5-Methoxytryptamine CAS 608-07-1 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly.
Cas:608-07-1
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name 5-Methoxytryptamine CAS number 608-07-1 Assay ≥99% Appearance Off-white powder Capacity 200mt/year Application Pharmaceutical intermediate
Cas:608-07-1
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inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or pale-white crystalline powder Storage:cool dry place Package:25kg/drum Application:pharmaceutical interm
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryProduct name: 5-Methoxytryptamine CAS No. 608-07-1 1.We have been specializing in special fine chemical for long, with strong R&D strength. 2.ISO9001. 3.We have been cooperating with oversea from Europe, USA, Korea, Japan etc... Appearan
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryName: 5-Methoxytryptamine CAS No.:608-07-1 Formula: C11H14N2O Molecular Weight : 190.27 Synonyms: Indole,3-(2-aminoethyl)-5-methoxy- (6CI,8CI);2-(5-Methoxyindol-3-yl)ethylamine;2-[5-(Methyloxy)-1H-indol-3-yl]ethanamine;3-(2-Aminoethyl)-5-metho
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry pla
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:White powder or refer to COA Storage:keep in co
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
Cas:608-07-1
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inquiry5-Methoxytryptamine CAS:608-07-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe,
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inquiryProduct Name: 5-Methoxytryptamine Synonyms: 3-(Aminoethyl)-5-methoxyindole;5-Methoxy-[1H]-indole-3-ethanamine;Meksamin;2-(5-methoxy-1H-indol-3-yl)acetic acid;5-Methoxyindoleacetate;5-METHOXYTRYPTAMINE 98+%;Methyl sulfone(MSM);3-(2-Aminoethyl)-5-
Cas:608-07-1
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inquiryOur Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
5-methoxy-3-(2-nitroethyl)-1H-indole
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In methanol at 20℃; | 99% |
With hydrogen; palladium on activated charcoal In ethanol under 2585.7 Torr; for 12h; |
methyl N-[2-(5-methoxy-1H-indol-3-yl)ethyl]carbamate
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With sodium hydroxide In methanol for 4h; Hydrolysis; decarboxylation; Heating; | 99% |
With water Hydrolysis; | |
With sodium hydroxide Heating; |
2-ethoxycarbonyl-3-(2-phthalimidoethyl)-5-methoxyindole
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Stage #1: 2-ethoxycarbonyl-3-(2-phthalimidoethyl)-5-methoxyindole With water; sodium hydroxide at 88 - 90℃; Stage #2: With hydrogenchloride In water at 10 - 110℃; Temperature; | 99% |
Multi-step reaction with 2 steps 1: 10 percent aq. NaOH / 0.08 h / Heating; microwave irradiation 2: 20 percent H2SO4 / 0.17 h / Heating; microwave irradiation View Scheme | |
With potassium hydroxide for 3h; Reflux; | 57 g |
Conditions | Yield |
---|---|
With ammonium bromide; ethylenediamine at 100℃; for 7h; Microwave irradiation; | 89% |
With sulfuric acid In water for 8h; Heating; | 69.7% |
With sodium hydroxide In 2-methyl-propan-1-ol |
2-(1-methanesulfonyl-5-methoxy-1H-indol-3-yl)ethylamine
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 9h; Heating; | 84% |
5-methoxy-3-(2-nitro-vinyl)-indole
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 40h; | 73% |
With lithium aluminium tetrahydride In tetrahydrofuran Heating; | |
Stage #1: 5-methoxy-3-(2-nitro-vinyl)-indole With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; Inert atmosphere; Stage #2: With water In tetrahydrofuran at 0℃; |
