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Hebei Miheng Trading Co., Ltd.

5-Methoxytryptamine CAS 608-07-1 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly.

5-Methoxytryptamine CAS 608-07-1

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $50.0 / 100.0

Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

5-Methoxytryptamine Manufacturer/High quality/Best price/In stock

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------

High purity 608-07-1 5-Methoxytryptamine

Cas:608-07-1

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Trading Company

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 5-Methoxytryptamine supplier in China

Cas:608-07-1

Min.Order:0 Metric Ton

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Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product description: Product name 5-Methoxytryptamine CAS number 608-07-1 Assay ≥99% Appearance Off-white powder Capacity 200mt/year Application Pharmaceutical intermediate

5-Methoxytryptamine

Cas:608-07-1

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

Factory 5-Methoxytryptamine in stock CAS 608-07-1

Cas:608-07-1

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need CMO

5-methoxy-tryptamine manufacturer/supplier

Cas:608-07-1

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or pale-white crystalline powder Storage:cool dry place Package:25kg/drum Application:pharmaceutical interm

Manufacturer high quality 5-Methoxytryptamine Cas 608-07-1 with good price

Cas:608-07-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-(5-methoxyindol-3-yl)ethylamine

Cas:608-07-1

Min.Order:1

Negotiable

Type:Other

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Wuhan Kemi-Works Chemical Co., Ltd

Product name: 5-Methoxytryptamine CAS No. 608-07-1 1.We have been specializing in special fine chemical for long, with strong R&D strength. 2.ISO9001. 3.We have been cooperating with oversea from Europe, USA, Korea, Japan etc... Appearan

5-Methoxytryptamine

Cas:608-07-1

Min.Order:1 Kilogram

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Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Content Natural Extract 5-Methoxytryptamine HACCP manufacturer

Cas:608-07-1

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality 5-Methoxytryptamine

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

5-Methoxytryptamine -- CHemwill

Cas:608-07-1

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

5-Methoxytryptamine CAS 608-07-1

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 608-07-1 with best quality

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

5-Methoxytryptamine 608-07-1

Cas:608-07-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Name: 5-Methoxytryptamine CAS No.:608-07-1 Formula: C11H14N2O Molecular Weight : 190.27 Synonyms: Indole,3-(2-aminoethyl)-5-methoxy- (6CI,8CI);2-(5-Methoxyindol-3-yl)ethylamine;2-[5-(Methyloxy)-1H-indol-3-yl]ethanamine;3-(2-Aminoethyl)-5-metho

5-Methoxytryptamine CAS: 608-07-1

Cas:608-07-1

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla

CAS 608-07-1 5-Methoxytryptamine with Free Sample

Cas:608-07-1

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

5-Methoxytryptamine 608-07-1

Cas:608-07-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:White powder or refer to COA Storage:keep in co

High quality 5-Methoxytryptamine with purity of 99% CAS 608-07-1 from China manufacturer

Cas:608-07-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,

5-Methoxytryptamine WITH BEST PRICE

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $400.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

5-Methoxytryptamine CAS:608-07-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme

5-Methoxytryptamine CAS:608-07-1

Cas:608-07-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Methoxytryptamine

Cas:608-07-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:608-07-1

Cas:608-07-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe,

5-Methoxytryptamine cas 608-07-1 O-methylserotonin

Cas:608-07-1

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Trading Company

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Wuhan Zenuo Biological Medicine Technology Co Ltd

Product Name: 5-Methoxytryptamine Synonyms: 3-(Aminoethyl)-5-methoxyindole;5-Methoxy-[1H]-indole-3-ethanamine;Meksamin;2-(5-methoxy-1H-indol-3-yl)acetic acid;5-Methoxyindoleacetate;5-METHOXYTRYPTAMINE 98+%;Methyl sulfone(MSM);3-(2-Aminoethyl)-5-

5-Methoxytryptamine high purity best quality

Cas:608-07-1

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Shanxi Ankesi Biotechnology Co., Ltd

Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual

High quality 5-Methoxytryptamine CAS 608-07-1

Cas:608-07-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

5-Methoxytryptamine

Cas:608-07-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

5-Methoxytryptamine

Cas:608-07-1

Min.Order:0

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Type:Lab/Research institutions

