With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:56105-81-8
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inquiry(2R)-2-(3-benzoylphenyl)propanoic acid CAS:56105-81-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:56105-81-8
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inquiry(2R)-2-(3-benzoylphenyl)propanoic acid Basic information Product Name: (2R)-2-(3-benzoylphenyl)propanoic acid Synonyms: (2R)-2-(3-benzoylphenyl)propanoic acid;(2R)-2-(3-Benzoylphenyl)propionic acid;(R)-2-(3-Benzoylphenyl)propionic acid;(R)-3-Be
Cas:56105-81-8
Min.Order:1 Milligram
Negotiable
Type:Lab/Research institutions
inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryBenzeneacetic acid,3-benzoyl-a-methyl-, (aR)-Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:56105-81-8
Min.Order:0
Negotiable
Type:Trading Company
inquiryUnited Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Cas:56105-81-8
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Type:Lab/Research institutions
inquiryShaanxi Cuicheng Biomedical Technology Co., Ltd. is located in Chuangzhi Industrial Park, Economic and Technological Development Zone, Hanzhong City, Shaanxi Province, China. It is a company specializing in natural medicines and high-throughput scree
The system can just identify the products information in first sheet, it is not be permitted to add or edit new sheet by userself.Our products are required in MG to Gram only. · Pharmaceutical Reference Standards· Traceable workin
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the (R)-(-)-Ketoprofen, CAS:56105-81-8 with the most competitive price and the best quali
(R)-Ketoprofen Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
Topbatt Chemical Co., Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutical Reference Standards and Stable Isotopes. Our Stable Isotopes produ
1. Our staff are all biomedical related majors with rich experience in the pharmaceutical industry, and can provide you with more professional services.2. Our supplier has a good quality management system, and the quality of products is reliable and
Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
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Type:Trading Company
inquiryHigh purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients
R-ketoprofen
Conditions | Yield |
---|---|
With hydrogenchloride In water at 10 - 35℃; | 98% |
(RS)-ketoprofen vinyl ester
A
(S)-ketoprofen vinyl ester
B
R-ketoprofen
Conditions | Yield |
---|---|
With immobilized Lipozyme In 1,4-dioxane; water at 25℃; for 96h; Enzymatic reaction; optical yield given as %ee; | A 90% B n/a |
(R)-2-(3-Benzoyl-phenyl)-propionic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester
R-ketoprofen
Conditions | Yield |
---|---|
With sodium carbonate In methanol; water for 2h; Ambient temperature; | 85% |
(3R)-1-phenyl-4,4-dimethyl-2-oxopyrrolidin-3-yl (αR)-2-(3-benzoylphenyl)propionate
R-ketoprofen
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid In water at 120℃; for 2.5h; optical yield given as %ee; | 63% |
(+)-α-(3-benzylphenyl)propionic acid
A
S-ketoprofen
B
(3-acetylphenyl)(phenyl)methanone
C
R-ketoprofen
Conditions | Yield |
---|---|
With sodium hydroxide; potassium permanganate In water for 6h; Ambient temperature; Yield given; | A n/a B 28.4% C n/a |
ketoprofen methyl ester
A
S-ketoprofen
B
R-ketoprofen
Conditions | Yield |
---|---|
With sodium hydroxide In water at 40℃; for 7.55h; titrisol buffer pH 8, carboxylesterase NP; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With tris hydrochloride; S. solfataricus esterase In water at 60℃; for 32h; pH=7.0; Enzymatic reaction; |
Conditions | Yield |
---|---|
