CAS No.6196-95-8,1,2-DIMETHYL-4-(1-PHENYL-ETHYL)-BENZENE Suppliers

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Synthetic route

: 95-47-6
o-xylene

: 93-96-9
bis(1-phenylethyl)ether

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iron(III) chloride; chloro-trimethyl-silane In 1,2-dichloro-ethane at 20℃; for 0.166667h; Friedel-Crafts Alkylation; Inert atmosphere;	100%

: 100-42-5
styrene

: 95-47-6
o-xylene

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With cross-linked poly acidic ionic liquids In N,N-dimethyl-formamide at 120℃; for 3h; Solvent; Temperature; High pressure;	99.67%
With phosphotungstic acid at 120℃; for 3h; Reagent/catalyst;	98.3%
With 12-tungstophosphoric acid supported 30percent triethylammonium acetate, P123 in micro/mesoporous silica at 119.84℃; for 3h; Catalytic behavior; Reagent/catalyst; Temperature; Friedel-Crafts Alkylation;	93.8%

: 100-42-5
styrene

: 95-47-6
o-xylene

A: 81749-28-2
1,2-dimethyl-2-(1-phenylethyl)benzene

B: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With immobilized 30percent 12-tungstophosphoric acid-imidazole(1H)-3-ium-3-triethoxysilylpropyl-1-(propyl-3-sulfonate) on mesoporous silica SBA-15 at 120℃; for 3h; Reagent/catalyst;	A n/a B 93.9%
With iron(III) chloride at 80℃; for 4h;
With SiO2-supported InCl2 at 80℃; for 3h;
With gold(III) chloride; silver hexafluoroantimonate In 1,2-dichloro-ethane at 50℃; for 5h; Inert atmosphere; Darkness; regioselective reaction;
With aminosilane-modified lanthanum-substituted mesoporous silica-supported phosphotungstic acid at 120℃; for 3h; regioselective reaction;

...Expand

: 95-47-6
o-xylene

: 92976-56-2
tert-butyldimethyl(1-phenylethoxy)silane

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 2.5h; Friedel-Crafts Alkylation; Inert atmosphere; regioselective reaction;	93%

: 95-47-6
o-xylene

: 14856-75-8
1-phenyl-1-trimethylsilyloxyethane

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 1h; Reagent/catalyst; Time; Friedel-Crafts Alkylation; Inert atmosphere; regioselective reaction;	92%

: 95-47-6
o-xylene

: 112473-30-0, 18442-52-9
triethyl(1-phenylethoxy)silane

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 1.5h; Friedel-Crafts Alkylation; Inert atmosphere; regioselective reaction;	91%

: 95-47-6
o-xylene

: 98-85-1, 13323-81-4
1-Phenylethanol

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
[Ir2(COD)2(SnCl3)2(Cl)2)(μ-Cl)2] In 1,2-dichloro-ethane at 80℃; for 12h;	89%
With 2,3,4,5-tetrafluorophenyl(dihydroxy)borane In nitromethane at 20℃; for 1h; Friedel-Crafts Alkylation;	88%
With triphenylphosphine ditriflate In dichloromethane at 20℃; for 1h; Friedel-Crafts benzylation;	79%

: 95-47-6
o-xylene

: 7214-61-1
(1-nitroethyl)benzene

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With tin(IV) chloride for 1h; Ambient temperature;	65%

: 95-47-6
o-xylene

: 93-96-9
bis(1-phenylethyl)ether

A: 98-85-1, 13323-81-4
1-Phenylethanol

B: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iron(III) chloride; Hexamethyldisiloxane In 1,2-dichloro-ethane at 20℃; for 0.5h; Friedel-Crafts Alkylation; Inert atmosphere;	A 14% B 22%
With iron(III) chloride In 1,2-dichloro-ethane at 20℃; for 0.5h; Friedel-Crafts Alkylation; Inert atmosphere;	A 11% B 9%

...Expand

: 100-42-5
styrene

: 95-47-6
o-xylene

A: 56525-86-1
1,3-diphenyl-1-(o-xylyl)butane

B: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With toluene-4-sulfonic acid; hydroquinone at 110℃; for 11.5h; Yield given. Yields of byproduct given;

...Expand

: 95-47-6
o-xylene

: 93-92-5, 50373-55-2
1-phenylethyl acetate

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With dihydrogen hexachloroplatinate at 80℃; for 1h; Friedel-Crafts alkylation;	99 % Chromat.
gold(III) chloride In nitromethane at 80℃; for 20h; Product distribution; Further Variations:; Catalysts; Solvents; Temperatures; Friedel-Crafts reaction;	99 % Chromat.
With iron(III) chloride at 50℃; for 20h; Friedel-Crafts alkylation;	99 % Chromat.
With 1-butyl-3-methylimidazolium tetrachloridoferrate(III) at 80℃; for 12h; Friedel-Crafts type benzylation; regioselective reaction;	98 %Chromat.