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Synthetic route

5-methoxy-3-(2-nitroethyl)-1H-indole
68935-49-9

5-methoxy-3-(2-nitroethyl)-1H-indole

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In methanol at 20℃;99%
With hydrogen; palladium on activated charcoal In ethanol under 2585.7 Torr; for 12h;
methyl N-[2-(5-methoxy-1H-indol-3-yl)ethyl]carbamate
67199-10-4

methyl N-[2-(5-methoxy-1H-indol-3-yl)ethyl]carbamate

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With sodium hydroxide In methanol for 4h; Hydrolysis; decarboxylation; Heating;99%
With water Hydrolysis;
With sodium hydroxide Heating;
2-ethoxycarbonyl-3-(2-phthalimidoethyl)-5-methoxyindole
55747-53-0

2-ethoxycarbonyl-3-(2-phthalimidoethyl)-5-methoxyindole

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Stage #1: 2-ethoxycarbonyl-3-(2-phthalimidoethyl)-5-methoxyindole With water; sodium hydroxide at 88 - 90℃;
Stage #2: With hydrogenchloride In water at 10 - 110℃; Temperature;
99%
Multi-step reaction with 2 steps
1: 10 percent aq. NaOH / 0.08 h / Heating; microwave irradiation
2: 20 percent H2SO4 / 0.17 h / Heating; microwave irradiation
View Scheme
With potassium hydroxide for 3h; Reflux;57 g
5-methoxy-N-acetyl-tryptamine
73-31-4

5-methoxy-N-acetyl-tryptamine

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With ammonium bromide; ethylenediamine at 100℃; for 7h; Microwave irradiation;89%
With sulfuric acid In water for 8h; Heating;69.7%
With sodium hydroxide In 2-methyl-propan-1-ol
2-(1-methanesulfonyl-5-methoxy-1H-indol-3-yl)ethylamine
627086-10-6

2-(1-methanesulfonyl-5-methoxy-1H-indol-3-yl)ethylamine

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With potassium hydroxide In methanol for 9h; Heating;84%
5-methoxy-3-(2-nitro-vinyl)-indole
61675-19-2

5-methoxy-3-(2-nitro-vinyl)-indole

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 40h;73%
With lithium aluminium tetrahydride In tetrahydrofuran Heating;
Stage #1: 5-methoxy-3-(2-nitro-vinyl)-indole With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; Inert atmosphere;
Stage #2: With water In tetrahydrofuran at 0℃;
2-(1-benzyl-5-methoxy-1H-indol-3-yl)ethylamine
40619-73-6

2-(1-benzyl-5-methoxy-1H-indol-3-yl)ethylamine

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With sodium In tetrahydrofuran; ammonia at -33℃; for 1.5h;66%
N-(2-(5-methoxy-1H-indol-3-yl)ethyl)-4-methylbenzenesulfonamide
102016-76-2

N-(2-(5-methoxy-1H-indol-3-yl)ethyl)-4-methylbenzenesulfonamide

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With ammonia; sodium In tetrahydrofuran at -78℃; for 0.25h;65%
5-methoxylindole
1006-94-6

5-methoxylindole

L-serin
56-45-1

L-serin

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Stage #1: 5-methoxylindole; L-serin With engineered tryptophan synthase In methanol; aq. phosphate buffer at 75℃; for 12h; pH=8.0; Enzymatic reaction;
Stage #2: With pyridoxal 5'-phosphate; Ruminococcus gnavus L-tryptophan decarboxylase In methanol; aq. phosphate buffer at 37℃; pH=8.0; Enzymatic reaction;
14%
5-methoxylindole
1006-94-6

5-methoxylindole

methyl magnesium iodide
917-64-6

methyl magnesium iodide

diethyl ether
60-29-7

diethyl ether

chloroacetonitrile
107-14-2

chloroacetonitrile

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
und Erwaermen des Reaktionsprodukts Natrium in Aethanol;
5-methoxylindole
1006-94-6

