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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3,6-Dibromo-9,10-phenanthrenequinone Manufacturer/High quality/Best price/In stock

Cas:53348-05-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3,6-Dibromo-Phenanthrenequinone

Cas:53348-05-3

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 53348-05-3 3,6-dibromo-phenanthrene-9,10-dione Manufacturer

Cas:53348-05-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Now we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti

53348-05-3

Cas:53348-05-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 53348-05-3 with competitive price

Cas:53348-05-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

3,6-dibromo-phenanthrene-9,10-dione 53348-05-3

Cas:53348-05-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Pharmaceutical Intermediate, 3,6-Dibromo-phenanthrenequinone CAS:53348-05-3

Cas:53348-05-3

Min.Order:1 Kilogram

FOB Price: $142.0 / 148.0

Type:Trading Company

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

3,6-dibromo-phenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

3,6-dibromo-phenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qua

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3,6-dibromo-phenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: 3,6-Dibromo-phenanthrenequinone Synonyms: 3,6-Dibromo-9,10-phenanthrenequinone;3,6-Dibromophenanthrene-9,10-dione;3,6-DibroMo-phenanthrenequ;3,6-Dibromo-9,10-dihydrophenanthrene-9,10-dione;3,6-Dibromo-9,10-phenanthrenedione;3,6-Di

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Henan Kanbei Chemical Co.,LTD

High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle

3,6-Dibromo-phenanthrenequinone 99%

Cas:53348-05-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Our company advantages: 1 The highest quality with the competitive price. 2、 Professional human services. 3、 The fastest and safest delivery service. 4、Our old customers all around the world. 5、 The high purity products. 6、We have a suf

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

53348-05-3 CAS NO.53348-05-3

Cas:53348-05-3

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

3,6-Dibromo-9,10-phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3,6-dibromophenanthrene-9,10-dione cas no. 53348-05-3 98%

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:1 Gram

Negotiable

Type:Manufacturers

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3,6-dibromophenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

3,6-DibroMophenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

3,6-Dibromophenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

3,6-Dibromo-Phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

3,6-Dibromophenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

3,6-dibroMo-phenanthrene-9,10-dione

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

3,6-Dibromo-Phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

3,6-Dibromo-phenanthrenequinone

Cas:53348-05-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

9,10-phenanthrenequinone
84-11-7

9,10-phenanthrenequinone

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
With bromine; dibenzoyl peroxide In nitrobenzene at 110℃; for 16h;95%
With bromine; dibenzoyl peroxide In nitrobenzene at 60℃; UV-irradiation;92%
With bromine; dibenzoyl peroxide In nitrobenzene at 120℃; for 1h;91%
2,9-dibromophenanthrene
174735-02-5

2,9-dibromophenanthrene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
With chromium(VI) oxide; acetic acid for 1h; Reflux; Inert atmosphere;78%
3-bromo-phenanthrene-quinone-(9.10)

3-bromo-phenanthrene-quinone-(9.10)

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
With bromine; nitrobenzene at 100 - 110℃;
phenanthrene
85-01-8

phenanthrene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium dichromate; sulfuric acid / water / 85 - 115 °C
2: bromine; dibenzoyl peroxide / nitrobenzene / 1 h / 75 °C / Irradiation
View Scheme
1-bromo-4-ethenyl-benzene
2039-82-9

1-bromo-4-ethenyl-benzene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium acetate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) / N,N-dimethyl acetamide / 48 h / 100 - 140 °C / Schlenk technique; Inert atmosphere
2: iodine / toluene / Irradiation; Inert atmosphere
3: chromium(VI) oxide; acetic acid / 1 h / Reflux; Inert atmosphere
View Scheme
4-bromo-benzaldehyde
1122-91-4

4-bromo-benzaldehyde

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: potassium carbonate / 1,2-dimethoxyethane / 1 h / Inert atmosphere
1.2: 24 h / 80 °C / Inert atmosphere
2.1: sodium acetate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) / N,N-dimethyl acetamide / 48 h / 100 - 140 °C / Schlenk technique; Inert atmosphere
3.1: iodine / toluene / Irradiation; Inert atmosphere
4.1: chromium(VI) oxide; acetic acid / 1 h / Reflux; Inert atmosphere
View Scheme
(E)-4,4'-dibromostilbene
18869-30-2

(E)-4,4'-dibromostilbene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: iodine / toluene / Irradiation; Inert atmosphere
2: chromium(VI) oxide; acetic acid / 1 h / Reflux; Inert atmosphere
View Scheme
3,6-dibromophenanthrene-9,10-diamine chloride

3,6-dibromophenanthrene-9,10-diamine chloride

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6,12,15-tetrabromo-tetrabenzophenazine