: 95-47-6
o-xylene

: 98-85-1, 13323-81-4
1-Phenylethanol

A: 81749-28-2
1,2-dimethyl-2-(1-phenylethyl)benzene

B: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iron(III) chloride at 80℃; for 24h; Friedel-Crafts alkylation;

...Expand

: 95-47-6
o-xylene

: 98-85-1, 13323-81-4
1-Phenylethanol

A: 7614-93-9
1,3-diphenyl-1-butene

B: 81749-28-2
1,2-dimethyl-2-(1-phenylethyl)benzene

C: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With bismuth(lll) trifluoromethanesulfonate at 100℃; for 1h; Friedel-Crafts-type benzylation;

...Expand

: 100-42-5
styrene

: 95-47-6
o-xylene

A: 7614-93-9
1,3-diphenyl-1-butene

B: 81749-28-2
1,2-dimethyl-2-(1-phenylethyl)benzene

C: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With iodine at 130℃; for 2h; Friedel-Crafts Reaction;

...Expand

: 98-85-1, 13323-81-4
1-Phenylethanol

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: pyridine / dichloromethane / 0 - 20 °C 2: 1-butyl-3-methylimidazolium tetrachloridoferrate(III) / 12 h / 80 °C View Scheme

: 14856-75-8
1-phenyl-1-trimethylsilyloxyethane

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: o-xylene; iron(III) chloride / 1,2-dichloro-ethane / 0.12 h / 20 °C / Inert atmosphere 2: iron(III) chloride; chloro-trimethyl-silane / 1,2-dichloro-ethane / 0.17 h / 20 °C / Inert atmosphere View Scheme
Multi-step reaction with 2 steps 1: o-xylene; iron(III) chloride / 1,2-dichloro-ethane / 0.12 h / 20 °C / Inert atmosphere 2: iron(III) chloride; Hexamethyldisiloxane / 1,2-dichloro-ethane / 0.5 h / 20 °C / Inert atmosphere View Scheme
Multi-step reaction with 2 steps 1: o-xylene; indium(III) chloride / 1,2-dichloro-ethane / 3 h / 20 °C / Inert atmosphere 2: iron(III) chloride / 1,2-dichloro-ethane / 6 h / 20 °C / Inert atmosphere View Scheme

: 95-47-6
o-xylene

: 14856-75-8
1-phenyl-1-trimethylsilyloxyethane

A: 93-96-9
bis(1-phenylethyl)ether

B: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 3h; Inert atmosphere;	A 58 %Spectr. B 42 %Spectr.

...Expand

: 2571-39-3
(3,4-dimethylphenyl)(phenyl)methanone

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C 1.2: -78 - 20 °C 2.1: (di-p-tolylmethyl)triethylsilane; C18H15FP(1+)*C24H20B(1-); bromobenzene-d5 / 24 h / 100 °C / 3040.2 Torr / Schlenk technique; Inert atmosphere; Cooling with liquid nitrogen View Scheme

: 38112-01-5
1-phenyl-1-(3,4-dimethylphenyl)ethylene

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With bromobenzene-d5; (di-p-tolylmethyl)triethylsilane; C18H15FP(1+)*C24H20B(1-) at 100℃; under 3040.2 Torr; for 24h; Schlenk technique; Inert atmosphere; Cooling with liquid nitrogen;

: 100-42-5
styrene

: 95-47-6
o-xylene

A: bis(1-phenyl ethanyl)orthoxylene

B: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

Conditions

Conditions	Yield
With aluminum (III) chloride; 1-n-butyl-3-methylimidazolim bromide at 30℃; for 1h; Catalytic behavior; Reagent/catalyst; Temperature; Overall yield = 98 %Chromat.;

...Expand

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

A: 95-65-8
3,4-Dimethylphenol

B: 98-86-2
acetophenone

C: 3637-01-2
3,4-dimethylacetophenone

D: 108-95-2
phenol

Conditions

Conditions	Yield
Stage #1: 1,2-dimethyl-4-(1-phenylethyl)benzene With oxygen; N-hydroxyphthalimide; 2,2'-azobis(isobutyronitrile) In acetonitrile at 75℃; under 760.051 Torr; for 6h; Stage #2: With sulfuric acid In water; acetonitrile at 0℃; for 0.5h;	A 46% B 50% C 2.7% D n/a
Stage #1: 1,2-dimethyl-4-(1-phenylethyl)benzene With oxygen; N-hydroxyphthalimide; 2,2'-azobis(isobutyronitrile) In acetonitrile at 75℃; under 760.051 Torr; for 6h; Stage #2: In acetonitrile at 0℃; for 1h; Product distribution / selectivity;	A 50% B 50% C 1% D n/a

...Expand

: 6196-95-8
1,2-dimethyl-4-(1-phenylethyl)benzene

: C16H18O2

Conditions

Conditions	Yield
With N-hydroxyphthalimide; 2,2'-azobis(isobutyronitrile); oxygen In acetonitrile at 75℃; under 760.051 Torr;

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Triumph International Development Limilted

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