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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiry(Z)-5-DECEN-1-OLAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the Z-5-Decen-1-ol, CAS:51652-47-2 with the most competitive price and the best quality.
intermediateAppearance:powder/liquid Storage:Normal temperature Package:1kg/25kg/customized Application:intermediate Transportation:By Ship/Air
(Z)-1-(2-tetrahydropyranyloxy)-dec-5-ene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In methanol at 50℃; for 2h; | 100% |
With pyridinium p-toluenesulfonate In methanol at 50℃; for 2h; | 100% |
With toluene-4-sulfonic acid In methanol for 6h; Ambient temperature; | 85% |
(5S,6R)-6-(Diphenyl-phosphinoyl)-decane-1,5-diol
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 98% |
98% |
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 50℃; for 2h; | 97.5% |
dec-5-yn-1-ol
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With ethanol; (NCP)IrHCl; tert-butylamine at 85℃; for 72h; Inert atmosphere; Sealed tube; stereoselective reaction; | 97% |
With hydrogen at 40℃; under 760.051 Torr; for 5h; stereoselective reaction; | 96% |
With quinoline; hydrogen In ethyl acetate for 3.5h; | 92% |
(Z)-5-Decensaeure-methylester
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In diethyl ether; toluene at 0 - 20℃; for 17h; | 95% |
With lithium aluminium tetrahydride In diethyl ether | 84% |
With lithium aluminium tetrahydride In tetrahydrofuran for 4h; Heating; |
(Z)-5-decenyl acetate
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 24h; | 93% |
(Z)-deca-1,5-diene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide In tetrahydrofuran; methanol Oxidation; | 92% |
(i) 9-bora-bicyclo<3.3.1>nonane, (ii) H2O2; Multistep reaction; | |
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide 1) 2h, THF; 2) 0 deg C; 3) 50 deg C; Multistep reaction; | |
With 9-borabicyclo[3.3.1]nonane dimer; hydroxide hydroboration-oxidation; |
Conditions | Yield |
---|---|
With dihydridotetrakis(triphenylphosphine)ruthenium; hydrogen In ethanol at 20℃; for 36h; optical yield given as %de; stereoselective reaction; | A 91% B n/a |
(Z)-dec-5-enal
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride | 85% |
With lithium aluminium tetrahydride In diethyl ether at 20℃; for 5h; | 85% |
With diisobutylaluminium hydride In diethyl ether; toluene at -10℃; for 1.5h; Yield given; | |
With diisobutylaluminium hydride In diethyl ether; toluene at -10℃; for 1.5h; Yield given; |
(Z)-6-iodo-5-hexene-1-ol
(s)-pinanediol butylboronate
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Stage #1: (s)-pinanediol butylboronate With sec.-butyllithium In tetrahydrofuran; cyclohexane at -78 - 20℃; for 1.5h; Suzuki-Miyaura reaction; Stage #2: (Z)-6-iodo-5-hexene-1-ol With sodium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran at 70 - 80℃; | 60% |
tetrahydro-2H-2-pyranol
pentylidenetriphenylphosphorane
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
52.5% |
tetrahydro-2H-2-pyranol
pentyltriphenylphosphonium bromide
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With sodium hydride; dimethyl sulfoxide |
Conditions | Yield |
---|---|
With tert.-butyl lithium 1.) ether, hexane, 0 deg C, 2 h, 2.) a) 0 deg C, 0.5 h, b) RT, 0.5 h; Yield given. Multistep reaction; |
5-hydroxypentanal
pentylidenetriphenylphosphorane
A
(Z)-dec-5-en-1-ol
B
(E)-5-decen-1-ol
Conditions | Yield |
---|---|
With sodium ethanolate In toluene at 25℃; for 2h; Yield given. Yields of byproduct given; | |
With n-butyllithium In toluene at 25℃; for 2h; Yield given. Yields of byproduct given; |
10-tosyloxy-5Z-decenal
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether at 0℃; for 4h; Yield given; |
A
(Z)-dec-5-en-1-ol
B
(E)-5-decen-1-ol
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given; |
[((Z)-Dec-5-enyl)oxy]-trimethyl-silane
