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Qingdao Beluga Import and Export Co., LTD

HEXADECADIENOLACETATE CAS:53042-79-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in

HEXADECADIENOLACETATE CAS:53042-79-8

Cas:53042-79-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

HEXADECADIENOLACETATE

Cas:53042-79-8

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

HEXADECADIENOLACETATE

Cas:53042-79-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

(Z,E)-7,11-Hexadecadien-1-yl acetate

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services：A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:

Z,E-7,11-Hexadecadienyl acetate53042-79-8

Cas:53042-79-8

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an

HEXADECADIENOLACETATE China manufacture

Cas:53042-79-8

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:White to Off-White Solid Storage:Keep it in dry,shady and cool place Package:as your requirement Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by Sea

HEXADECADIENOLACETATE

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

(Z,Z)-7,11-HEXADECADIEN-1-OL ACETATEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

(Z,Z)-7,11-HEXADECADIEN-1-OL ACETATE

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

HEXADECADIENOLACETATE

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

HEXADECADIENOLACETATE

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Kunming Biohome Technology Co. Ltd.

BIOHOMEAppearance:Colorless?to?pale?yellow?liquid Application:Angoumois grain moth (Sitotroga cerealella), Dichomeris oceana

Z,E-7,11-Hexadecadienyl acetate

Cas:53042-79-8

Min.Order:0

Negotiable

Type:

inquiry

Zhengzhou Kingorgchem Chemical Technology Co., Ltd.

1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume

National Research Platform ISO 9001 53042-79-8

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

U-Chemo Holding Co.,Limited

U-CHEMO Holding Co.,Limited is a very fast developing high-technology enterprise combining with manufacture and sales.U-CHEMO supply high quality products and excellent service to our customers.We make the insect pheromones, censor in the quality con

7Z11E-16Ac

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Raymon Biotech Co., Ltd.

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Petrochemical Co.,Ltd

intermediateAppearance:powder/liquid Storage:Normal temperature Package:1kg/25kg/customized Application:intermediate Transportation:By Ship/Air

Z,E-7,11-Hexadecadienyl acetate

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Other

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

53042-79-8

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemical Co.Ltd

Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

7,11-Hexadecadien-1-ol,1-acetate, (7Z,11E)-

Cas:53042-79-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry
View More

Synthetic route

(E)-11-hexadecen-7-ynyl acetate
53042-78-7

(E)-11-hexadecen-7-ynyl acetate

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
With quinoline; hydrogen; Lindlar's catalyst In ethanol under 760 Torr;94%
With quinoline; hydrogen; Lindlar's catalyst In methanol
(7Z,11E)-1-(2'-tetrahydropyranyloxy)hexadeca-7,11-diene
53155-14-9

(7Z,11E)-1-(2'-tetrahydropyranyloxy)hexadeca-7,11-diene

acetyl chloride
75-36-5

acetyl chloride

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
With acetic acid Heating;92%
In acetic acid for 5h; Heating;81%
With pyridine; acetic acid for 12h; Ambient temperature;80%
In acetic acid
(7Z,11E)-hexadeca-7,11-dien-1-ol
53963-09-0

(7Z,11E)-hexadeca-7,11-dien-1-ol

acetic anhydride
108-24-7

acetic anhydride

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
With pyridine62%
With pyridine
With pyridine for 24h; Ambient temperature; Yield given;
ethyl 3-hydroxy-heptanoate
126784-39-2

ethyl 3-hydroxy-heptanoate

Acetic acid (Z)-10-iodo-dec-7-enyl ester

Acetic acid (Z)-10-iodo-dec-7-enyl ester

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multistep reaction;
11-(Z/E)-Hexadecen-7-yn-1-yl acetate
53042-78-7, 53042-80-1

11-(Z/E)-Hexadecen-7-yn-1-yl acetate

A

(7Z,11Z)-7,11-hexadecadien-1-yl acetate
52207-99-5

(7Z,11Z)-7,11-hexadecadien-1-yl acetate

B

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
With quinoline; hydrogen; Pd-BaSO4 In methanol under 3800 Torr; Ambient temperature; Yield given. Yields of byproduct given;
2-[((7Z,11Z)-Hexadeca-7,11-dienyl)oxy]-tetrahydro-pyran
53155-14-9, 53155-15-0, 53155-16-1, 53155-17-2