3,6,12,15-tetrabromo-tetrabenzophenazine

Conditions
ConditionsYield
With acetic acid; triethylamine In ethanol at 100 - 130℃; for 6h; Inert atmosphere;100%
3-phenyl-1-(1H-pyrazol-1-yl)but-3-en-1-one

3-phenyl-1-(1H-pyrazol-1-yl)but-3-en-1-one

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

A

(R)-3,6-dibromo-4′-phenyl-10H-spiro[phenanthrene-9,2′-pyran]-6′,10(3′H)-dione

(R)-3,6-dibromo-4′-phenyl-10H-spiro[phenanthrene-9,2′-pyran]-6′,10(3′H)-dione

B

(S)-3,6-dibromo-4′-phenyl-10H-spiro[phenanthrene-9,2′-pyran]-6′,10(3′H)-dione

(S)-3,6-dibromo-4′-phenyl-10H-spiro[phenanthrene-9,2′-pyran]-6′,10(3′H)-dione

Conditions
ConditionsYield
With C26H26F5N3S In dichloromethane at 25℃; for 6h; enantioselective reaction;A 99%
B n/a
dimethyl sulfate
77-78-1

dimethyl sulfate

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromo-9,10-bis-methoxyphenanthrene
888728-75-4

3,6-dibromo-9,10-bis-methoxyphenanthrene

Conditions
ConditionsYield
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water Inert atmosphere;
Stage #2: dimethyl sulfate With sodium hydroxide In tetrahydrofuran; water Cooling with ice; Inert atmosphere;
98%
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water for 0.0833333h;
Stage #2: dimethyl sulfate With sodium hydroxide In tetrahydrofuran; water for 0.25h; Cooling with ice;
92%
With sodium hydroxide; sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water for 0.25h;90%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,4-diaminobenzoic acid
619-05-6

3,4-diaminobenzoic acid

2,7-dibromodibenzo[a,c]phenazine-11-carboxylic acid
1616777-39-9

2,7-dibromodibenzo[a,c]phenazine-11-carboxylic acid

Conditions
ConditionsYield
With acetic acid In ethanol for 2h; Reflux;98%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

4,5-diaminophthalonitrile
129365-93-1

4,5-diaminophthalonitrile

3,6-dibromodibenzo[a,c]phenazine-11,12-dicarbonitrile

3,6-dibromodibenzo[a,c]phenazine-11,12-dicarbonitrile

Conditions
ConditionsYield
With acetic acid In ethanol; 1,2-dichloro-benzene for 48h; Sealed tube; Reflux;98%
With acetic acid for 8h; Inert atmosphere; Schlenk technique; Reflux;92%
1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromodibenzo[a,c]phenazine
112865-07-3

3,6-dibromodibenzo[a,c]phenazine

Conditions
ConditionsYield
With acetic acid In methanol for 3h; Reflux;97%
With acetic acid In ethanol for 3h; Reflux; Inert atmosphere;96%
With acetic acid In ethanol at 80℃; for 4h;91%
With acetic acid
2,6-dibromobenzaldehyde
67713-23-9

2,6-dibromobenzaldehyde

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

6,9-dibromo-2-(2,6-dibromophenyl)-1H-phenanthro[9,10-d]imidazole
892550-50-4

6,9-dibromo-2-(2,6-dibromophenyl)-1H-phenanthro[9,10-d]imidazole

Conditions
ConditionsYield
With ammonium acetate; acetic acid In water; toluene for 22h; Heating / reflux;97%
With ammonium acetate; acetic acid for 16h; Heating / reflux;97%
With ammonium acetate In acetic acid for 16h; Heating / reflux;97%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

4,5-dibromo-1,2-diaminobenzene
49764-63-8

4,5-dibromo-1,2-diaminobenzene

3,6,11,12-tetrabromodibenzo[a,c]phenazine

3,6,11,12-tetrabromodibenzo[a,c]phenazine

Conditions
ConditionsYield
In ethanol for 10h; Reflux; Inert atmosphere;96%
With acetic acid at 110℃; for 6h; Temperature;90%
With acetic acid at 110℃; for 3h; Inert atmosphere;
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

2,9-dibromo-5,6-dihydroxyphenanthrene
952054-63-6

2,9-dibromo-5,6-dihydroxyphenanthrene

Conditions
ConditionsYield
With sodium dithionite In tetrahydrofuran; water at 20℃; for 6h; Inert atmosphere;95%
With sodium dithionite In N,N-dimethyl-formamide for 0.25h;
With sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water for 0.5h;
With sodium dithionite In tetrahydrofuran; water at 20℃; for 6h;1.4 g
With sodium dithionite In tetrahydrofuran; water at 20℃; for 6h; Inert atmosphere;
1,2-diamine-3,6-dibromobenzene
69272-50-0

1,2-diamine-3,6-dibromobenzene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6,10,13-tetrabromophenanthridine

