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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryCAS4943-85-5 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE Application:CAS4943-85-5 2-AMINO-N-(2-METHYLPHENYL)BENZAMIDE
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inquirybest seller Application:API
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:beige crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use
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inquiryConditions | Yield |
---|---|
With tetrahydroxydiboron; 5%-palladium/activated carbon; water In acetonitrile at 50℃; for 24h; | 99% |
With tetrahydroxydiboron; palladium on activated charcoal; water In acetonitrile at 50℃; for 24h; Inert atmosphere; | 99% |
With hydrogen; palladium on activated charcoal In ethyl acetate under 750.075 Torr; | 87% |
2-methylchlorobenzene
anthranilic acid amide
A
2-amino-N-(2-methylphenyl)benzamide
B
2-(2-methylphenylamino)benzamide
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate; XPhos In tert-butyl alcohol at 110℃; for 17h; | A 10% B 87% |
Conditions | Yield |
---|---|
With aqueous extract of mesocarp of fruit of Balanites roxburghii plant at 60℃; for 0.333333h; | 83% |
In ethanol for 20h; Reflux; | 67% |
o-toluidine
2-aminobenzoyl chloride
2-amino-N-(2-methylphenyl)benzamide
Conditions | Yield |
---|---|
In diethyl ether at 0 - 10℃; for 0.5h; | 81.39% |
Conditions | Yield |
---|---|
In ethyl acetate at 90℃; for 18h; | 50% |
methaqualone
A
2-Acetamidobenzoesaeure-2'-methylanilid
B
2-amino-N-(2-methylphenyl)benzamide
C
o-toluidine
Conditions | Yield |
---|---|
With sodium hydroxide for 7h; Heating; hydrolysis; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 63 percent / aq. K2CO3 / tetrahydrofuran / 12 h / Heating 2: 51 percent / H2 / 5percent Pd/C / 3 h / 2327.2 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 63 percent / aq. K2CO3 / tetrahydrofuran / 12 h / Heating 2: 51 percent / H2 / 5percent Pd/C / 3 h / 2327.2 Torr View Scheme |
2-methylchlorobenzene
anthranilic acid amide
A
2-amino-N-(2-methylphenyl)benzamide
B
2-(2-methylphenylamino)benzamide
Conditions | Yield |
---|---|
With potassium carbonate; tris-(dibenzylideneacetone)dipalladium(0) In hexane | A 98 mg (87%) B n/a |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / 4.5 h / 80 °C 2: diethyl ether / 0.5 h / 0 - 10 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C 2: triethylamine / dichloromethane 3: ammonium chloride; zinc / tetrahydrofuran; water / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / dichloromethane 2: ammonium chloride; zinc / tetrahydrofuran; water / 20 °C View Scheme |
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In water; ethyl acetate at 100℃; for 24h; | 99% |
With camphor-10-sulfonic acid In water at 100℃; for 24h; Green chemistry; | 69% |
Conditions | Yield |
---|---|
Stage #1: ethanol With oxygen; eosin y In dimethyl sulfoxide at 25℃; for 20h; Sealed tube; Irradiation; Green chemistry; Stage #2: 2-amino-N-(2-methylphenyl)benzamide With toluene-4-sulfonic acid In dimethyl sulfoxide at 25℃; for 24h; Reagent/catalyst; Wavelength; Temperature; Solvent; Sealed tube; Irradiation; Green chemistry; | 98% |
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] at 150℃; for 24h; Inert atmosphere; Sealed tube; | 97% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 95% |
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In water at 100℃; for 16h; Green chemistry; | 93% |
With camphor-10-sulfonic acid In water at 100℃; for 24h; | 93% |
With toluene-4-sulfonic acid In toluene at 120℃; for 10h; Sealed tube; | 89% |
With iron(III) chloride hexahydrate In water at 100℃; for 24h; Green chemistry; | 73% |
