CAS No.5376-10-3,(1-BENZYL-1H-IMIDAZOL-2-YL)METHANOL Suppliers

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BUTTPARK 29\04-90; 1-BENZYL-2-(HYDROXYMETHYL)IMIDAZOLE;(1-BENZYL-1H-IMIDAZOL-2-YL)METHANOL; 1-Benzyl-2-(hydroxymethyl)-1H-imidazole 97%;1 -Benzyl-2-(hydroxymethyl)-1H-imidazole; 1-Benzyl-1H-imidazole-2-methanol; (1-Benzyl-1H-imidazol-2-yl)methanol

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Synthetic route

: 10045-65-5
N-benzylimidazole-2-carboxaldehyde

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

Conditions

Conditions	Yield
With sodium tetrahydroborate In methanol at 0℃; for 2.5h;	93.1%
With sodium tetrahydroborate In methanol at 0℃; for 2.5h;
With methanol; sodium tetrahydroborate at 0 - 20℃;

: 4238-71-5
1-benzylimidazole

: 50-00-0
formaldehyd

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

Conditions

Conditions	Yield
In water at 150℃; for 3h;	92%
In water for 72h; Heating;	56%
In 1,4-dioxane at 135℃; under 5250.53 Torr; for 20h; Autoclave;	50%

: 4238-71-5
1-benzylimidazole

: 50-00-0
formaldehyd

A: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

B: 115960-26-4
1-benzylimidazole-2,5-dimethanol

C: 118599-62-5
1-benzylimidazole-2,4,5-trimethanol

Conditions

Conditions	Yield
With sodium acetate In water; acetic acid at 140℃; for 12h;	A 10% B 20% C 5%

...Expand

: 4238-71-5
1-benzylimidazole

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 1.) n-BuLi / 1.) Et2O, hexane, -45 deg C, 30 min, 2 a.) -75 deg C, b.) 0 deg C, 10 min 2: NaBH4 / methanol / 2.5 h / 0 °C View Scheme
With sodium hydroxide; formaldehyd
With sodium hydroxide; formaldehyd

: 23269-10-5
1-benzyl-1H-imidazole-2-thione

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: aqueous HNO3 View Scheme

: 61190-10-1
N-benzyl-N-(2,2-diethoxyethyl)amine

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: ethanol; aqueous HCl 2: aqueous HNO3 View Scheme
Multi-step reaction with 3 steps 1: ethanol; aqueous HCl 2: aqueous HNO3 View Scheme

: 100-39-0
benzyl bromide

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: potassium hydroxide / acetone / 2 h 2: sodium tetrahydroborate / methanol / 2.5 h / 0 °C View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 19276-03-0
1-(phenylmethyl)-2-chloromethyl-1H-imidazole monohydrochloride

Conditions

Conditions	Yield
With thionyl chloride In chloroform for 2h; Heating;	95%
Multi-step reaction with 2 steps 1: HCl / CH2Cl2 2: SOCl2 / 0.5 h / Ambient temperature View Scheme
With thionyl chloride In dichloromethane
With thionyl chloride In dichloromethane

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: cadmium(II) nitrate tetrhydrate

: [Cd(1-benzyl-2-hydroxymethylimidazole)4](NO3)2(H2O)2

Conditions

Conditions	Yield
In methanol; water soln. of ligand in MeOH stirred with aq. soln. of metal salt in molar ratio of 4:1; crystd. at room temp. for 1 wk, filtered, dried in vac.; elem. anal.;	88%

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 110-75-8
2-chloroetyl vinyl ether

: 959857-27-3
1-benzyl-2-(vinyloxyethyloxymethyl)imidazole

Conditions

Conditions	Yield
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water; toluene at 90℃; for 24h;	87%
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In toluene at 90℃; for 24h;	85%

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: silver nitrate

: tetrakis(2-hydroxymethyl-N-benzylimidazole)disilver(I) nitrate

Conditions

Conditions	Yield
In ethanol stoich., stirred at room temp. for 24 h; filtred, ethyl acetate added, slowly evapd.: elem. anal.;	72.8%

: zinc(II) nitrate hexahydrate

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: [Zn(1-benzyl-2-hydroxymethylimidazole)4](NO3)2*1.5H2O

Conditions

Conditions	Yield
In methanol; water soln. of ligand in MeOH stirred for 4 h with aq. soln. of metal salt in molar ratio of 4:1; crystd. at room temp. for 2 wk, filtered, dried in vac.; elem. anal.;	72%

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 202931-56-4
6-chloro-3-phenyl-7,8,9,10-tetrahydro-(7,10-ethano)-1,2,4-triazolo[3,4-a]phthalazine

: 6-(1-benzylimidazol-2-yl)methyloxy-3-phenyl-7,8,9,10-tetrahydro-(7,10-ethano)-1,2,4-triazolo[3,4-a]phthalazine