2-[((7Z,11Z)-Hexadeca-7,11-dienyl)oxy]-tetrahydro-pyran

acetyl chloride
75-36-5

acetyl chloride

A

(7Z,11Z)-7,11-hexadecadien-1-yl acetate
52207-99-5

(7Z,11Z)-7,11-hexadecadien-1-yl acetate

B

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
In acetic acid for 0.5h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
In acetic acid for 3h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
...Expand
7,11-hexadecadienal
96883-53-3, 96883-54-4, 131392-75-1, 131400-46-9

7,11-hexadecadienal

acetyl chloride
75-36-5

acetyl chloride

A

(7Z,11Z)-7,11-hexadecadien-1-yl acetate
52207-99-5

(7Z,11Z)-7,11-hexadecadien-1-yl acetate

B

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
In pyridine at 0℃; for 0.166667h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
...Expand
acetic acid 7-oxo-heptyl ester
29425-54-5

acetic acid 7-oxo-heptyl ester

<(E)-4-Nonenyl>-triphenylphosphonium-bromid
59512-90-2

<(E)-4-Nonenyl>-triphenylphosphonium-bromid

A

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

B

(7Z,11Z/E)-7,11-hexadecadienyl acetate
53042-81-2

(7Z,11Z/E)-7,11-hexadecadienyl acetate

Conditions
ConditionsYield
With sodium hexamethyldisilazane 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
...Expand
2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran
53963-10-3

2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1) LiNH2 / 1) NH3(l), 3 h; 2) abs THF, 20-25 deg C, 13 h.
2: 80 percent / nickel acetate, NaBH4, ethylene diamine / ethanol
3: 80 percent / pyridinium chlorochromate / CH2Cl2
4: 1) butyllithium, 2) butyllithium, 3) ethanol / 1) abs. THF, hexan, -30 deg C, 90 min; 2) abs. THF, hexan, 40 min at -60 deg C and 15 min at -30 deg C; 3) 30 min at -30 deg C and 24 h at -40 deg C.
5: 92 percent / glacial acetic acid / Heating
View Scheme
Multi-step reaction with 5 steps
1: 76 percent / LiNH2, NH3 (liquid) / tetrahydrofuran / 5 h
2: ethylene diamine, H2 / Ni(OAc)2.4H2O, NaBH4 / ethanol; H2O
3: 90 percent / pyridine, CrO3 / CH2Cl2 / 0.25 h
4: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h; 2.) ether, hexane, -40 deg C, 80 min
5: acetic acid / 3 h / Ambient temperature
View Scheme
pent-1-yn-5-ol
5390-04-5

pent-1-yn-5-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1) LiNH2 / 1) NH3(l), 3 h; 2) abs THF, 20-25 deg C, 13 h.
2: 80 percent / nickel acetate, NaBH4, ethylene diamine / ethanol
3: 80 percent / pyridinium chlorochromate / CH2Cl2
4: 1) butyllithium, 2) butyllithium, 3) ethanol / 1) abs. THF, hexan, -30 deg C, 90 min; 2) abs. THF, hexan, 40 min at -60 deg C and 15 min at -30 deg C; 3) 30 min at -30 deg C and 24 h at -40 deg C.
5: 92 percent / glacial acetic acid / Heating
View Scheme
Multi-step reaction with 5 steps
1: 76 percent / LiNH2, NH3 (liquid) / tetrahydrofuran / 5 h
2: ethylene diamine, H2 / Ni(OAc)2.4H2O, NaBH4 / ethanol; H2O
3: 90 percent / pyridine, CrO3 / CH2Cl2 / 0.25 h
4: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h; 2.) ether, hexane, -40 deg C, 80 min
5: acetic acid / 3 h / Ambient temperature
View Scheme
Multi-step reaction with 6 steps
1: 81 percent / LiNH2, NH3 (liquid) / 4 h
2: H2, Na/NH3 / Ni(OAc)2.4H2O, NaBH4
3: 81 percent / triphenylphosphine, Br2, pyridine / CH2Cl2; CCl4 / Ambient temperature
4: acetonitrile / Heating
5: 1.) 2M dimsyl sodium / 1.) THF, DMSO, RT, 30 min; 2.) THF, DMSO, a.) -30 deg C up to RT, RT
6: acetic acid
View Scheme
(Z)-11-(2'-tetrahydropyranyloxy)undec-4-en-1-ol
94141-78-3