5-methoxylindole

methyl magnesium iodide
917-64-6

methyl magnesium iodide

chloroacetonitrile
107-14-2

chloroacetonitrile

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With diethyl ether Erwaermen des Reaktionsprodukts mit Natrium und Aethanol;
(5-methoxy-2-oxo-2,3-dihydro-1H-indol-3-yl)acetonitrile
70351-49-4

(5-methoxy-2-oxo-2,3-dihydro-1H-indol-3-yl)acetonitrile

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With 2-methyl-propan-1-ol; sodium
5-methoxytryptamine-2-carboxylic acid
52648-13-2

5-methoxytryptamine-2-carboxylic acid

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With hydrogenchloride
4-Methoxyphenylhydrazine
3471-32-7

4-Methoxyphenylhydrazine

4-amino-butyraldehyde diethyl acetate

4-amino-butyraldehyde diethyl acetate

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With zinc(II) chloride at 180℃;
5-methoxy-3-indoleglyoxylylamide
52055-22-8

5-methoxy-3-indoleglyoxylylamide

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 8h; Heating;
With lithium aluminium tetrahydride In tetrahydrofuran for 18h; Reflux;
5-methoxy-3-(2-phthalimido-ethyl)-indole-2-carboxylic acid
55747-60-9

5-methoxy-3-(2-phthalimido-ethyl)-indole-2-carboxylic acid

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
With sulfuric acid for 0.166667h; Heating; microwave irradiation;
tryptamine
61-54-1

tryptamine

phenyl halide

phenyl halide

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 100 percent / Et3N
2: Et3SiH / trifluoroacetic acid
3: 63 percent / Na2WO4*2H2O; aq. H2O2 / methanol; H2O
4: 85 percent / BF3
5: NaOH / Heating
View Scheme
methyl 2-(1-H-indol-3-yl)ethylcarbamate
58635-45-3

methyl 2-(1-H-indol-3-yl)ethylcarbamate

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: Et3SiH / trifluoroacetic acid
2: 63 percent / Na2WO4*2H2O; aq. H2O2 / methanol; H2O
3: 85 percent / BF3
4: NaOH / Heating
View Scheme
Multi-step reaction with 4 steps
1: 97 percent / Et3SiH / trifluoroacetic acid / 3 h / 60 °C
2: 65 percent / H2O2 / Na2WO4*2H2O / methanol; H2O / 0.5 h / 20 °C
3: 94 percent / BF3 / 0.67 h / Heating
4: 99 percent / aq. NaOH / methanol / 4 h / Heating
View Scheme
2,3-dihydro-Nb-methoxycarbonyltryptamine
180910-64-9

2,3-dihydro-Nb-methoxycarbonyltryptamine

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 63 percent / Na2WO4*2H2O; aq. H2O2 / methanol; H2O
2: 85 percent / BF3
3: NaOH / Heating
View Scheme
Multi-step reaction with 3 steps
1: 65 percent / H2O2 / Na2WO4*2H2O / methanol; H2O / 0.5 h / 20 °C
2: 94 percent / BF3 / 0.67 h / Heating
3: 99 percent / aq. NaOH / methanol / 4 h / Heating
View Scheme
1-hydroxy-Nb-methoxycarbonyltryptamine
180910-53-6

1-hydroxy-Nb-methoxycarbonyltryptamine

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 85 percent / BF3
2: NaOH / Heating
View Scheme
Multi-step reaction with 2 steps
1: 94 percent / BF3 / 0.67 h / Heating
2: 99 percent / aq. NaOH / methanol / 4 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 85 percent / BF3*MeOH / 0.17 h / Heating
2: H2O
View Scheme
5-methoxylindole
1006-94-6