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With hydrogenchloride for 0.5h; Yield given; |
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride |
4-iodobutoxy-trimethyl-silane
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
5-hydroxypentanal
pentyltriphenylphosphonium bromide
A
(Z)-dec-5-en-1-ol
B
(E)-5-decen-1-ol
Conditions | Yield |
---|---|
Stage #1: pentyltriphenylphosphonium bromide With potassium tert-butylate In toluene Dehydrobromination; Heating; Stage #2: 5-hydroxypentanal In toluene at 25℃; for 2h; Wittig reaction; |
pentanal
5-hydroxypentyltriphenylphosphonium bromide
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Stage #1: 5-hydroxypentyltriphenylphosphonium bromide With sodium hydride In tetrahydrofuran; dimethyl sulfoxide at 15℃; Stage #2: pentanal In tetrahydrofuran; dimethyl sulfoxide for 24h; Wittig reaction; | 164 mg |
1Z,6Z-cyclodecadiene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 2: pyridine / 15 h / -10 °C 3: Zn, sodium iodide / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 4: 10percent aq. hydrochloric acid / acetone / 6 h / Ambient temperature 5: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C View Scheme | |
Multi-step reaction with 5 steps 1: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 2: pyridine / 15 h / -10 °C 3: pyridinium p-toluenesulfonate / acetone; H2O / 2 h / Heating 4: lithium aluminum hydride / diethyl ether / 4 h / 0 °C View Scheme | |
Multi-step reaction with 6 steps 1: 1.) O3, glacial acetic acid, 2.) sodium acetate, 3.) toluene-p-sulfonic acid / 1.) ctclohexane, 8 deg C 2: 95 percent / DIBAH / diethyl ether; toluene / 19.5 h 3: pyridine / 15 h / -10 °C 4: sodium iodide, zinc / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 5: aq. HCl / acetone / 6 h 6: DIBAH / diethyl ether; toluene / 1.5 h / -10 °C View Scheme |
1,1-dimethoxy-5Z-decene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 10percent aq. hydrochloric acid / acetone / 6 h / Ambient temperature 2: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C View Scheme | |
Multi-step reaction with 2 steps 1: aq. HCl / acetone / 6 h 2: DIBAH / diethyl ether; toluene / 1.5 h / -10 °C View Scheme |
1,1-dimethoxy-10-hydroxy-5Z-decene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: pyridine / 15 h / -10 °C 2: Zn, sodium iodide / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 3: 10percent aq. hydrochloric acid / acetone / 6 h / Ambient temperature 4: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C View Scheme | |
Multi-step reaction with 3 steps 1: pyridine / 15 h / -10 °C 2: pyridinium p-toluenesulfonate / acetone; H2O / 2 h / Heating 3: lithium aluminum hydride / diethyl ether / 4 h / 0 °C View Scheme | |
Multi-step reaction with 4 steps 1: pyridine / 15 h / -10 °C 2: sodium iodide, zinc / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 3: aq. HCl / acetone / 6 h 4: DIBAH / diethyl ether; toluene / 1.5 h / -10 °C View Scheme |
methyl 10,10-dimethoxy-5Z-decenoate
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 2: pyridine / 15 h / -10 °C 3: Zn, sodium iodide / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 4: 10percent aq. hydrochloric acid / acetone / 6 h / Ambient temperature 5: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C View Scheme | |
Multi-step reaction with 4 steps 1: 95 percent / diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 2: pyridine / 15 h / -10 °C 3: pyridinium p-toluenesulfonate / acetone; H2O / 2 h / Heating 4: lithium aluminum hydride / diethyl ether / 4 h / 0 °C View Scheme | |
Multi-step reaction with 5 steps 1: 95 percent / DIBAH / diethyl ether; toluene / 19.5 h 2: pyridine / 15 h / -10 °C 3: sodium iodide, zinc / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 4: aq. HCl / acetone / 6 h 5: DIBAH / diethyl ether; toluene / 1.5 h / -10 °C View Scheme |