Conditions

Conditions	Yield
Stage #1: 1-benzyl-2-(hydroxymethyl)imidazole With sodium hydride In N,N-dimethyl-formamide at 20℃; Stage #2: 6-chloro-3-phenyl-7,8,9,10-tetrahydro-(7,10-ethano)-1,2,4-triazolo[3,4-a]phthalazine In N,N-dimethyl-formamide at 20℃;	67%

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 156-57-0
2-mercaptoethylamine hydrochloride

: 141995-51-9
2-<<(1-benzylimidazol-2-yl)methyl>thio>ethanamine dihydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In isopropyl alcohol for 5h; Heating;	65%

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1-benzyl-2-[(tertiary-butyldimethylsilanyloxy)methyl]-1H-imidazole

Conditions

Conditions	Yield
With 1H-imidazole In N,N-dimethyl-formamide at 25 - 30℃;	47.5%

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 3724-26-3
2-hydroxymethyl-1H-imidazole

Conditions

Conditions	Yield
With ammonia; sodium

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 16042-26-5
1-(phenylmethyl)-1H-imidazole-2-carboxylic acid

Conditions

Conditions	Yield
With potassium permanganate

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 74104-89-5
p-nitrophenyl picolinate

: 100-02-7
4-nitro-phenol

Conditions

Conditions	Yield
With potassium nitrate In water at 25℃; Rate constant; Mechanism; 2,6-lutidine-HNO3 buffer, pH:7.06; add. of CTABr in EtOH and/or Zn(II);

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 58610-70-1
1-benzyl-2-imidazolylmethyl chloride

Conditions

Conditions	Yield
With sulfuryl dichloride
With thionyl chloride
With thionyl chloride

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 5272-57-1
1-benzyl-2-(hydroxymethyl)imidazole hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In dichloromethane

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 1-benzyl-2-(N-hydroxymethylaminomethyl)imidazole

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 2: Na2CO3 / methanol; H2O View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 83219-46-9
1,6-bis(N-benzylimidazol-2-yl)-2,5-dithiahexane

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: 95 percent / SOCl2 / CHCl3 / 2 h / Heating 2: 97 percent / dimethylformamide / 1 h / 80 °C 3: 85 percent / aq. NaOH / 1.17 h / Heating 4: 44 percent / ethanol / 4.5 h / Heating View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 83219-47-0
2-(1-Benzyl-1H-imidazol-2-ylmethyl)-isothiourea; hydrochloride

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 95 percent / SOCl2 / CHCl3 / 2 h / Heating 2: 97 percent / dimethylformamide / 1 h / 80 °C View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 83219-48-1
Sodium; (1-benzyl-1H-imidazol-2-yl)-methanethiolate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 95 percent / SOCl2 / CHCl3 / 2 h / Heating 2: 97 percent / dimethylformamide / 1 h / 80 °C 3: 85 percent / aq. NaOH / 1.17 h / Heating View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 141995-60-0
N-Benzoyl-N'-[2-(1-benzyl-1H-imidazol-2-ylmethylsulfanyl)-ethyl]-N''-[3-(1H-imidazol-4-yl)-propyl]-guanidine

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 65 percent / conc. HCl / propan-2-ol / 5 h / Heating 2: 2) pyridine / 1) CH2Cl2, RT, 15 min, 2) 1-2h, reflux View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 141995-50-8
N-[2-(1-Benzyl-1H-imidazol-2-ylmethylsulfanyl)-ethyl]-N'-[3-(1H-imidazol-4-yl)-propyl]-guanidine; hydrochloride

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 65 percent / conc. HCl / propan-2-ol / 5 h / Heating 2: 2) pyridine / 1) CH2Cl2, RT, 15 min, 2) 1-2h, reflux 3: 80 percent / 20percent HCl / Heating View Scheme

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: 85102-36-9
1-Benzyl-2-morpholinomethylimidazole

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: HCl / CH2Cl2 2: SOCl2 / 0.5 h / Ambient temperature 3: ethanol View Scheme

: cobalt(II) nitrate hexahydrate

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: trans(O)-[tetrakis(1-benzyl-2-hydroxymethylimidazole)cobalt(II)] nitrate

Conditions

Conditions	Yield
In further solvent(s) Co:ligand 1:6 molar ratio, a soln. of ligand added dropwise to a soln. of Co salt (trimethyl orthoformate), left to stand for a few d; crysts. filtered, washed (cold diethyl ether), dried (3 d, vac.); elem. anal.;

: cobalt(II) nitrate hexahydrate

: 5376-10-3
1-benzyl-2-(hydroxymethyl)imidazole

: cis(O)-[tetrakis(1-benzyl-2-hydroxymethylimidazole)cobalt(II)] nitrate hydrate

Conditions

Conditions	Yield
In further solvent(s) Co:ligand 1:4 molar ratio, a soln. of ligand added dropwise to a soln. of Co salt (trimethyl orthoformate), left to stand for a few d; crysts. filtered, washed (cold diethyl ether), dried (3 d, vac.); elem. anal.;

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