5-methoxylindole

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: POCl3 / 0 °C
2: NH4OAc / 70 °C
3: LiAlH4 / tetrahydrofuran / Heating
View Scheme
Multi-step reaction with 3 steps
1: diethyl ether / 6 h / Heating
2: NH3 / dioxane / 8 h / 20 °C
3: lithium aluminum hydride / tetrahydrofuran / 8 h / Heating
View Scheme
Multi-step reaction with 5 steps
1.1: BuLi / tetrahydrofuran; hexane / 0.25 h / -10 °C
1.2: tetrahydrofuran; hexane / 3 h / 0 °C
2.1: 5.4 g / NBS / tetrahydrofuran; hexane / 3 h / -78 °C
3.1: t-BuLi / pentane; diethyl ether / 0.17 h / -78 °C
3.2: CuBr*SMe2 / pentane; diethyl ether / 0.25 h / -78 °C
3.3: 50 percent / BF3*Et2O / pentane; diethyl ether / 4 h / -78 °C
4.1: 89 percent / Bu4NF / tetrahydrofuran / 0.17 h / 20 °C
5.1: 65 percent / NH3; Na / tetrahydrofuran / 0.25 h / -78 °C
View Scheme
5-methoxyindole-3-carboxaldehyde
10601-19-1

5-methoxyindole-3-carboxaldehyde

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NH4OAc / 70 °C
2: LiAlH4 / tetrahydrofuran / Heating
View Scheme
Multi-step reaction with 3 steps
1: ammonium acetate / benzene / Reflux
2: sodium tetrahydroborate / tetrahydrofuran; methanol / 20 °C
3: palladium on activated charcoal; hydrogen / methanol / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: piperidine; acetic acid / benzene / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux
View Scheme
Multi-step reaction with 2 steps
1: ammonium acetate / 1.5 h / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / 40 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: ammonium acetate / 1.5 h / Reflux; Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 36 h / 0 - 20 °C / Inert atmosphere
View Scheme
2-iodo-4-methoxylaniline
191348-14-8

2-iodo-4-methoxylaniline

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: 96 percent / 4-dimethylaminopyridine; pyridine / 14 h / 20 °C
2.1: 82 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
3.1: tristrimethylsilylsilane; azoisobutyronitrile / toluene / 12 h / Heating
3.2: 74 percent / p-toluenesulfonic acid / toluene / 2 h / Heating
4.1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating
5.1: 84 percent / KOH / methanol / 9 h / Heating
View Scheme
N-(2-iodo-4-methoxyphenyl)methanesulfonamide
627086-06-0

N-(2-iodo-4-methoxyphenyl)methanesulfonamide

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 82 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
2.1: tristrimethylsilylsilane; azoisobutyronitrile / toluene / 12 h / Heating
2.2: 74 percent / p-toluenesulfonic acid / toluene / 2 h / Heating
3.1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating
4.1: 84 percent / KOH / methanol / 9 h / Heating
View Scheme
2-[2-(1-methanesulfonyl-5-methoxy-1H-indol-3-yl)ethyl]isoindole-1,3-dione
627086-09-3

2-[2-(1-methanesulfonyl-5-methoxy-1H-indol-3-yl)ethyl]isoindole-1,3-dione

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating
2: 84 percent / KOH / methanol / 9 h / Heating
View Scheme
N-[4-(1,3-dioxodihydroisoindol-2-yl)but-2-ynyl]-N-(2'-iodo-4'-methoxyphenyl)methanesulfonamide
627086-07-1

N-[4-(1,3-dioxodihydroisoindol-2-yl)but-2-ynyl]-N-(2'-iodo-4'-methoxyphenyl)methanesulfonamide

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: tristrimethylsilylsilane; azoisobutyronitrile / toluene / 12 h / Heating
1.2: 74 percent / p-toluenesulfonic acid / toluene / 2 h / Heating
2.1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating
3.1: 84 percent / KOH / methanol / 9 h / Heating
View Scheme
(5-methoxy-1H-indol-3-yl)oxoacetyl chloride
2426-19-9

(5-methoxy-1H-indol-3-yl)oxoacetyl chloride

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NH3 / dioxane / 8 h / 20 °C
2: lithium aluminum hydride / tetrahydrofuran / 8 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: ammonia / 1,4-dioxane / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / Reflux
View Scheme
1-benzyl-5-methoxy-1H-indole-3-acetamide
93879-42-6