2-(1-benzyl-5-methoxy-1H-indol-3-yl)ethylamine
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With sodium In tetrahydrofuran; ammonia at -33℃; for 1.5h; | 66% |
N-(2-(5-methoxy-1H-indol-3-yl)ethyl)-4-methylbenzenesulfonamide
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With ammonia; sodium In tetrahydrofuran at -78℃; for 0.25h; | 65% |
Conditions | Yield |
---|---|
Stage #1: 5-methoxylindole; L-serin With engineered tryptophan synthase In methanol; aq. phosphate buffer at 75℃; for 12h; pH=8.0; Enzymatic reaction; Stage #2: With pyridoxal 5'-phosphate; Ruminococcus gnavus L-tryptophan decarboxylase In methanol; aq. phosphate buffer at 37℃; pH=8.0; Enzymatic reaction; | 14% |
5-methoxylindole
methyl magnesium iodide
diethyl ether
chloroacetonitrile
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
und Erwaermen des Reaktionsprodukts Natrium in Aethanol; |
5-methoxylindole
methyl magnesium iodide
chloroacetonitrile
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With diethyl ether Erwaermen des Reaktionsprodukts mit Natrium und Aethanol; |
(5-methoxy-2-oxo-2,3-dihydro-1H-indol-3-yl)acetonitrile
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With 2-methyl-propan-1-ol; sodium |
5-methoxytryptamine-2-carboxylic acid
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
With zinc(II) chloride at 180℃; |
5-methoxy-3-indoleglyoxylylamide
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 8h; Heating; | |
With lithium aluminium tetrahydride In tetrahydrofuran for 18h; Reflux; |
5-methoxy-3-(2-phthalimido-ethyl)-indole-2-carboxylic acid
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
With sulfuric acid for 0.166667h; Heating; microwave irradiation; |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 100 percent / Et3N 2: Et3SiH / trifluoroacetic acid 3: 63 percent / Na2WO4*2H2O; aq. H2O2 / methanol; H2O 4: 85 percent / BF3 5: NaOH / Heating View Scheme |
methyl 2-(1-H-indol-3-yl)ethylcarbamate
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Et3SiH / trifluoroacetic acid 2: 63 percent / Na2WO4*2H2O; aq. H2O2 / methanol; H2O 3: 85 percent / BF3 4: NaOH / Heating View Scheme | |
Multi-step reaction with 4 steps 1: 97 percent / Et3SiH / trifluoroacetic acid / 3 h / 60 °C 2: 65 percent / H2O2 / Na2WO4*2H2O / methanol; H2O / 0.5 h / 20 °C 3: 94 percent / BF3 / 0.67 h / Heating 4: 99 percent / aq. NaOH / methanol / 4 h / Heating View Scheme |
2,3-dihydro-Nb-methoxycarbonyltryptamine
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 63 percent / Na2WO4*2H2O; aq. H2O2 / methanol; H2O 2: 85 percent / BF3 3: NaOH / Heating View Scheme | |
Multi-step reaction with 3 steps 1: 65 percent / H2O2 / Na2WO4*2H2O / methanol; H2O / 0.5 h / 20 °C 2: 94 percent / BF3 / 0.67 h / Heating 3: 99 percent / aq. NaOH / methanol / 4 h / Heating View Scheme |
1-hydroxy-Nb-methoxycarbonyltryptamine
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / BF3 2: NaOH / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 94 percent / BF3 / 0.67 h / Heating 2: 99 percent / aq. NaOH / methanol / 4 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 85 percent / BF3*MeOH / 0.17 h / Heating 2: H2O View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: POCl3 / 0 °C 2: NH4OAc / 70 °C 3: LiAlH4 / tetrahydrofuran / Heating View Scheme | |
Multi-step reaction with 3 steps 1: diethyl ether / 6 h / Heating 2: NH3 / dioxane / 8 h / 20 °C 3: lithium aluminum hydride / tetrahydrofuran / 8 h / Heating View Scheme | |
