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Cas:550-89-0
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Min.Order:1 Gram
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Type:Lab/Research institutions
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Min.Order:1 Gram
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Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:10 Gram
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Type:Lab/Research institutions
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Min.Order:0
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Min.Order:1 Metric Ton
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Type:Trading Company
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Conditions | Yield |
---|---|
With thionyl chloride und anschliessend Behandeln mit konz.wss.NH3; | |
Multi-step reaction with 2 steps 1: concentrated H2SO4 2: concentrated aqueous NH3 View Scheme | |
Multi-step reaction with 2 steps 1: methanol / 20 °C / Darkness 2: ammonia / methanol / 20 °C View Scheme |
Conditions | Yield |
---|---|
With ammonium hydroxide | |
With ammonia In methanol at 20℃; | 11.4 mg |
5,10-dihydro-phenazine-1-carboxylic acid amide
phenazine-1-carboxamide
Conditions | Yield |
---|---|
at 200℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: KOH / 145 - 160 °C 2: concentrated H2SO4 3: concentrated aqueous NH3 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: KOH / 145 - 160 °C 2: concentrated H2SO4 3: concentrated aqueous NH3 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N-ethylmorpholine;; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere 2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere 3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere 4: ammonia / water; dichloromethane / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1: N-ethylmorpholine;; 2.3-butanediol; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere 2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere 3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere 4: ammonium hydroxide / water; dichloromethane / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: copper(l) chloride; copper; N-ethylmorpholine; / 15 h / 70 °C 2.1: sodium hydroxide; sodium tetrahydroborate / 5 h / Reflux 3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Cooling with ice; Inert atmosphere 3.2: 0.5 h / 0 °C View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
With ammonia In dichloromethane; water at 20℃; Inert atmosphere; | 100 mg |
With ammonium hydroxide In dichloromethane; water at 20℃; Inert atmosphere; | 100 mg |
With ammonia; triethylamine In dichloromethane at 0℃; Reflux; |
6-nitrodiphenylamine-2-carboxylic acid
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere 2: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere 3: ammonia / water; dichloromethane / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere 2: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere 3: ammonium hydroxide / water; dichloromethane / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydroxide; sodium tetrahydroborate / 5 h / Reflux 2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Cooling with ice; Inert atmosphere 2.2: 0.5 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N-ethylmorpholine;; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere 2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere 3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere 4: ammonia / water; dichloromethane / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1: N-ethylmorpholine;; 2.3-butanediol; copper(l) chloride; copper / 16 h / 70 °C / Inert atmosphere 2: sodium tetrahydroborate; sodium ethanolate / ethanol / 24 h / 65 °C / Inert atmosphere 3: thionyl chloride / toluene / 4 h / 65 °C / Inert atmosphere 4: ammonium hydroxide / water; dichloromethane / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: copper(l) chloride; copper; N-ethylmorpholine; / 15 h / 70 °C 2.1: sodium hydroxide; sodium tetrahydroborate / 5 h / Reflux 3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Cooling with ice; Inert atmosphere 3.2: 0.5 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: phenazine-1-carboxamide With bromine; sodium methylate In tetrahydrofuran; methanol at -78 - 55℃; for 75h; Stage #2: With sodium hydroxide In methanol; water at 90℃; for 4h; | 82% |
With sodium hypobromide; water |
Conditions | Yield |
---|---|
at 130℃; for 1h; | 68% |
phenazine-1-carboxamide
5,10-dihydro-phenazine-1-carboxylic acid amide
phenazine-1-carboxamide; compound with 5,10-dihydro-phenazine-1-carboxylic acid amide
Conditions | Yield |
---|---|
With ethanol | |
With acetic acid |
phenazine-1-carboxamide
5,10-dihydro-phenazine-1-carboxylic acid amide
phenazine-1-carboxamide; compound with 5,10-dihydro-phenazine-1-carboxylic acid amide
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
With palladium Hydrogenation.und anschliessenden Erhitzen; |
Conditions | Yield |
---|---|
With palladium Hydrogenation.und anschliessenden Erhitzen in Gegenwart von ZnCl2; |
Conditions | Yield |
---|---|
With potassium hydroxide | |
With hydrogenchloride | |
With sulfuric acid | |
With water Acidic conditions; |
phenazine-1-carboxamide
5,10-dihydro-phenazine-1-carboxylic acid amide
Conditions | Yield |
---|---|
With acetic acid; zinc | |
With methanol; palladium Hydrogenation; | |
With methanol; nickel Hydrogenation; |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
With acetic anhydride; palladium Hydrogenation; |
phenazine-1-carboxamide
phenazine-1-carboxamide; compound with 5,10-dihydro-phenazine-1-carboxylic acid amide
Conditions | Yield |
---|---|
With water; zinc | |
Multi-step reaction with 2 steps 1: Raney nickel; methanol / Hydrogenation 2: ethanol View Scheme |
Conditions | Yield |
---|---|
Hydrogenation; |
Conditions | Yield |
---|---|
Hydrogenation; |
Conditions | Yield |
---|---|
Hydrogenation; |
phenazine-1-carboxamide
phenazine-1-carboxamide; compound with 5,10-dihydro-phenazine-1-carboxylic acid amide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Raney nickel; methanol / Hydrogenation 2: ethanol View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium methylate; bromine / methanol; tetrahydrofuran / 75 h / -78 - 55 °C 1.2: 4 h / 90 °C 2.1: N-ethyl-N,N-diisopropylamine; dmap / 16 h / 20 °C View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium methylate; bromine / methanol; tetrahydrofuran / 75 h / -78 - 55 °C 1.2: 4 h / 90 °C 2.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 16.08 h / 0 - 20 °C 3.1: dichloromethane / 19.5 h / 20 - 50 °C View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium methylate; bromine / methanol; tetrahydrofuran / 75 h / -78 - 55 °C 1.2: 4 h / 90 °C 2.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 16.08 h / 0 - 20 °C View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium methylate; bromine / methanol; tetrahydrofuran / 75 h / -78 - 55 °C 1.2: 4 h / 90 °C 2.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 16.08 h / 0 - 20 °C 3.1: dichloromethane / 19.5 h / 20 - 50 °C 4.1: triethylamine / dichloromethane 4.2: chromolith View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium methylate; bromine / methanol; tetrahydrofuran / 75 h / -78 - 55 °C 1.2: 4 h / 90 °C 2.1: pyridine / 16.08 h / 0 - 20 °C View Scheme |
phenazine-1-carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium methylate; bromine / methanol; tetrahydrofuran / 75 h / -78 - 55 °C 1.2: 4 h / 90 °C 2.1: pyridine / 16.08 h / 0 - 20 °C 3.1: chloroform / 23 h / 20 - 70 °C 3.2: 24 h / 20 °C / Reflux 3.3: chromolith View Scheme |
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