With phosphate buffer; sodium dodecyl-sulfate; vancomycin at 20℃; Product distribution; electrophoretic enantioseparations, various substrates; | |
EtOH, TAPS/Tris buffer, pH 7.7; | |
lipase from Candida rugosa In 2,2,4-trimethylpentane; acetone Product distribution / selectivity; Resolution of racemate; |
Conditions | Yield |
---|---|
With (-)-Diop; chloro(1,5-hexadiene)rhodium(I) dimer; hydrogen; triethylamine; benzene In ethanol under 53200 Torr; for 20h; Ambient temperature; Yield given. Title compound not separated from byproducts; | |
With (-)-Diop; chloro(1,5-hexadiene)rhodium(I) dimer; hydrogen; triethylamine In ethanol; benzene under 11172 - 77140 Torr; Product distribution; different solvents, without NEt3, with KOH; other object: optical yield; |
2-chloroethyl ester of 2-(3-benzoylphenyl)propionic acid
A
S-ketoprofen
B
R-ketoprofen
Conditions | Yield |
---|---|
With water at 40℃; for 40h; Candida rugosa lipase, pH 5; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With Candida rugosa lipase (Lipase OF); Tween-80 In water at 30℃; for 24h; pH=2.5; Title compound not separated from byproducts; |
B
R-ketoprofen
Conditions | Yield |
---|---|
With human serum albumin In water at 37℃; pH=7.4; Enzyme kinetics; Further Variations:; Reagents; Hydrolysis; Enzymatic reaction; isotonic 0.067 M phosphate buffer; |
ketoprofen chloride
A
S-ketoprofen
B
R-ketoprofen
Conditions | Yield |
---|---|
Stage #1: ketoprofen chloride With (S)-(3-OH-4,4-di-Me-2-oxopyrrolidin-1-yl)CH2COOH on resin; triethylamine In tetrahydrofuran at 0℃; Stage #2: With lithium hydroxide In tetrahydrofuran; water at 20℃; for 4h; Further stages. Title compound not separated from byproducts.; |
(S)-2-(3-Benzoyl-phenyl)-propionic acid (S)-1-carbamoylmethyl-4,4-dimethyl-2-oxo-pyrrolidin-3-yl ester
A
S-ketoprofen
B
R-ketoprofen
Conditions | Yield |
---|---|
With lithium hydroxide In tetrahydrofuran; water at 20℃; for 1h; |
(R)-(-)-2-(3-benzoylphenyl)propionic acid ethyl ester
R-ketoprofen
Conditions | Yield |
---|---|
With novozyme 435 In water; acetonitrile at 45℃; for 45h; | 360 mg |
ketoprofen
R-ketoprofen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Novozyme 435 / toluene / 2 h / 45 °C 2: 360 mg / Novozyme 435 / acetonitrile; H2O / 45 h / 45 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: oxalyl chloride / 12 h / 40 °C 2.1: rink amide linker modified polystyrene grafted crowns; piperidine; benzotriazolyloxy-tris(dimethylamino)phosphonium(1+) PF6(1-) / diisopropylethylamine / dimethylformamide / 12 h / 20 °C 2.2: triethylamine / tetrahydrofuran / 12 h / 0 °C 2.3: 104 mg / trifluoroacetic acid / CH2Cl2 / 0.67 h 3.1: LiOH / tetrahydrofuran; H2O / 1 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: oxalyl chloride / 12 h / 40 °C 2.1: triethylamine; (S)-(3-OH-4,4-di-Me-2-oxopyrrolidin-1-yl)CH2COOH on resin / tetrahydrofuran / 0 °C 2.2: LiOH*H2O / tetrahydrofuran; H2O / 4 h / 20 °C View Scheme |
ketoprofen chloride
R-ketoprofen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: rink amide linker modified polystyrene grafted crowns; piperidine; benzotriazolyloxy-tris(dimethylamino)phosphonium(1+) PF6(1-) / diisopropylethylamine / dimethylformamide / 12 h / 20 °C 1.2: triethylamine / tetrahydrofuran / 12 h / 0 °C 1.3: 104 mg / trifluoroacetic acid / CH2Cl2 / 0.67 h 2.1: LiOH / tetrahydrofuran; H2O / 1 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 99.5 percent Spectr. / Et3N / toluene / -10 °C 2: 85 percent / Na2CO3 / methanol; H2O / 2 h / Ambient temperature View Scheme |
ethyl α-(3-benzoylphenyl)acrylate
R-ketoprofen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 93 percent / 3percent KOH/H2O / tetrahydrofuran / 24 h / Ambient temperature 2: H2, 2/(-)-DIOP/NEt3 / ethanol; benzene / 11172 - 77140 Torr / different solvents, without NEt3, with KOH; other object: optical yield View Scheme |