1-benzyl-5-methoxy-1H-indole-3-acetamide

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 60.5 percent / LiAlH4 / diethyl ether / 48 h / Heating
2: 66 percent / Na / tetrahydrofuran; liquid ammonia / 1.5 h / -33 °C
View Scheme
methyl 1-benzyl-5-methoxy-1H-indole-3-acetate
419569-93-0

methyl 1-benzyl-5-methoxy-1H-indole-3-acetate

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 83 percent / NH3 / methanol / 192 h / 20 °C
2: 60.5 percent / LiAlH4 / diethyl ether / 48 h / Heating
3: 66 percent / Na / tetrahydrofuran; liquid ammonia / 1.5 h / -33 °C
View Scheme
succinic acid anhydride
108-30-5

succinic acid anhydride

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

3-<(5-methoxy-3-indolyl)ethylamino>propionic acid
58714-14-0

3-<(5-methoxy-3-indolyl)ethylamino>propionic acid

Conditions
ConditionsYield
In chloroform at 0 - 5℃; for 0.25h;100%
In dichloromethane at 20℃; for 18h;99%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

acetic anhydride
108-24-7

acetic anhydride

5-methoxy-N-acetyl-tryptamine
73-31-4

5-methoxy-N-acetyl-tryptamine

Conditions
ConditionsYield
With pyridine In dichloromethane100%
In 1,2-dichloro-ethane at 0℃; for 1h;96%
With triethylamine95%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

formic acid ethyl ester
109-94-4

formic acid ethyl ester

N-(2-(5-methoxy-1H-indol-3-yl)ethyl)formamide
104510-12-5

N-(2-(5-methoxy-1H-indol-3-yl)ethyl)formamide

Conditions
ConditionsYield
for 10h; Reflux;100%
for 10h; Reflux;100%
for 12h; Reflux;100%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Trifluoroacetaldehyde ethyl hemiacetal
433-27-2

Trifluoroacetaldehyde ethyl hemiacetal

6-methoxy-1-trifluoromethyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole
126260-64-8

6-methoxy-1-trifluoromethyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole

Conditions
ConditionsYield
at 110 - 120℃; for 5h;99.7%
4-methyleneoxetan-2-one
674-82-8

4-methyleneoxetan-2-one

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

N-<2-(5-methoxy-1H-indol-3-yl)ethyl>-3-oxobutyramide
112081-40-0

N-<2-(5-methoxy-1H-indol-3-yl)ethyl>-3-oxobutyramide

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 24h;99%
In dichloromethane at 0℃; for 12.5h;
phthalic anhydride
85-44-9

phthalic anhydride

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

2-(2-(5-methoxy-1H-indol-3-yl)ethyl)isoindoline-1,3-dione
55747-66-5

2-(2-(5-methoxy-1H-indol-3-yl)ethyl)isoindoline-1,3-dione

Conditions
ConditionsYield
With triethylamine In toluene for 24h; Reflux; Dean-Stark;99%
at 206℃;88%
With triethylamine In toluene for 24h; Reflux;87%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole
380358-27-0

3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 12h;99%
With triethylamine In tetrahydrofuran at 10℃; for 1h; Inert atmosphere;99%
With triethylamine In tetrahydrofuran at 10℃; for 1h;99%
1-methyl-1H-indole-2,3-dione
2058-74-4

1-methyl-1H-indole-2,3-dione

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

(S)-6'-methoxy-1-methyl-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one
1340563-49-6

(S)-6'-methoxy-1-methyl-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one

Conditions
ConditionsYield
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In N,N-dimethyl-formamide at 40℃; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction;99%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

5-bromo-1-methyl-1H-indole-2,3-dione
2058-72-2

5-bromo-1-methyl-1H-indole-2,3-dione

5-bromo-6'-methoxy-1-methyl-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one
904501-92-4

5-bromo-6'-methoxy-1-methyl-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one

Conditions
ConditionsYield
With scandium(III) chloride; sodium sulfate In dichloromethane at 23℃; Pictet-Spengler cyclisation; Inert atmosphere;99%
3-methylbutyric acid
503-74-2