1,1-dimethoxy-10-tosyloxy-5Z-decene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Zn, sodium iodide / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 2: 10percent aq. hydrochloric acid / acetone / 6 h / Ambient temperature 3: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C View Scheme | |
Multi-step reaction with 2 steps 1: pyridinium p-toluenesulfonate / acetone; H2O / 2 h / Heating 2: lithium aluminum hydride / diethyl ether / 4 h / 0 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium iodide, zinc / bis-(2-methoxy-ethyl) ether / 1.5 h / Heating 2: aq. HCl / acetone / 6 h 3: DIBAH / diethyl ether; toluene / 1.5 h / -10 °C View Scheme |
1,5-cis,cis-cyclooctadiene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 55 g / Me4Sn / MoCl5/SiO2 / toluene / 24 h / 20 °C 2: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 1 h / 20 °C 3: 92 percent / 9-BBN; NaOH; H2O2 / tetrahydrofuran; methanol View Scheme |
(Z)-deca-1,5,9-triene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 1 h / 20 °C 2: 92 percent / 9-BBN; NaOH; H2O2 / tetrahydrofuran; methanol View Scheme | |
Multi-step reaction with 2 steps 1: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 2 h 2: 9-BBN; OH(1-) View Scheme |
1,5-dicyclooctadiene
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 68.4 percent / MoCl5/SiO2; SnMe4 / toluene / 24 h / 20 °C / 19000 Torr 2: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 2 h 3: 9-BBN; OH(1-) View Scheme |
2-(5-decynyloxy)tetrahydro-2H-pyran
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: TsOH / methanol; H2O / 24 h 2: 1.) i-BuMgBr, 2.) Cp2TiCl2, 3.) aq. HCl / 1) Et2O, 0 deg C, 15 min; 2) Et2O, 20 deg C, 1-1.5 h; 3) Et2O, 20 deg C, 0.5 h View Scheme |
Conditions | Yield |
---|---|
In pyridine | 98% |
With pyridine for 24h; Ambient temperature; | 97% |
With pyridine; dmap at 0℃; for 0.333333h; | 97% |
(Z)-dec-5-en-1-ol
isopentanoyl chloride
dec-5(Z)-en-1-yl 3-methylbutanoate
Conditions | Yield |
---|---|
With pyridine In dichloromethane for 18h; Ambient temperature; | 98% |
With pyridine In dichloromethane Ambient temperature; | 95% |
With pyridine In dichloromethane at 20℃; for 18h; | 87% |
(Z)-dec-5-en-1-ol
(Z)-dec-5-enal
Conditions | Yield |
---|---|
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -60 - -15℃; for 1.5h; | 96% |
With pyridinium chlorochromate | 74.7% |
With Pyr*CrO3*HCl | 70% |
Conditions | Yield |
---|---|
With pyridine In hexane at 12 - 20℃; for 2h; Acetylation; | 93% |
With pyridine In benzene at 20℃; for 0.666667h; | 85% |
(Z)-dec-5-en-1-ol
tert-butyl N-tosyloxycarbamate
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 18h; Mitsunobu Displacement; Inert atmosphere; | 89% |
(Z)-dec-5-en-1-ol
1-bromo-dec-5c-ene
Conditions | Yield |
---|---|
With bromine; triethylphosphine In tetrachloromethane 1.) 15 deg C, 1h, 2.) RT, 15 h; | 87% |
With pyridine; phosphorus tribromide | |
Multi-step reaction with 2 steps 1: 1.81 g / Py / 15 h / 0 °C 2: 80 percent / LiBr / acetone / 3 h / 40 °C View Scheme |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triethylamine In tetrahydrofuran at 20℃; for 16.5h; | 71% |
(Z)-dec-5-en-1-ol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran; toluene at 0 - 20℃; for 15h; | 67% |
Conditions | Yield |
---|---|
Stage #1: (Z)-dec-5-en-1-ol With 1H-imidazole; dmap In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: triethylsilyl chloride In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 56% |
(Z)-dec-5-en-1-ol
acetic anhydride
A
(Z)-5-decenyl acetate
B
(E)-5-decen-1-yl acetate
Conditions | Yield |
---|---|
With pyridine Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
(Z)-dec-5-en-1-ol
p-toluenesulfonyl chloride
Toluene-4-sulfonic acid (Z)-dec-5-enyl ester
Conditions | Yield |
---|---|
With pyridine at 0℃; for 15h; | 1.81 g |
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