(Z)-11-(2'-tetrahydropyranyloxy)undec-4-en-1-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 80 percent / pyridinium chlorochromate / CH2Cl2
2: 1) butyllithium, 2) butyllithium, 3) ethanol / 1) abs. THF, hexan, -30 deg C, 90 min; 2) abs. THF, hexan, 40 min at -60 deg C and 15 min at -30 deg C; 3) 30 min at -30 deg C and 24 h at -40 deg C.
3: 92 percent / glacial acetic acid / Heating
View Scheme
Multi-step reaction with 3 steps
1: 90 percent / pyridine, CrO3 / CH2Cl2 / 0.25 h
2: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h; 2.) ether, hexane, -40 deg C, 80 min
3: acetic acid / 3 h / Ambient temperature
View Scheme
11-<(tetrahydro-2H-pyran-2-yl)oxy>undec-4-yn-1-ol
94141-77-2

11-<(tetrahydro-2H-pyran-2-yl)oxy>undec-4-yn-1-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 80 percent / nickel acetate, NaBH4, ethylene diamine / ethanol
2: 80 percent / pyridinium chlorochromate / CH2Cl2
3: 1) butyllithium, 2) butyllithium, 3) ethanol / 1) abs. THF, hexan, -30 deg C, 90 min; 2) abs. THF, hexan, 40 min at -60 deg C and 15 min at -30 deg C; 3) 30 min at -30 deg C and 24 h at -40 deg C.
4: 92 percent / glacial acetic acid / Heating
View Scheme
Multi-step reaction with 6 steps
1: 78 percent / pyridinium fluorochromate / CH2Cl2 / 3 h / Ambient temperature
2: 1) NaNH2 / 1) THF, HMPA, r.t., 90 min, 2) THF, r.t., 6 h
3: 90 percent / PPTS, pyridine / methanol / 2 h / Heating
4: pyridine / DMAP / 2 h / Ambient temperature
5: 1.33 g / aq.NaNO2, 6M HNO3 / 0.5 h / 70 - 75 °C
6: 94 percent / H2, quinoline / Lindlar catalyst / ethanol / 760 Torr
View Scheme
Multi-step reaction with 4 steps
1: ethylene diamine, H2 / Ni(OAc)2.4H2O, NaBH4 / ethanol; H2O
2: 90 percent / pyridine, CrO3 / CH2Cl2 / 0.25 h
3: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h; 2.) ether, hexane, -40 deg C, 80 min
4: acetic acid / 3 h / Ambient temperature
View Scheme
(Z)-11-(2'-tetrahydropyranyloxy)undec-4-en-1-al
94141-79-4

(Z)-11-(2'-tetrahydropyranyloxy)undec-4-en-1-al

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1) butyllithium, 2) butyllithium, 3) ethanol / 1) abs. THF, hexan, -30 deg C, 90 min; 2) abs. THF, hexan, 40 min at -60 deg C and 15 min at -30 deg C; 3) 30 min at -30 deg C and 24 h at -40 deg C.
2: 92 percent / glacial acetic acid / Heating
View Scheme
Multi-step reaction with 2 steps
1: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h; 2.) ether, hexane, -40 deg C, 80 min
2: acetic acid / 3 h / Ambient temperature
View Scheme
(E)-4-none-1-ol
16695-34-4

