CAS No.5961-83-1,Propanoic acid,3,3'-oxybis- Suppliers

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Propanoic acid,3,3'-oxybis- cas 5961-83-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Synthetic route

: 1656-48-0
2-cyanoethyl ether

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

Conditions

Conditions	Yield
With hydrogenchloride for 5h; Hydrolysis; Heating;	93%
With hydrogenchloride 1.) 50 deg C, 24 h, 2.) RT, 12 h;	75%
With hydrogenchloride In water at 50℃; for 24h;	70%

: 1427320-41-9
3-(2-tert-butoxycarbonylethoxy)propionic acid tert-butyl ester

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

Conditions

Conditions	Yield
With trifluoroacetic acid at 20℃; for 1h;	90%

: 94102-60-0
4-oxa-1,7-heptanedioic acid dimethyl ester

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

Conditions

Conditions	Yield
With sodium hydroxide In water at 20℃; for 14h;	87%

: 57-57-8
β-Propiolactone

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

Conditions

Conditions	Yield
With water at 90 - 110℃;

: 57-57-8
β-Propiolactone

: 7732-18-5
water

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

Conditions

Conditions	Yield
Erhitzen;

: 79-10-7
acrylic acid

A: 5961-83-1
3-(2-carboxyethoxy)propionic acid

B: 503-66-2
3-hydroxypropionic acid

Conditions

Conditions	Yield
With water; carbon dioxide at 200℃; under 10343.2 - 20686.5 Torr; for 3h;	A 4.6 %Chromat. B 54.0 %Chromat.
With water; calcium oxide at 160℃; for 19h;	A 9.0 %Chromat. B 52.0 %Chromat.
With water; ammonia at 200℃; for 3h;	A 20.5 %Chromat. B 41.2 %Chromat.
With water; magnesium oxide at 170℃; for 18h;	A 13.1 %Chromat. B 68.7 %Chromat.

: 67-56-1
methanol

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 94102-60-0
4-oxa-1,7-heptanedioic acid dimethyl ester

Conditions

Conditions	Yield
With thionyl chloride at 0 - 20℃; for 6h; Inert atmosphere;	84%

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 192803-37-5
3-tert-butyl-2,5-dihydroxybenzaldehyde

: 646705-10-4
3-[2-(3-tert-butyl-5-formyl-4-hydroxy-phenoxycarbonyl)-ethoxy]-propionic acid 3-tert-butyl-5-formyl-4-hydroxy-phenyl ester

Conditions

Conditions	Yield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 3h; Inert atmosphere;	82%
With dmap; diisopropyl-carbodiimide In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃;	56%

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 44995-78-0
3,3'oxybispropionic acid dichloride

Conditions

Conditions	Yield
With thionyl chloride; N,N-dimethyl-formamide In benzene 1.) 40 deg C, 9 h, 2.) RT; 15 h;	74%
With thionyl chloride
With thionyl chloride for 3h; Heating; Yield given;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 192803-37-5
3-tert-butyl-2,5-dihydroxybenzaldehyde

: 1612884-37-3
3-[2-(3-tert-butyl-5-formyl-4-hydroxyphenoxycarbonyl)ethoxy]propionic acid

Conditions

Conditions	Yield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3.5h; Inert atmosphere;	69%

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 1448297-52-6
(2S,4R)-1-[(2S)-2-azanyl-3,3-dimethylbutanoyl]-N-[[4-(4-methyl-1,3-thiazol-5-yl)phenyl]methyl]-4-oxidanylpyrrolidine-2-carboxamide

: 3-(3-(((S)-1-((2S,4R)-4-hydroxy-2-((4-(4-methylthiazol-5-yl)benzyl)carbamoyl)pyrrolidin-1-yl)-3,3-dimethyl-1-oxobutan-2-yl)amino)-3- oxopropoxy)propanoic acid

Conditions

Conditions	Yield
With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dimethyl sulfoxide at 0 - 20℃;	63%
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane	42%
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃;	42%
With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane	42%

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: (2S,4R)-1-[(2S)-2-amino-3,3-dimethylbutanoyl]-4-hydroxy-N-[(1S)-1-[4-(4-methyl-1,3-thiazol-5-yl)phenyl]ethyl]pyrrolidine-2-carboxamide