Multi-step reaction with 5 steps 1.1: BuLi / tetrahydrofuran; hexane / 0.25 h / -10 °C 1.2: tetrahydrofuran; hexane / 3 h / 0 °C 2.1: 5.4 g / NBS / tetrahydrofuran; hexane / 3 h / -78 °C 3.1: t-BuLi / pentane; diethyl ether / 0.17 h / -78 °C 3.2: CuBr*SMe2 / pentane; diethyl ether / 0.25 h / -78 °C 3.3: 50 percent / BF3*Et2O / pentane; diethyl ether / 4 h / -78 °C 4.1: 89 percent / Bu4NF / tetrahydrofuran / 0.17 h / 20 °C 5.1: 65 percent / NH3; Na / tetrahydrofuran / 0.25 h / -78 °C View Scheme |
5-methoxyindole-3-carboxaldehyde
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NH4OAc / 70 °C 2: LiAlH4 / tetrahydrofuran / Heating View Scheme | |
Multi-step reaction with 3 steps 1: ammonium acetate / benzene / Reflux 2: sodium tetrahydroborate / tetrahydrofuran; methanol / 20 °C 3: palladium on activated charcoal; hydrogen / methanol / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: piperidine; acetic acid / benzene / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate / 1.5 h / Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 40 h / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: ammonium acetate / 1.5 h / Reflux; Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 36 h / 0 - 20 °C / Inert atmosphere View Scheme |
2-iodo-4-methoxylaniline
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 96 percent / 4-dimethylaminopyridine; pyridine / 14 h / 20 °C 2.1: 82 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C 3.1: tristrimethylsilylsilane; azoisobutyronitrile / toluene / 12 h / Heating 3.2: 74 percent / p-toluenesulfonic acid / toluene / 2 h / Heating 4.1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating 5.1: 84 percent / KOH / methanol / 9 h / Heating View Scheme |
N-(2-iodo-4-methoxyphenyl)methanesulfonamide
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 82 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C 2.1: tristrimethylsilylsilane; azoisobutyronitrile / toluene / 12 h / Heating 2.2: 74 percent / p-toluenesulfonic acid / toluene / 2 h / Heating 3.1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating 4.1: 84 percent / KOH / methanol / 9 h / Heating View Scheme |
2-[2-(1-methanesulfonyl-5-methoxy-1H-indol-3-yl)ethyl]isoindole-1,3-dione
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating 2: 84 percent / KOH / methanol / 9 h / Heating View Scheme |
N-[4-(1,3-dioxodihydroisoindol-2-yl)but-2-ynyl]-N-(2'-iodo-4'-methoxyphenyl)methanesulfonamide
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tristrimethylsilylsilane; azoisobutyronitrile / toluene / 12 h / Heating 1.2: 74 percent / p-toluenesulfonic acid / toluene / 2 h / Heating 2.1: 85 percent / hydrazine monohydrate / ethanol / 3 h / Heating 3.1: 84 percent / KOH / methanol / 9 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NH3 / dioxane / 8 h / 20 °C 2: lithium aluminum hydride / tetrahydrofuran / 8 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: ammonia / 1,4-dioxane / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 18 h / Reflux View Scheme |
1-benzyl-5-methoxy-1H-indole-3-acetamide
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60.5 percent / LiAlH4 / diethyl ether / 48 h / Heating 2: 66 percent / Na / tetrahydrofuran; liquid ammonia / 1.5 h / -33 °C View Scheme |
methyl 1-benzyl-5-methoxy-1H-indole-3-acetate
2-(5-methoxyindol-3-yl)ethylamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 83 percent / NH3 / methanol / 192 h / 20 °C 2: 60.5 percent / LiAlH4 / diethyl ether / 48 h / Heating 3: 66 percent / Na / tetrahydrofuran; liquid ammonia / 1.5 h / -33 °C View Scheme |
succinic acid anhydride