(E)-4-none-1-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 82 percent / PCC / CHCl3 / 2 h
2: 1.) PPh3, t-BuOK / 1.) 160 deg C, 8 h; THF, -30 deg C, 0.5 h, 2.) -70 deg C, 3 h; room temperature, overnight
3: 81 percent / acetic acid / 5 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 65 percent / pyridine, phosphorus tribromide / benzene / 6 h / Heating
2: tetrahydrofuran / Ambient temperature
3: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
Multi-step reaction with 4 steps
1: 81 percent / triphenylphosphine, Br2, pyridine / CH2Cl2; CCl4 / Ambient temperature
2: acetonitrile / Heating
3: 1.) 2M dimsyl sodium / 1.) THF, DMSO, RT, 30 min; 2.) THF, DMSO, a.) -30 deg C up to RT, RT
4: acetic acid
View Scheme
Multi-step reaction with 5 steps
1: (i) TsCl, Py, (ii) LiBr, DMF
2: Heating
3: dimsyl sodium / dimethylsulfoxide
4: LiAlH4 / diethyl ether
5: Py
View Scheme
1-hepten-3-ol
4938-52-7

1-hepten-3-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 77 percent / propionic acid / 2 h / 135 - 137 °C
2: 78 percent / LiAlH4 / diethyl ether / 0 - 20 °C
3: 82 percent / PCC / CHCl3 / 2 h
4: 1.) PPh3, t-BuOK / 1.) 160 deg C, 8 h; THF, -30 deg C, 0.5 h, 2.) -70 deg C, 3 h; room temperature, overnight
5: 81 percent / acetic acid / 5 h / Heating
View Scheme
Multi-step reaction with 7 steps
1: propionic acid / 145 °C
2: LiAlH4 / diethyl ether
3: (i) TsCl, Py, (ii) LiBr, DMF
4: Heating
5: dimsyl sodium / dimethylsulfoxide
6: LiAlH4 / diethyl ether
7: Py
View Scheme
(E)-non-4-enal
2277-16-9

(E)-non-4-enal

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) PPh3, t-BuOK / 1.) 160 deg C, 8 h; THF, -30 deg C, 0.5 h, 2.) -70 deg C, 3 h; room temperature, overnight
2: 81 percent / acetic acid / 5 h / Heating
View Scheme
ethyl (4E)-non-4-enoate
69361-38-2

ethyl (4E)-non-4-enoate

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 78 percent / LiAlH4 / diethyl ether / 0 - 20 °C
2: 82 percent / PCC / CHCl3 / 2 h
3: 1.) PPh3, t-BuOK / 1.) 160 deg C, 8 h; THF, -30 deg C, 0.5 h, 2.) -70 deg C, 3 h; room temperature, overnight
4: 81 percent / acetic acid / 5 h / Heating
View Scheme
Multi-step reaction with 6 steps
1: LiAlH4 / diethyl ether
2: (i) TsCl, Py, (ii) LiBr, DMF
3: Heating
4: dimsyl sodium / dimethylsulfoxide
5: LiAlH4 / diethyl ether
6: Py
View Scheme
1,7-heptandiol
629-30-1

1,7-heptandiol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 80 percent / pyridine / benzene / 6 h
2: 75 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 1.5 h
3: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
1,2-dibromohexane
624-20-4

1,2-dibromohexane

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 85 percent / potassium hydroxide, tetrabutylammonium chloride, 2,5-hexanediol / 0.5 h
2: 1.) lithium amide, liq. ammonia / 1.) THF, 1 h, 2.) THF, 2 h
3: p-toluenesulfonic acid / methanol / 24 h
4: 80 percent / LiAlH4, / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 2 h / Heating
5: 65 percent / pyridine, phosphorus tribromide / benzene / 6 h / Heating
6: tetrahydrofuran / Ambient temperature
7: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
(E)-4-nonen-1-yl bromide
16695-35-5

(E)-4-nonen-1-yl bromide

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tetrahydrofuran / Ambient temperature
2: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
Multi-step reaction with 3 steps
1: acetonitrile / Heating
2: 1.) 2M dimsyl sodium / 1.) THF, DMSO, RT, 30 min; 2.) THF, DMSO, a.) -30 deg C up to RT, RT
3: acetic acid
View Scheme
Multi-step reaction with 4 steps
1: Heating
2: dimsyl sodium / dimethylsulfoxide
3: LiAlH4 / diethyl ether
4: Py
View Scheme
4-nonyne-1-ol
49826-98-4