: 3 -(3-(((S)-1-((2S,4R)-4-hydroxy-2-(((S)-1-(4-(4-methylthiazol-5-yl)phenyl)ethyl)carbamoyl)pyrrolidin-1-yl)-3,3-dimethyl-1-oxobutan-2-yl)amino)-3-oxopropoxy)propanoic acid

Conditions

Conditions	Yield
With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 1h;	62%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: bis(2,5-dioxopyrrolidin-1-yl) 3,3’-oxydipropanoate

Conditions

Conditions	Yield
With dicyclohexyl-carbodiimide In tetrahydrofuran	60%

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 1613552-03-6
[(S)-1-((S)-2-{(2S,4S)-4-amino-2-[(R)-(1,2,3,4-tetrahydro-naphthalen-1-yl)carbamoyl]-pyrrolidin-1-yl}-1-cyclohexyl-2-oxo-ethylcarbamoyl)-ethyl]-methyl-carbamic acid tert-butyl ester

: 3-(3-(((3S,5S)-1-((S)-2-((S)-2-((tert-butoxycarbonyl)(methyl)amino)propanamido)-2-cyclohexylacetyl)-5-(((R)-1,2,3,4-tetrahydronaphthalen-1-yl)carbamoyl)pyrrolidin-3-yl)amino)-3-oxopropoxy)propanoic acid

Conditions

Conditions	Yield
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate at 20℃; for 16h; Inert atmosphere;	58%

: 64-17-5
ethanol

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 17615-27-9
diethyl 3,3-oxydipropanoate

Conditions

Conditions	Yield
With sulfuric acid In chloroform at 95℃; for 20h; Dean-Stark;	50%
With sulfuric acid for 2h; Esterification; Heating;	21.6 g
With thionyl chloride at 0℃; Reflux;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 99616-81-6
bis-4-(3-bromopropoxy)butyl furan-3,4-dicarboxylate

A: 96357-03-8, 99631-35-3, 99664-97-8
6,28-Dimethyl-7,8,11,12,15,16,18,19,23,24,27,28-dodecahydro-6H,10H,22H,26H-2,5,9,13,17,21,25,29-octaoxa-cyclopentacyclononacosene-4,14,20,30-tetraone

: 96357-03-8, 99631-35-3, 99664-97-8
(6R,28R)-6,28-Dimethyl-7,8,11,12,15,16,18,19,23,24,27,28-dodecahydro-6H,10H,22H,26H-2,5,9,13,17,21,25,29-octaoxa-cyclopentacyclononacosene-4,14,20,30-tetraone

Conditions

Conditions	Yield
With potassium carbonate 1.) water, ethanol, pH 7; 2.) dimethylformamide, 22h, 70-80 deg.C; Yield given. Multistep reaction;	A 43% B n/a
With potassium carbonate 1.) water, ethanol, pH 7; 2.) dimethylformamide, 22h, 70-80 deg.C; Yield given. Multistep reaction;	A n/a B 16%

...Expand

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: (2S,4R)-1-[(2S)-2-amino-3,3-dimethylbutanoyl]-4-hydroxy-N-[(1S)-1-[4-(4-methyl-1,3-thiazol-5-yl)phenyl]ethyl]pyrrolidine-2-carboxamide hydrochloride

: 3 -(3-(((S)-1-((2S,4R)-4-hydroxy-2-(((S)-1-(4-(4-methylthiazol-5-yl)phenyl)ethyl)carbamoyl)pyrrolidin-1-yl)-3,3-dimethyl-1-oxobutan-2-yl)amino)-3-oxopropoxy)propanoic acid

Conditions

Conditions	Yield
Stage #1: 3-(2-carboxyethoxy)propionic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 0.0833333h; Stage #2: (2S,4R)-1-[(2S)-2-amino-3,3-dimethylbutanoyl]-4-hydroxy-N-[(1S)-1-[4-(4-methyl-1,3-thiazol-5-yl)phenyl]ethyl]pyrrolidine-2-carboxamide hydrochloride In dichloromethane for 0.5h;	35%

Yield

Stage #1: 3-(2-carboxyethoxy)propionic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 0.0833333h;
Stage #2: (2S,4R)-1-[(2S)-2-amino-3,3-dimethylbutanoyl]-4-hydroxy-N-[(1S)-1-[4-(4-methyl-1,3-thiazol-5-yl)phenyl]ethyl]pyrrolidine-2-carboxamide hydrochloride In dichloromethane for 0.5h;