2-(5-methoxyindol-3-yl)ethylamine
3-<(5-methoxy-3-indolyl)ethylamino>propionic acid
Conditions | Yield |
---|---|
In chloroform at 0 - 5℃; for 0.25h; | 100% |
In dichloromethane at 20℃; for 18h; | 99% |
2-(5-methoxyindol-3-yl)ethylamine
acetic anhydride
5-methoxy-N-acetyl-tryptamine
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 100% |
In 1,2-dichloro-ethane at 0℃; for 1h; | 96% |
With triethylamine | 95% |
2-(5-methoxyindol-3-yl)ethylamine
formic acid ethyl ester
N-(2-(5-methoxy-1H-indol-3-yl)ethyl)formamide
Conditions | Yield |
---|---|
for 10h; Reflux; | 100% |
for 10h; Reflux; | 100% |
for 12h; Reflux; | 100% |
2-(5-methoxyindol-3-yl)ethylamine
Trifluoroacetaldehyde ethyl hemiacetal
6-methoxy-1-trifluoromethyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole
Conditions | Yield |
---|---|
at 110 - 120℃; for 5h; | 99.7% |
4-methyleneoxetan-2-one
2-(5-methoxyindol-3-yl)ethylamine
N-<2-(5-methoxy-1H-indol-3-yl)ethyl>-3-oxobutyramide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 24h; | 99% |
In dichloromethane at 0℃; for 12.5h; |
phthalic anhydride
2-(5-methoxyindol-3-yl)ethylamine
2-(2-(5-methoxy-1H-indol-3-yl)ethyl)isoindoline-1,3-dione
Conditions | Yield |
---|---|
With triethylamine In toluene for 24h; Reflux; Dean-Stark; | 99% |
at 206℃; | 88% |
With triethylamine In toluene for 24h; Reflux; | 87% |
2-(5-methoxyindol-3-yl)ethylamine
di-tert-butyl dicarbonate
3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 12h; | 99% |
With triethylamine In tetrahydrofuran at 10℃; for 1h; Inert atmosphere; | 99% |
With triethylamine In tetrahydrofuran at 10℃; for 1h; | 99% |
1-methyl-1H-indole-2,3-dione
2-(5-methoxyindol-3-yl)ethylamine
(S)-6'-methoxy-1-methyl-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one
Conditions | Yield |
---|---|
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In N,N-dimethyl-formamide at 40℃; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
2-(5-methoxyindol-3-yl)ethylamine
5-bromo-1-methyl-1H-indole-2,3-dione
5-bromo-6'-methoxy-1-methyl-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one
Conditions | Yield |
---|---|
With scandium(III) chloride; sodium sulfate In dichloromethane at 23℃; Pictet-Spengler cyclisation; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine at 20℃; for 18h; | 99% |
2-(5-methoxyindol-3-yl)ethylamine
acetyl chloride
5-methoxy-N-acetyl-tryptamine
Conditions | Yield |
---|---|
In dichloromethane at 25 - 30℃; Temperature; | 98.3% |
With triethylamine In dichloromethane at 20℃; | |
With triethylamine In dichloromethane at 0 - 20℃; for 5h; |
2-(5-methoxyindol-3-yl)ethylamine
2-bromoallyl bromide
2-bromo-N-[2-(5-methoxy-1H-indol-3-yl)ethyl]prop-2-en-1-amine
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 20℃; | 98% |
2-(5-methoxyindol-3-yl)ethylamine
2-(2'-phenylethynyl)benzoic acid
3-benzyl-3-hydroxy-2-(2-(5-methoxy-1H-indol-3-yl)ethyl)isoindolin-1-one
Conditions | Yield |
---|---|
Stage #1: 2-(2'-phenylethynyl)benzoic acid With tetrabutylammonium acetate In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Stage #2: 2-(5-methoxyindol-3-yl)ethylamine In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; regioselective reaction; | 98% |
2-(5-methoxyindol-3-yl)ethylamine
benzaldehyde
N-benzyl-2-(5-methoxy-1H-indol-3-yl)ethan-1-amine
Conditions | Yield |
---|---|
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde In methanol at 20℃; for 36h; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 1h; | 98% |
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde In methanol at 20℃; Stage #2: With sodium tetrahydroborate at 20℃; Borch Reduction; | 98% |