4-nonyne-1-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 80 percent / LiAlH4, / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 2 h / Heating
2: 65 percent / pyridine, phosphorus tribromide / benzene / 6 h / Heating
3: tetrahydrofuran / Ambient temperature
4: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
Multi-step reaction with 5 steps
1: H2, Na/NH3 / Ni(OAc)2.4H2O, NaBH4
2: 81 percent / triphenylphosphine, Br2, pyridine / CH2Cl2; CCl4 / Ambient temperature
3: acetonitrile / Heating
4: 1.) 2M dimsyl sodium / 1.) THF, DMSO, RT, 30 min; 2.) THF, DMSO, a.) -30 deg C up to RT, RT
5: acetic acid
View Scheme
acetic acid 7-hydroxyheptyl ester
59694-63-2

acetic acid 7-hydroxyheptyl ester

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 75 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 1.5 h
2: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
hex-1-yne
693-02-7

hex-1-yne

monobromohexylene

monobromohexylene

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1.) lithium amide, liq. ammonia / 1.) THF, 1 h, 2.) THF, 2 h
2: p-toluenesulfonic acid / methanol / 24 h
3: 80 percent / LiAlH4, / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 2 h / Heating
4: 65 percent / pyridine, phosphorus tribromide / benzene / 6 h / Heating
5: tetrahydrofuran / Ambient temperature
6: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
2-Non-4-ynyloxy-tetrahydro-pyran
65370-57-2

2-Non-4-ynyloxy-tetrahydro-pyran

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: p-toluenesulfonic acid / methanol / 24 h
2: 80 percent / LiAlH4, / bis-(2-methoxy-ethyl) ether; tetrahydrofuran / 2 h / Heating
3: 65 percent / pyridine, phosphorus tribromide / benzene / 6 h / Heating
4: tetrahydrofuran / Ambient temperature
5: 1.) sodium hexamethyldisilazylamide / 1.) THF, RT, 1 h, 2.) THF, from -60 to -50 deg C, 6 h
View Scheme
2-(5-bromopentyloxy)tetrahydropyran
37935-47-0

2-(5-bromopentyloxy)tetrahydropyran

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) Mg; 2.) Li2CuCl4 / 1.) THF; 2.) 5 h, -10 deg C;
2: 80 percent / acetic acid, pyridine / 12 h / Ambient temperature
View Scheme
(E)-oct-3-en-1-ol
18185-81-4, 20125-84-2, 20125-85-3

(E)-oct-3-en-1-ol

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 68 percent / PBr3, pyridine / diethyl ether / 2 h / Heating
2: 1.) ethylmagnesiumbromide, 2.) cuprous chloride / 1.) THF, 6 h, 40-50 deg C
3: 58 percent / PTS / methanol / 6 h / 55 °C
4: H2, quinoline / Lindlar's catalyst / hexane
5: PBr3, pyridine / diethyl ether
6: 1.) Mg; 2.) Li2CuCl4 / 1.) THF; 2.) 5 h, -10 deg C;
7: 80 percent / acetic acid, pyridine / 12 h / Ambient temperature
View Scheme
Multi-step reaction with 5 steps
1: 83 percent / Br2, triphenylphosphine / CCl4 / 1 h / Ambient temperature
2: 1.) Li, ferric chloride, liquid ammonia / 1.) THF, 1 h, 2.) DMSO, -35 deg C, 3 h
3: TsOH, H2O / methanol / 24 h / Ambient temperature
4: NaBH4, ethylenediamine, nickel acetate / ethanol / Ambient temperature
5: pyridine / 24 h / Ambient temperature
View Scheme
(E)-oct-3-enoic acid
5163-67-7