2-amino-N-(2-methylphenyl)benzamide
Glyoxilic acid
3-(2-methylphenyl)quinazolin-4(3H)-one
Conditions | Yield |
---|---|
With N,N,N,N,-tetramethylethylenediamine; di-tert-butyl peroxide; copper(II) bis(trifluoromethanesulfonate) In 1,2-dichloro-ethane at 120℃; for 24h; Schlenk technique; | 92% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 91% |
2-amino-N-(2-methylphenyl)benzamide
3-(2-methylphenyl)benzo-1,2,3-triazin-4(3H)-one
Conditions | Yield |
---|---|
With tert.-butylnitrite; saccharin In ethanol at 50℃; for 6h; Green chemistry; | 90% |
With tert.-butylnitrite; tetra-(n-butyl)ammonium iodide In acetonitrile at 60℃; for 12h; Green chemistry; | 85% |
With toluene-4-sulfonic acid In methanol at 0 - 40℃; for 5h; | 77% |
2-amino-N-(2-methylphenyl)benzamide
acetaldehyde
2-methyl-3-(o-tolyl)-2,3-dihydro-4(1H)-quinazolinone
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 88% |
With L-Tartaric acid; N,N'-Dimethylurea at 90℃; Green chemistry; | 87% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 85% |
2-amino-N-(2-methylphenyl)benzamide
butanone
2-methyl-2-ethyl-3-(o-tolyl)-2,3-dihydro-4(1H)-quinazolinone
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 85% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 81% |
formaldehyd
2-amino-N-(2-methylphenyl)benzamide
3-(o-tolyl)-2,3-dihydro-4(1H)-quinazolinone
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 75% |
bis(1-methyl-1-phenylethyl)peroxide
2-amino-N-(2-methylphenyl)benzamide
3-(2-methylphenyl)quinazolin-4(3H)-one
Conditions | Yield |
---|---|
With 1H-imidazole; copper(II) acetate monohydrate In chlorobenzene at 120℃; for 10h; | 75% |
2-amino-N-(2-methylphenyl)benzamide
benzaldehyde
2-phenyl-3-(o-tolyl)-2,3-dihydro-4(1H)-quinazolinone
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 72% |
Conditions | Yield |
---|---|
With p-toluenesulfonic acid monohydrate; oxygen at 110℃; Sealed tube; Green chemistry; | 71% |
tert-butylisonitrile
2-amino-N-(2-methylphenyl)benzamide
3-(2-methylphenyl)quinazolin-4(3H)-one
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In acetonitrile at 70℃; for 24h; | 70% |
2-amino-N-(2-methylphenyl)benzamide
vanillin
2-(4-Hydroxy-3-methoxy-phenyl)-3-o-tolyl-2,3-dihydro-1H-quinazolin-4-one
Conditions | Yield |
---|---|
In ethanol water bath; | 67% |
2-amino-N-(2-methylphenyl)benzamide
Benzoylformic acid
3-(2-methylphenyl)-2-phenylquinazolin-4(3H)-one
Conditions | Yield |
---|---|
With tetraethylammonium hexafluorophosphate In 2,2,2-trifluoroethanol at 20℃; for 6h; Electrochemical reaction; Green chemistry; | 66% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In water; 1,2-dichloro-ethane at 80℃; for 36h; | 63% |
2-amino-N-(2-methylphenyl)benzamide
dimethyl sulfoxide
3-(2-methylphenyl)quinazolin-4(3H)-one
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; dipotassium peroxodisulfate at 160℃; for 2h; Microwave irradiation; | 61% |
(E)-3-phenylpropenal
2-amino-N-(2-methylphenyl)benzamide
2-((E)-Styryl)-3-o-tolyl-2,3-dihydro-1H-quinazolin-4-one
Conditions | Yield |
---|---|
In ethanol water bath; | 60% |
2-amino-N-(2-methylphenyl)benzamide
sodium chlorodifluoroacetate
3-(2-methylphenyl)quinazolin-4(3H)-one
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 120℃; for 24h; Schlenk technique; | 60% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; dipotassium peroxodisulfate In 5,5-dimethyl-1,3-cyclohexadiene at 160℃; for 2h; Microwave irradiation; | 57% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Heating; | 54% |
2-amino-N-(2-methylphenyl)benzamide
salicylaldehyde
2-(2-Hydroxy-phenyl)-3-o-tolyl-2,3-dihydro-1H-quinazolin-4-one
Conditions | Yield |
---|---|
In ethanol water bath; | 50% |
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