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde In methanol at 20℃; for 36h; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 1h; | |
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; benzaldehyde With sodium sulfate In methanol for 12h; Stage #2: With sodium tetrahydroborate In methanol at 0℃; |
2-(5-methoxyindol-3-yl)ethylamine
Glyoxilic acid
6-methoxy-2,3,4,9-tetrahydro-1H-β-carboline-1-carboxylic acid
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate at 20℃; for 24h; pH=5; Pictet-Spengler Synthesis; | 98% |
2-(5-methoxyindol-3-yl)ethylamine
2-((4-methoxyphenyl)ethynyl)benzoic acid
3-hydroxy-2-(2-(5-methoxy-1H-indol-3-yl)ethyl)-3-(4-methoxybenzyl)isoindolin-1-one
Conditions | Yield |
---|---|
Stage #1: 2-((4-methoxyphenyl)ethynyl)benzoic acid With tetrabutylammonium acetate In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Stage #2: 2-(5-methoxyindol-3-yl)ethylamine In water at 100℃; for 0.166667h; Microwave irradiation; Inert atmosphere; regioselective reaction; | 97% |
2-(5-methoxyindol-3-yl)ethylamine
dimethyl 2-ketoglutarate
methyl 8-methoxy-2,3,5,6,11,11b-hexahydro-3-oxo-1H-indolizino<8,7-b>indole-11b-carboxylate
Conditions | Yield |
---|---|
With acetic acid for 4h; Reflux; Inert atmosphere; | 97% |
2-(5-methoxyindol-3-yl)ethylamine
potassium thioacetate
5-methoxy-N-acetyl-tryptamine
Conditions | Yield |
---|---|
With tetrabutylammonium tetrafluoroborate In ethyl acetate at 20℃; Electrochemical reaction; | 97% |
Conditions | Yield |
---|---|
In toluene for 1h; Ambient temperature; | 96% |
2-(5-methoxyindol-3-yl)ethylamine
7-(trifluoromethyl)-3,4,5,6-tetrahydro-2H-azepine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 168h; Pictet-Spengler Synthesis; | 96% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane | 95% |
With acetic acid In methanol at 80℃; for 1h; | 83% |
With sulfuric acid Erhitzen des Reaktionsprodukts mit wss. H2SO4; |
2-(5-methoxyindol-3-yl)ethylamine
di-tert-butyl dicarbonate
benzenesulfonyl chloride
3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole
A
1-(benzenesulfonyl)-3-[2-[(tert-butyloxycarbonyl)amino]ethyl]-5-methoxy-1H-indole
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane | A n/a B 95% |
2-(5-methoxyindol-3-yl)ethylamine
1-benzylisatin
(S)-1-benzyl-6'-methoxy-2',3',4',9'-tetrahydrospiro[indoline-3,1'-pyrido[3,4-b]indol]-2-one
Conditions | Yield |
---|---|
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In N,N-dimethyl-formamide at 40℃; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; Pictet-Spengler Synthesis; | 95% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; Schlenk technique; | 95% |
2-(5-methoxyindol-3-yl)ethylamine
(4-fluorophenyl)glyoxal
(4-fluorophenyl)(6-methoxy-9H-pyrido[3,4-b]indol-1-yl)methanone
Conditions | Yield |
---|---|
Stage #1: 2-(5-methoxyindol-3-yl)ethylamine; (4-fluorophenyl)glyoxal In dichloromethane Stage #2: With montmorillonite K-10; palladium 10% on activated carbon In methanol; dichloromethane for 0.0833333h; Pictet-Spengler cyclisation; Stage #3: at 130℃; for 0.116667h; Microwave irradiation; | 94% |
With 5%-palladium/activated carbon; montmorillonite K10 Clay at 130℃; Microwave irradiation; |
2-(5-methoxyindol-3-yl)ethylamine
levulinic acid
8-Methoxy-2,3,5,6,11,11b-hexahydro-3-oxo-11b-methyl-1H-indolizino<8,7-b>indole
Conditions | Yield |
---|---|
at 180℃; under 11251.1 Torr; for 0.0333333h; Pictet-Spengler condensation; Microwave irradiation; Neat (no solvent); | 94% |
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