(E)-oct-3-enoic acid

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1: 69 percent / triethylamine / CH2Cl2 / 4 h / 0 °C
2: 68 percent / NaBH4 / ethanol / 3 h
3: 68 percent / PBr3, pyridine / diethyl ether / 2 h / Heating
4: 1.) ethylmagnesiumbromide, 2.) cuprous chloride / 1.) THF, 6 h, 40-50 deg C
5: 58 percent / PTS / methanol / 6 h / 55 °C
6: H2, quinoline / Lindlar's catalyst / hexane
7: PBr3, pyridine / diethyl ether
8: 1.) Mg; 2.) Li2CuCl4 / 1.) THF; 2.) 5 h, -10 deg C;
9: 80 percent / acetic acid, pyridine / 12 h / Ambient temperature
View Scheme
Multi-step reaction with 7 steps
1: 89 percent / TsOH / 24 h / Ambient temperature
2: 93 percent / diisobutylaluminum hydride (DIBAH) / diethyl ether; toluene / 2 h / -20 °C
3: 83 percent / Br2, triphenylphosphine / CCl4 / 1 h / Ambient temperature
4: 1.) Li, ferric chloride, liquid ammonia / 1.) THF, 1 h, 2.) DMSO, -35 deg C, 3 h
5: TsOH, H2O / methanol / 24 h / Ambient temperature
6: NaBH4, ethylenediamine, nickel acetate / ethanol / Ambient temperature
7: pyridine / 24 h / Ambient temperature
View Scheme
(E)-1-oct-3-enyl bromide
53155-10-5

(E)-1-oct-3-enyl bromide

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1.) ethylmagnesiumbromide, 2.) cuprous chloride / 1.) THF, 6 h, 40-50 deg C
2: 58 percent / PTS / methanol / 6 h / 55 °C
3: H2, quinoline / Lindlar's catalyst / hexane
4: PBr3, pyridine / diethyl ether
5: 1.) Mg; 2.) Li2CuCl4 / 1.) THF; 2.) 5 h, -10 deg C;
6: 80 percent / acetic acid, pyridine / 12 h / Ambient temperature
View Scheme
Multi-step reaction with 4 steps
1: 1.) Li, ferric chloride, liquid ammonia / 1.) THF, 1 h, 2.) DMSO, -35 deg C, 3 h
2: TsOH, H2O / methanol / 24 h / Ambient temperature
3: NaBH4, ethylenediamine, nickel acetate / ethanol / Ambient temperature
4: pyridine / 24 h / Ambient temperature
View Scheme
C11H18O4
126629-19-4

C11H18O4

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: 68 percent / NaBH4 / ethanol / 3 h
2: 68 percent / PBr3, pyridine / diethyl ether / 2 h / Heating
3: 1.) ethylmagnesiumbromide, 2.) cuprous chloride / 1.) THF, 6 h, 40-50 deg C
4: 58 percent / PTS / methanol / 6 h / 55 °C
5: H2, quinoline / Lindlar's catalyst / hexane
6: PBr3, pyridine / diethyl ether
7: 1.) Mg; 2.) Li2CuCl4 / 1.) THF; 2.) 5 h, -10 deg C;
8: 80 percent / acetic acid, pyridine / 12 h / Ambient temperature
View Scheme
Dimethyldisulphide
624-92-0

Dimethyldisulphide

1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

2-<1-acetoxy-7-(methylthio)heptan-7-yl>-5-<1-(methylthio)pentan-1-yl>tetrahydrothiophene
105836-08-6

2-<1-acetoxy-7-(methylthio)heptan-7-yl>-5-<1-(methylthio)pentan-1-yl>tetrahydrothiophene

Conditions
ConditionsYield
With iodine at 50℃; for 5h;80%
1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

(7Z,11E)-hexadeca-7,11-dien-1-ol
53963-09-0

(7Z,11E)-hexadeca-7,11-dien-1-ol

Conditions
ConditionsYield
With potassium carbonate In methanol
1-acetoxyhexadeca-7Z,11E-diene
53042-79-8

1-acetoxyhexadeca-7Z,11E-diene

(7Z,11E)-7,11-hexadecadienal

(7Z,11E)-7,11-hexadecadienal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / methanol
2: pyridinium chlorochromate / CH2Cl2
View Scheme

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