ketoprofen
bis(1-naphthyl)methanol
A
(R)-ketoprofen di(1-naphthyl)methyl ester
C
S-ketoprofen
D
R-ketoprofen
Conditions | Yield |
---|---|
With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; p-Methoxybenzoic anhydride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 12h; Resolution of racemate; optical yield given as %ee; | |
With (-)-(S)-β-Np-BTM; 2,2-dimethylpropanoic anhydride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 12h; Inert atmosphere; Resolution of racemate; optical yield given as %ee; enantioselective reaction; | |
With benzoic acid anhydride; N-ethyl-N,N-diisopropylamine; (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole In dichloromethane at 20℃; for 6h; Product distribution / selectivity; Resolution of racemate; | A n/a B n/a C n/a D n/a |
(R,S)-N-ketoprofenyl-1,2,4-triazole
A
(S)-N-ketoprofenyl-1,2,4-triazole
B
R-ketoprofen
Conditions | Yield |
---|---|
With Novozym 435; water In tert-butyl methyl ether at 45℃; Kinetics; Solvent; Concentration; |
ketoprofen methyl ester
A
R-ketoprofen
C
(R)-(-)-2-(3-benzoylphenyl)propionic acid methyl ester
Conditions | Yield |
---|---|
With Novozym 435; water In tert-butyl methyl ether at 45℃; Kinetics; Solvent; Concentration; optical yield given as %ee; |
C
S-ketoprofen
D
R-ketoprofen
Conditions | Yield |
---|---|
Stage #1: 4-nitrophenyl 2-(3-benzoylphenyl)propanoate With Pseudomonas aeruginosa lipase Met16Ala/Leu17Phe/Leu162Asn mutant In acetonitrile at 30℃; for 1.5h; pH=7.5; aq. phosphate buffer; Resolution of racemate; Enzymatic reaction; Stage #2: With hydrogenchloride In water; acetonitrile enantioselective reaction; |
ketoprofen
9,9‘-bis-phenanthrylmethanol
A
(R)-ketoprofen di(9-phenanthryl)methyl ester
C
S-ketoprofen
D
R-ketoprofen
Conditions | Yield |
---|---|
With p-Methoxybenzoic anhydride; N-ethyl-N,N-diisopropylamine; (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole In dichloromethane at 20℃; for 12h; Product distribution / selectivity; Resolution of racemate; | A n/a B n/a C n/a D n/a |
With (R)-(+)-2-phenyl-2,3-dihydrobenzo[d]imidazo[2,1-b]thiazole; p-Methoxybenzoic anhydride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 12h; optical yield given as %ee; enantioselective reaction; |
Conditions | Yield |
---|---|
With Candida antarctica lipase B; water In tert-butyl methyl ether at 45℃; for 2h; Resolution of racemate; Enzymatic reaction; optical yield given as %ee; enantioselective reaction; |
Conditions | Yield |
---|---|
With copper(l) chloride In methanol at 40℃; Inert atmosphere; optical yield given as %ee; |
2-methyl-2-(3-benzoylphenyl)malonic acid
R-ketoprofen
Conditions | Yield |
---|---|
With Mesorhizobium sp. BNC1 arylmalonate decarboxylase Enzymatic reaction; enantioselective reaction; |
Conditions | Yield |
---|---|
With Thermotoga maritima esterase Tm1160 In aq. acetate buffer at 70℃; for 32h; pH=5.5; Enzymatic reaction; enantioselective reaction; | A n/a B n/a |
ethyl 2-<3-benzoylphenyl>propionate
A
S-ketoprofen
B
R-ketoprofen
D
(R)-(-)-2-(3-benzoylphenyl)propionic acid methyl ester
Conditions | Yield |
---|---|
With Yarrowia lipolytica Lip2p lipase In decane at 20℃; for 100h; Kinetics; Enzymatic reaction; enantioselective reaction; |
ethyl 2-<3-benzoylphenyl>propionate
A
R-ketoprofen
Conditions | Yield |
---|---|
With Candida rugose lipase CRL4 10X In decane at 20℃; for 100h; Kinetics; Enzymatic reaction; enantioselective reaction; |
Conditions | Yield |
---|---|
In 2,2,4-trimethylpentane at 30℃; lyophilized crude lipase (olive oil); | 85% |
R-ketoprofen
1-amino-3-(dimethylamino)propane