3,6,10,13-tetrabromophenanthridine

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 100℃; for 4h;95%
With sodium hydroxide In ethanol at 100℃; for 4h;95%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

4-Bromo-benzene-1,2-diamine
1575-37-7

4-Bromo-benzene-1,2-diamine

3,6,11‑tribromodibenzo[a,c]phenazine

3,6,11‑tribromodibenzo[a,c]phenazine

Conditions
ConditionsYield
In ethanol at 100℃; for 2h; Inert atmosphere;95%
With acetic acid at 110℃; for 6h; Temperature;95%
With acetic acid for 3h; Reflux;93%
terephthalaldehyde,
623-27-8

terephthalaldehyde,

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

4-(6,9-dibromo-1H-phenanthro[9,10-d]imidazol-2-yl)benzaldehyde

4-(6,9-dibromo-1H-phenanthro[9,10-d]imidazol-2-yl)benzaldehyde

Conditions
ConditionsYield
With ammonium acetate; acetic acid for 8h; Reflux; Inert atmosphere;95%
2-amino-4,5-difluoroaniline
76179-40-3

2-amino-4,5-difluoroaniline

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromo-11,12-difluorodibenzo[a,c]phenazine

3,6-dibromo-11,12-difluorodibenzo[a,c]phenazine

Conditions
ConditionsYield
In ethanol at 80℃; for 2h; Inert atmosphere;95%
4-benzoylbenzene-1,2-diamine
39070-63-8

4-benzoylbenzene-1,2-diamine

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

(3,6-dibromodibenzo[a,c]phenazin-11-yl)(phenyl)methanone

(3,6-dibromodibenzo[a,c]phenazin-11-yl)(phenyl)methanone

Conditions
ConditionsYield
With acetic acid for 3h; Reflux;93%
With acetic acid for 8h; Reflux;83%
1,2-diaminopropan
78-90-0, 10424-38-1

1,2-diaminopropan

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

C17H10Br2N2

C17H10Br2N2

Conditions
ConditionsYield
Stage #1: 1,2-diaminopropan; 3,6-dibromo-phenanthrene-9,10-dione In toluene for 24h; Reflux;
Stage #2: With manganese(IV) oxide In toluene at 93℃; for 0.75h; Solvent; Inert atmosphere;
92%
ethylene glycol
107-21-1

ethylene glycol

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromophenanthren-9,10-di(ethyleneglycol)ketal
887127-61-9

3,6-dibromophenanthren-9,10-di(ethyleneglycol)ketal

Conditions
ConditionsYield
With 10-camphorsufonic acid In methanol at 120℃; for 3h; Inert atmosphere;91%
With toluene-4-sulfonic acid In toluene at 140℃; for 14h;75%
With camphor-10-sulfonic acid In methanol at 120 - 130℃; for 24h;60%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

[4-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)phenyl]diphenylamine
408359-97-7

[4-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)phenyl]diphenylamine

3,6-bis[4-(diphenylamino)phenyl]-9,10-phenanthrenequinone
1415100-79-6

3,6-bis[4-(diphenylamino)phenyl]-9,10-phenanthrenequinone

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 60 - 85℃; for 16h; Inert atmosphere;91%
ethyl 3,4-diaminobenzoate
37466-90-3

ethyl 3,4-diaminobenzoate

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

ethyl 2,7-dibromodibenzo[a,c]phenazine-11-carboxylate
1616777-40-2

ethyl 2,7-dibromodibenzo[a,c]phenazine-11-carboxylate

Conditions
ConditionsYield
With acetic acid In ethanol for 2h; Reflux;91%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

C26H30B2O6

C26H30B2O6

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In N,N-dimethyl-formamide at 150℃; for 10h; Inert atmosphere;90%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane for 3h; Inert atmosphere; Reflux;86%
4-tert-Butylbenzaldehyde
939-97-9

4-tert-Butylbenzaldehyde

aniline
62-53-3

aniline

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

C31H24Br2N2

C31H24Br2N2

Conditions
ConditionsYield
With ammonium acetate; acetic acid at 120℃; for 4h; Inert atmosphere;90%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6‐dibromo‐2‐iodophenanthrene‐9,10‐dione

3,6‐dibromo‐2‐iodophenanthrene‐9,10‐dione

Conditions
ConditionsYield
With N-iodo-succinimide; sulfuric acid; trifluoroacetic acid at 50℃; for 72h; Inert atmosphere; Schlenk technique; chemoselective reaction;90%
2,3-Diaminonaphthalene
771-97-1

2,3-Diaminonaphthalene

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromotribenzo[a,c,i]phenazine

3,6-dibromotribenzo[a,c,i]phenazine

Conditions
ConditionsYield
With acetic acid Reflux;89%
With acetic acid for 3h; Reflux;
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromofluoren-9-one
216312-73-1

