecologanin

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 5 steps 1: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature 2: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h 3: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min 4: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 5: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

Yield

: 109922-58-9
(4S,5R,6S)-5-Ethyl-4-((E)-3-quinolin-4-yl-allyl)-6-((2R,3S,4R,5R,6S)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-5,6-dihydro-4H-pyran-3-carboxylic acid methyl ester

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h 2: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min 3: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 4: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

: 19351-28-1, 19351-63-4
secologanoside

: 485-64-3
(-)-hydrocinchonidine

Conditions

Conditions	Yield
Multi-step reaction with 6 steps 1: catalytic hydrogenation 2: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature 3: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h 4: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min 5: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h 6: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h View Scheme

Yield

Multi-step reaction with 6 steps
1: catalytic hydrogenation
2: 90 percent / pyridine hydrochloride / methanol; pyridine; various solvent(s) / 36 h / Ambient temperature
3: 1) water 2.) NH4OAc, NaCNBH3 / 1) β-glucosidase / 2.) pH=6.2, 18 h
4: 1.) 3percent HCl, 2.) NaCNBH3 / 1.) aq MeOH, reflux, 40 min
5: 2.) CF3CO3H, Na2HPO4 / 1.) 0 grad C, 2.) CH2Cl2, rt, 12 h
6: 1.) K2CO3 / 1.) MeOH, rt, 2 h, 2.) toluene, EtOH, reflux 24 h
View Scheme

: 38309-89-6
2,7-bis(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: 2,7-bis(hydrocinchonidinium-N-methyl)naphthalene dibromide

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;	97%
In ethanol; chloroform; N,N-dimethyl-formamide at 100 - 120℃; for 2h;	60%

: 31640-94-5
2-(chloromethyl)pyridine N-oxide

: 485-64-3
(-)-hydrocinchonidine

: N-(1-oxypyridin-2-ylmethyl)hydrocinchonidinium bromide

Conditions

Conditions	Yield
Stage #1: 2-(chloromethyl)pyridine N-oxide; (-)-hydrocinchonidine In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 3h; Stage #2: With bromide	93%

: 2595-90-6
1-bromomethylpyrene

: 485-64-3
(-)-hydrocinchonidine

: N-[(1-pyrenyl)methyl]hydrocinchonidinium bromide

Conditions

Conditions	Yield
In toluene at 100℃; for 8h;	92%

: 22115-41-9
2-(bromomethyl)benzonitrile

: 485-64-3
(-)-hydrocinchonidine

: N-(2'-cyanobenzyl)hydrocinchonidinium bromide

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 4h;	92%

: 485-64-3
(-)-hydrocinchonidine

: 13-(bromomethyl)picene

: N-[(13-picenyl)methyl]hydrocinchonidinium bromide

Conditions

Conditions	Yield
In toluene at 100℃; for 8h;	91%

: 1308718-76-4
4-(bromomethyl)-N-(phenyl)benzenesulfonamide

: 485-64-3
(-)-hydrocinchonidine

: C32H36N3O3S(1+)*Br(1-)

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 25℃; for 20h;	83%

: 485-64-3
(-)-hydrocinchonidine

: 1253690-81-1
(S)-((1S,2S,4S,5R)-5-ethylquinuclidin-2-yl)(quinolin-4-yl)methanamine

Conditions

Conditions	Yield
Stage #1: (-)-hydrocinchonidine With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine In tetrahydrofuran at 0 - 50℃; for 24h; Inert atmosphere; Stage #2: With triphenylphosphine In tetrahydrofuran at 50℃; for 4h; Inert atmosphere; Stage #3: With water In tetrahydrofuran at 20℃; Inert atmosphere;	67%

: 24463-19-2
anthracenylmethyl chloride

: 485-64-3
(-)-hydrocinchonidine

: (2S,5R,1'R)-1-(9-anthracenyl)methyl-5-ethyl-2-<1-hydroxy-1-(quinol-4-yl)>methyl-1-azoniabicyclo<2.2.2>octane chloride

Conditions

Conditions	Yield
In toluene for 24h; Heating;	66%

: 485-64-3
(-)-hydrocinchonidine

: 34304-08-0
10,11-dihydrocinchonanone

Conditions

Conditions	Yield
Oppenauer Oxidation;	62%

: 485-64-3
(-)-hydrocinchonidine

palladium/charcoal: palladium/charcoal

A: 491-35-0
C6H4NCH2CHCCH2

B: 612-11-3
3,4-diethyl-pyridine

Conditions

Conditions	Yield
at 250 - 310℃;

...Expand

: 485-64-3
(-)-hydrocinchonidine

: 486-74-8
4-quinolinic acid

: 7647-01-0
hydrogenchloride

: 485-64-3
(-)-hydrocinchonidine

epihydrocinchonidine: epihydrocinchonidine

: 64-19-7
acetic acid

: 485-64-3
(-)-hydrocinchonidine

colloidal platinum: colloidal platinum

hexahydro-cinchonidine: hexahydro-cinchonidine

Conditions

Conditions	Yield
at 53℃; unter Druck.Hydrogenation;

...Expand

: 38998-33-3
2,3-di(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: C50H58N4O2(2+)*2Br(1-)

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;

: 58791-49-4
1,4-bis(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: C50H58N4O2(2+)*2Br(1-)

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;

: 21646-18-4
1,5-di(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: C50H58N4O2(2+)*2Br(1-)

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;

: 2025-95-8
1,8-bis(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: C50H58N4O2(2+)*2Br(1-)

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;

: 4542-77-2
2,6-bis(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: C50H58N4O2(2+)*2Br(1-)

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;

: 38309-89-6
2,7-bis(bromomethyl)naphthalene

: 485-64-3
(-)-hydrocinchonidine

: C50H58N4O2(2+)*2Br(1-)

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide at 100℃; for 6h;

: 485-64-3
(-)-hydrocinchonidine

: 626-15-3
1,3-bis-(bromomethyl)benzene

: 1,3-bis(hydrocinchonidinium-N-methyl)benzene dibromide

Conditions

Conditions	Yield
In ethanol; chloroform; N,N-dimethyl-formamide

: 485-64-3
(-)-hydrocinchonidine

: 2,7-bis[O(9)-allylhydrocinchonidinium-N-methyl]naphthalene dibromide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 97 percent / dimethylformamide; ethanol; CHCl3 / 6 h / 100 °C 2: 95 percent / KOH / CH2Cl2; H2O / 4 h / 20 °C View Scheme

: 485-64-3
(-)-hydrocinchonidine

: N-(2'-cyanobenzyl)-O(9)-allylhydrocinchonidinium bromide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 92 percent / ethanol; dimethylformamide; CHCl3 / 4 h / 100 °C 2: 94 percent / aq. KOH / CH2Cl2 / 4 h / 20 °C View Scheme

: 485-64-3
(-)-hydrocinchonidine

: N-[(1-pyrenyl)methyl]-O(9)-allylhydrocinchonidinium bromide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 92 percent / toluene / 8 h / 100 °C 2: KOH / CH2Cl2; H2O / 20 °C View Scheme

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