35%

: 571190-30-2
PD 0332991

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 1448297-52-6
(2S,4R)-1-[(2S)-2-azanyl-3,3-dimethylbutanoyl]-N-[[4-(4-methyl-1,3-thiazol-5-yl)phenyl]methyl]-4-oxidanylpyrrolidine-2-carboxamide

: (2S,4R)-1-((S)-2-(3-(3-(4-(6-((6-acetyl-8-cyclopentyl-5-methyl-7-oxo-7,8-dihydropyrido[2,3-d]pyrimidin-2-yl)amino)pyridin-3-yl)piperazin-1-yl)-3-oxopropoxy)propanamido)-3,3-dimethylbutanoyl)-4-hydroxy-N-(4-(4-methylthiazol-5-yl)benzyl)pyrrolidine-2-carboxamide

Conditions

Conditions	Yield
Stage #1: PD 0332991; 3-(2-carboxyethoxy)propionic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 20℃; Stage #2: (2S,4R)-1-[(2S)-2-amino-3,3-dimethylbutanoyl]-4-hydroxy-N-[[4-(4-methyl-1,3-thiazol-5-yl)phenyl]methyl]pyrrolidine-2-carboxamide With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In dimethyl sulfoxide	18%

Yield

Stage #1: PD 0332991; 3-(2-carboxyethoxy)propionic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 20℃;
Stage #2: (2S,4R)-1-[(2S)-2-amino-3,3-dimethylbutanoyl]-4-hydroxy-N-[[4-(4-methyl-1,3-thiazol-5-yl)phenyl]methyl]pyrrolidine-2-carboxamide With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In dimethyl sulfoxide

18%

...Expand

: 104-76-7
2-Ethylhexyl alcohol

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 2155-31-9
4-oxa-heptanedioic acid bis-(2-ethyl-hexyl ester)

Conditions

Conditions	Yield
With toluene-4-sulfonic acid; benzene unter Entfernen des entstehenden Wassers;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 107-95-9
3-amino propanoic acid

Conditions

Conditions	Yield
With ammonia; water; diphenylamine at 200℃;
With ammonia; water; diphenylamine at 200℃;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 107-18-6
allyl alcohol

: 100521-54-8
4-oxa-heptanedioic acid diallyl ester

Conditions

Conditions	Yield
With sulfuric acid; benzene unter Entfernen des entstehenden Wassers;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: 99629-66-0
bis-3-(3-tosylpropoxy)propyl 3-oxaheptanedioate

: 96356-99-9
1,5,9,13,17,21,25,29-Octaoxa-cyclodotriacontane-2,8,18,24-tetraone

Conditions

Conditions	Yield
With potassium carbonate 1.) Water, ethanol, pH 7; 2.) dimethylformamide, 22h 70-80 deg.C; Yield given. Multistep reaction;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

tetrahydro-γ-pyrone: tetrahydro-γ-pyrone

Conditions

Conditions	Yield
at 350 - 450℃; Das Calciumsalz;
at 350 - 450℃; Das Calciumsalz;

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: (6R,11R)-4,13-Dioxo-1-oxa-8,9-dithia-5,12-diaza-cyclopentadecane-6,11-dicarboxylic acid dimethyl ester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 / 3 h / Heating 2: 75 percent / NEt3 / CH2Cl2 / 12 h / 20 °C View Scheme

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: C26H36N2O11

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 / 3 h / Heating 2: 73 percent / NEt3 / CH2Cl2 / 12 h / 20 °C View Scheme

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: (S)-2-{[(6R,11R)-11-((S)-1-Methoxycarbonyl-3-methyl-butylcarbamoyl)-4,13-dioxo-1-oxa-8,9-dithia-5,12-diaza-cyclopentadecane-6-carbonyl]-amino}-4-methyl-pentanoic acid methyl ester

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 / 3 h / Heating 2: 67 percent / NEt3 / CH2Cl2 / 12 h / 20 °C View Scheme

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: (6R,11R)-4,13-Dioxo-1-oxa-8,9-dithia-5,12-diaza-cyclopentadecane-6,11-dicarboxylic acid bis-adamantan-1-ylamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 / 3 h / Heating 2: 69 percent / NEt3 / CH2Cl2 / 12 h / 20 °C View Scheme

: 5961-83-1
3-(2-carboxyethoxy)propionic acid

: C38H58N4O13

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: SOCl2 / 3 h / Heating 2: 67 percent / NEt3 / CH2Cl2 / 12 h / 20 °C View Scheme

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