3,6-dibromofluoren-9-one

Conditions
ConditionsYield
With potassium permanganate; potassium hydroxide In water at 130℃; for 1h; Inert atmosphere;88%
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With potassium hydroxide In water at 130℃; for 0.5h;
Stage #2: With potassium permanganate In water at 130℃; for 3h;
72%
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With potassium hydroxide In water at 130℃; for 0.5h;
Stage #2: With potassium permanganate at 130℃; for 78h;
72%
3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

9,9-dioctylfluorene-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
302554-81-0

9,9-dioctylfluorene-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

3,6-bis(9',9'-dioctylfluoren-2'-yl)-9,10-phenanthraquinone
1174669-48-7

3,6-bis(9',9'-dioctylfluoren-2'-yl)-9,10-phenanthraquinone

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; water Suzuki coupling; Reflux;88%
1-bromo-hexane
111-25-1

1-bromo-hexane

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6-dibromo-9,10-bis(hexyloxy)phenanthrene
1029694-69-6

3,6-dibromo-9,10-bis(hexyloxy)phenanthrene

Conditions
ConditionsYield
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 1-bromo-hexane With potassium hydroxide In tetrahydrofuran; water at 80℃; for 3h; Inert atmosphere;
88%
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With sodium dithionite In N,N-dimethyl-formamide for 0.25h; Inert atmosphere;
Stage #2: 1-bromo-hexane With tetrabutylammomium bromide; potassium hydroxide In N,N-dimethyl-formamide at 60℃; for 60h; Inert atmosphere;
42%
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water Inert atmosphere;
Stage #2: 1-bromo-hexane With potassium hydroxide In tetrahydrofuran; water at 20℃; for 48h; Inert atmosphere;
Stage #1: 3,6-dibromo-phenanthrene-9,10-dione With sodium dithionite; tetrabutylammomium bromide In tetrahydrofuran; water for 1h;
Stage #2: 1-bromo-hexane With potassium hydroxide In tetrahydrofuran; water at 25℃; for 48h;
2,3-Diamino-6-bromopyridine
129012-04-0

2,3-Diamino-6-bromopyridine

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

3,6,11-tribromodibenzo[f,h]pyrido[2,3-b]quinoxaline

3,6,11-tribromodibenzo[f,h]pyrido[2,3-b]quinoxaline

Conditions
ConditionsYield
In ethanol at 90℃; Inert atmosphere;88%
tert-butyl 2-oxo-3-(propan-2-ylidene)indoline-1-carboxylate
1374605-89-6

tert-butyl 2-oxo-3-(propan-2-ylidene)indoline-1-carboxylate

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

tert-butyl (2-(3,6-dibromo-4′-methyl-6′,10-dioxo-3′,6′-dihydro-10H-spiro[phenanthrene-9,2′-pyran]-5′-yl)phenyl)carbamate

tert-butyl (2-(3,6-dibromo-4′-methyl-6′,10-dioxo-3′,6′-dihydro-10H-spiro[phenanthrene-9,2′-pyran]-5′-yl)phenyl)carbamate

Conditions
ConditionsYield
With 3-((3,5-bis(trifluoromethyl)phenyl)amino)-4-(((S)-(6-methoxyquinoline-4-yl))((1S,2S,4S,5R-5-vinylquinuclidine-2-yl)methyl)amino)cyclobutan-3-ene-1,2-dione In dichloromethane at 20℃; for 24h; enantioselective reaction;88%
2-chloro-6-fluorobenzaldehyde
387-45-1

2-chloro-6-fluorobenzaldehyde

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

6,9-dibromo-2-(2-chloro-6-fluorophenyl)-1H-phenanthro[9,10-d]imidazole
892550-42-4

6,9-dibromo-2-(2-chloro-6-fluorophenyl)-1H-phenanthro[9,10-d]imidazole

Conditions
ConditionsYield
With ammonium bicarbonate In acetic acid at 130℃;87%
With ammonium bicarbonate; acetic acid In water; toluene at 20 - 130℃; Heating / reflux;80%
With ammonium bicarbonate; acetic acid at 130℃; Heating / reflux;80%
With ammonium bicarbonate In acetic acid at 130℃;80%
terephthalaldehyde,
623-27-8

terephthalaldehyde,

4-methoxy-aniline
104-94-9

4-methoxy-aniline

3,6-dibromo-phenanthrene-9,10-dione
53348-05-3

3,6-dibromo-phenanthrene-9,10-dione

4-(6,9-dibromo-1-(4-methoxyphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)benzaldehyde

4-(6,9-dibromo-1-(4-methoxyphenyl)-1H-phenanthro[9,10-d]imidazol-2-yl)benzaldehyde

Conditions
ConditionsYield
With ammonium acetate; acetic acid for 18h; Reflux; Inert atmosphere;87%
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