3-methylbutyric acid

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

C16H22N2O2

C16H22N2O2

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine at 20℃; for 18h;99%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

acetyl chloride
75-36-5

acetyl chloride

5-methoxy-N-acetyl-tryptamine
73-31-4

5-methoxy-N-acetyl-tryptamine

Conditions
ConditionsYield
In dichloromethane at 25 - 30℃; Temperature;98.3%
With triethylamine In dichloromethane at 20℃;
With triethylamine In dichloromethane at 0 - 20℃; for 5h;
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

2-bromoallyl bromide
513-31-5

2-bromoallyl bromide

2-bromo-N-[2-(5-methoxy-1H-indol-3-yl)ethyl]prop-2-en-1-amine
1036862-81-3

2-bromo-N-[2-(5-methoxy-1H-indol-3-yl)ethyl]prop-2-en-1-amine

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran at 20℃;98%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

2-(2'-phenylethynyl)benzoic acid
1084-95-3

2-(2'-phenylethynyl)benzoic acid

3-benzyl-3-hydroxy-2-(2-(5-methoxy-1H-indol-3-yl)ethyl)isoindolin-1-one
1246168-38-6

3-benzyl-3-hydroxy-2-(2-(5-methoxy-1H-indol-3-yl)ethyl)isoindolin-1-one

Conditions
ConditionsYield
Stage #1: 2-(2'-phenylethynyl)benzoic acid With tetrabutylammonium acetate In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere;
Stage #2: 2-(5-methoxyindol-3-yl)ethylamine In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; regioselective reaction;
98%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

benzaldehyde
100-52-7

benzaldehyde

N-benzyl-2-(5-methoxy-1H-indol-3-yl)ethan-1-amine
25119-60-2

N-benzyl-2-(5-methoxy-1H-indol-3-yl)ethan-1-amine

Conditions
ConditionsYield
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde In methanol at 20℃; for 36h;
Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 1h;
98%
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde In methanol at 20℃;
Stage #2: With sodium tetrahydroborate at 20℃; Borch Reduction;
98%
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde In methanol at 20℃; for 36h;
Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 1h;
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde With sodium sulfate In methanol for 12h;
Stage #2: With sodium tetrahydroborate In methanol at 0℃;
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

Glyoxilic acid
298-12-4

Glyoxilic acid

6-methoxy-2,3,4,9-tetrahydro-1H-β-carboline-1-carboxylic acid
17952-63-5

6-methoxy-2,3,4,9-tetrahydro-1H-β-carboline-1-carboxylic acid

Conditions
ConditionsYield
With potassium carbonate In water; ethyl acetate at 20℃; for 24h; pH=5; Pictet-Spengler Synthesis;98%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

2-((4-methoxyphenyl)ethynyl)benzoic acid
859829-95-1

2-((4-methoxyphenyl)ethynyl)benzoic acid

3-hydroxy-2-(2-(5-methoxy-1H-indol-3-yl)ethyl)-3-(4-methoxybenzyl)isoindolin-1-one
1246168-42-2

3-hydroxy-2-(2-(5-methoxy-1H-indol-3-yl)ethyl)-3-(4-methoxybenzyl)isoindolin-1-one

Conditions
ConditionsYield
Stage #1: 2-((4-methoxyphenyl)ethynyl)benzoic acid With tetrabutylammonium acetate In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere;
Stage #2: 2-(5-methoxyindol-3-yl)ethylamine In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; regioselective reaction;
97%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

dimethyl 2-ketoglutarate
13192-04-6

dimethyl 2-ketoglutarate

methyl 8-methoxy-2,3,5,6,11,11b-hexahydro-3-oxo-1H-indolizino<8,7-b>indole-11b-carboxylate
129968-05-4

methyl 8-methoxy-2,3,5,6,11,11b-hexahydro-3-oxo-1H-indolizino<8,7-b>indole-11b-carboxylate

Conditions
ConditionsYield
With acetic acid for 4h; Reflux; Inert atmosphere;97%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

potassium thioacetate
10387-40-3

potassium thioacetate

5-methoxy-N-acetyl-tryptamine
73-31-4

5-methoxy-N-acetyl-tryptamine

Conditions
ConditionsYield
With tetrabutylammonium tetrafluoroborate In ethyl acetate at 20℃; Electrochemical reaction;97%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

n-valeryl chloride
638-29-9

n-valeryl chloride

N-<2-(5-methoxy-1H-indol-3-yl)ethyl>pentanamide

N-<2-(5-methoxy-1H-indol-3-yl)ethyl>pentanamide

Conditions
ConditionsYield
In toluene for 1h; Ambient temperature;96%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