Conditions | Yield |
---|---|
Stage #1: R-ketoprofen With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; Stage #2: 1-amino-3-(dimethylamino)propane In dichloromethane at 20℃; | 75% |
Conditions | Yield |
---|---|
Stage #1: R-ketoprofen With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 5℃; for 2h; Stage #2: methanesulfonamide With 1,2-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 4h; | 74% |
epicholesterol
R-ketoprofen
epi-cholesteryl (R)-2-(3-benzoylphenyl)propionate
Conditions | Yield |
---|---|
Stage #1: R-ketoprofen With dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Stage #2: epicholesterol With dmap In dichloromethane at 0℃; for 8h; | 74% |
Conditions | Yield |
---|---|
Stage #1: R-ketoprofen With 2,6-dimethylpyridine; chloroformic acid ethyl ester In dichloromethane at 20℃; for 1h; Stage #2: coenzyme A With sodium hydroxide In tetrahydrofuran; water at 20℃; for 2h; pH=6.2; |
methanol
R-ketoprofen
(R)-(-)-2-(3-benzoylphenyl)propionic acid methyl ester
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; | |
With sulfuric acid at 80℃; |
glycine ethyl ester hydrochloride
R-ketoprofen
Conditions | Yield |
---|---|
Stage #1: R-ketoprofen With 1-hydroxybenzotriazol-hydrate; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 0 - 5℃; for 1h; Stage #2: glycine ethyl ester hydrochloride In N,N-dimethyl-formamide at 20℃; |
R-ketoprofen
Conditions | Yield |
---|---|
With thionyl chloride for 3h; Heating; |
cholesterol
R-ketoprofen
epi-cholesteryl (R)-2-(3-benzoylphenyl)propionate
Conditions | Yield |
---|---|
Mitsunobu reaction; |
R-ketoprofen
3-ethylbenzophenone
Conditions | Yield |
---|---|
In phosphate buffer at 25℃; pH=7.4; Quantum yield; Kinetics; Further Variations:; Reagents; Photolysis; |
R-ketoprofen
methyl (2R)-2-[3-(1-phenylethyl)phenyl]propanoate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: H2SO4 / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 3 h / 0 - 5 °C 2.2: 71 percent / tetrahydrofuran; hexane / 20 °C 3.1: H2 / Pd/C / ethanol / 18 h View Scheme |
R-ketoprofen
(R),(R',S')-2-[3-(α-methylbenzyl)phenyl]propionyl chloride
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: H2SO4 / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 3 h / 0 - 5 °C 2.2: 71 percent / tetrahydrofuran; hexane / 20 °C 3.1: H2 / Pd/C / ethanol / 18 h 4.1: 0.29 g / aq. KOH / dioxane / 20 °C 5.1: SOCl2 / 8 h / Heating View Scheme |
R-ketoprofen
(2R)-2-[3-(1-phenylethyl)phenyl]propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: H2SO4 / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 3 h / 0 - 5 °C 2.2: 71 percent / tetrahydrofuran; hexane / 20 °C 3.1: H2 / Pd/C / ethanol / 18 h 4.1: 0.29 g / aq. KOH / dioxane / 20 °C View Scheme |
R-ketoprofen
methyl (2R)-2-[3-(1-phenylvinyl)phenyl]propanoate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: H2SO4 / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 3 h / 0 - 5 °C 2.2: 71 percent / tetrahydrofuran; hexane / 20 °C View Scheme |
R-ketoprofen
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: H2SO4 / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 3 h / 0 - 5 °C 2.2: 71 percent / tetrahydrofuran; hexane / 20 °C 3.1: H2 / Pd/C / ethanol / 18 h 4.1: 0.29 g / aq. KOH / dioxane / 20 °C 5.1: 1,1'-carbonyldiimidazole / CH2Cl2 / 2 h / 0 - 5 °C 5.2: 30 percent / diazabicyclo[5.4.0]undec-7-ene / CH2Cl2 / 4 h View Scheme |
R-ketoprofen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 1-hydroxybenzotriazole hydrate; 1,3-dicyclohexylcarbodiimide / dimethylformamide / 1 h / 0 - 5 °C 1.2: dimethylformamide / 20 °C 2.1: 0.31 g / aq. NaOH / dioxane / 20 °C View Scheme |
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