7-(trifluoromethyl)-3,4,5,6-tetrahydro-2H-azepine
1146222-77-6

7-(trifluoromethyl)-3,4,5,6-tetrahydro-2H-azepine

5-(6-methoxy-1-(trifluoromethyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)pentan-1-amine

5-(6-methoxy-1-(trifluoromethyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)pentan-1-amine

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 168h; Pictet-Spengler Synthesis;96%
formaldehyd
50-00-0

formaldehyd

2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

pinoline
20315-68-8

pinoline

Conditions
ConditionsYield
With chloro-trimethyl-silane95%
With acetic acid In methanol at 80℃; for 1h;83%
With sulfuric acid Erhitzen des Reaktionsprodukts mit wss. H2SO4;
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

tetra(n-butyl)ammonium hydrogen sulfate

tetra(n-butyl)ammonium hydrogen sulfate

benzenesulfonyl chloride
98-09-9

benzenesulfonyl chloride

3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole
380358-27-0

3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole

A

1-(benzenesulfonyl)-3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole
297751-49-6

1-(benzenesulfonyl)-3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole

B

2-[1-(benzenesulfonyl)-5-methoxy-1H-indol-3-yl]ethylamine hydrochloride

2-[1-(benzenesulfonyl)-5-methoxy-1H-indol-3-yl]ethylamine hydrochloride

Conditions
ConditionsYield
With sodium hydroxide In dichloromethaneA n/a
B 95%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

1-benzylisatin
1217-89-6

1-benzylisatin

(S)-1-benzyl-6'-methoxy-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one
1340563-51-0

(S)-1-benzyl-6'-methoxy-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one

Conditions
ConditionsYield
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In N,N-dimethyl-formamide at 40℃; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction;95%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

cyclohexanecarbaldehyde
2043-61-0

cyclohexanecarbaldehyde

1-cyclohexyl-6-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

1-cyclohexyl-6-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; Pictet-Spengler Synthesis;95%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

4-Nitrobenzenesulfonyl chloride
98-74-8

4-Nitrobenzenesulfonyl chloride

N-(2-(5-methoxy-1H-indol-3-yl)ethyl)-4-nitrobenzenesulfonamide

N-(2-(5-methoxy-1H-indol-3-yl)ethyl)-4-nitrobenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; Schlenk technique;95%
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

(4-fluorophenyl)glyoxal
403-32-7

(4-fluorophenyl)glyoxal

(4-fluorophenyl)(6-methoxy-9H-pyrido[3,4-b]indol-1-yl)methanone
1148028-92-5

(4-fluorophenyl)(6-methoxy-9H-pyrido[3,4-b]indol-1-yl)methanone

Conditions
ConditionsYield
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; (4-fluorophenyl)glyoxal In dichloromethane
Stage #2: With montmorillonite K-10; palladium 10% on activated carbon In methanol; dichloromethane for 0.0833333h; Pictet-Spengler cyclisation;
Stage #3: at 130℃; for 0.116667h; Microwave irradiation;
94%
With 5%-palladium/activated carbon; montmorillonite K10 Clay at 130℃; Microwave irradiation;
2-(5-methoxyindol-3-yl)ethylamine
608-07-1

2-(5-methoxyindol-3-yl)ethylamine

levulinic acid
123-76-2

levulinic acid

8-Methoxy-2,3,5,6,11,11b-hexahydro-3-oxo-11b-methyl-1H-indolizino<8,7-b>indole
734-15-6

8-Methoxy-2,3,5,6,11,11b-hexahydro-3-oxo-11b-methyl-1H-indolizino<8,7-b>indole

Conditions
ConditionsYield
at 180℃; under 11251.1 Torr; for 0.0333333h; Pictet-Spengler condensation; Microwave irradiation; Neat (no solvent);94%
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