Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:6258-66-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:6258-66-8
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:6258-66-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:6258-66-8
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:6258-66-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:6258-66-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:6258-66-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:6258-66-8
Min.Order:1 Kilogram
FOB Price: $50.0 / 100.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:6258-66-8
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:6258-66-8
Min.Order:0 Metric Ton
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Type:Other
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:6258-66-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:6258-66-8
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:6258-66-8
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:6258-66-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:6258-66-8
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:6258-66-8
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:6258-66-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry4-Chlorobenzyl mercaptanAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Cas:6258-66-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
FandaChem, a China-based chemical company, specialize in exporting 4-Chlorobenzyl mercaptan / C7H7ClS cas 6258-66-8 (Fandachem), Please contact us by email freely. Appearance:white crystalline powder Storage:Store in dry, dark
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Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryOur own factory produces direct sales with absolute price advantage Application:Pharmaceutical industry Transportation:By sea Port:Shanghai/tianjin
Cas:6258-66-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for
Cas:6258-66-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
Cas:6258-66-8
Min.Order:0
Negotiable
Type:Trading Company
inquiryKnown for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Prompt reaction, good quality and best service make us reliable and outstanding in this industry.Appearance:Detailed see specifications
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Min.Order:0
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Type:Lab/Research institutions
inquiry6258-66-8 Application:intermediate
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Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With pyrrolidine In acetonitrile at 20℃; | 95% |
Conditions | Yield |
---|---|
With hydrosulfide exchange resin In acetonitrile at 25℃; for 0.25h; | 93% |
With tetraethylammonium iodide; 1-(2-hydroxyethyl)-4,6-diphenylpyridin-2-thione In acetonitrile for 24h; Ambient temperature; | 72% |
With sodium hydrogensulfide |
S-(4-chlorobenzyl) ethanethioate
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With methanol; tetra-n-butylammonium cyanide In chloroform at 20℃; for 3h; | 92% |
Acid hydrolysis; |
1-(2-hydroxyethyl)-4,6-diphenylpyridin-2-thione
A
2,3-dihydro-5,7-diphenyloxazolo(3,2-a)pyridinium iodide
B
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With 1-chloro-4-(iodomethyl)benzene In benzene at 20℃; for 3h; various alkyl and aryl halogenides; | A n/a B 89% |
1-chloro-4-(iodomethyl)benzene
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With 1-(2-hydroxyethyl)-4,6-diphenylpyridin-2-thione In benzene at 20℃; for 3h; | 89% |
acetic anhydride
2-(4-chlorobenzyl)isothiouronium bromide
A
4-(4-Chloro-benzylsulfanyl)-6-methyl-[1,3,5]triazin-2-ylamine
B
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
In pyridine for 0.5h; Heating; | A 60% B n/a |
propionic acid anhydride
2-(4-chlorobenzyl)isothiouronium bromide
A
4-(4-Chloro-benzylsulfanyl)-6-ethyl-[1,3,5]triazin-2-ylamine
B
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
In pyridine for 0.5h; Heating; | A 57% B n/a |
4-chlorobenzyl dimethylcarbamodithioate
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium hydroxide |
1-Chloro-4-(chloromethyl)benzene
thiourea
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With ethanol Erwaermen des Reaktionsgemisches mit wss. NaOH; |
ethanol
dithiocarbonic acid O,S-bis-(4-chloro-benzyl ester)
phenylhydrazine
B
(4-chlorophenyl)methanethiol
ethanol
dithiocarbonic acid O-benzyl ester-S-(4-chloro-benzyl ester)
phenylhydrazine
A
3-phenyl-thiocarbazic acid O-benzyl ester
B
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With ethanol; potassium hydrosulfide |
S-(4-chlorobenzyl)isothiourea
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium hydroxide at 70℃; for 0.333333h; |
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; Rate constant; |
[(4-Chloro-benzylsulfanyl)-dimethylamino-methylene]-dimethyl-ammonium; iodide
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium hydroxide at 20℃; Rate constant; |
1-(4-Chloro-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium hydroxide; thiourea 1.) 170 deg C, 1 h; 2.) reflux, 3 h; Yield given. Multistep reaction; |
N-Acetylcysteine
A
(4-chlorophenyl)methanethiol
B
2-hydroxyethanethiol
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane at 25℃; Rate constant; pH 7.4; |
A
dioctyl disulfide
B
Octanethiol
C
para-chlorotoluene
D
1,2-bis(4-chlorophenyl)ethane
E
1-chloro-4-nonylbenzene
F
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With hydrogen In acetone at -78℃; under 3.5 Torr; for 0.0833333h; Mechanism; Product distribution; other alkyl substituted-benzyl sulfides and alkyl sulfides, competition with n-octyl benzyl sulfide, reaction rate relative to n-octyl benzyl sulfide, microwave generation of H from H2; | A 0.36 % Chromat. B 6.33 % Chromat. C 0.25 % Chromat. D 2.11 % Chromat. E 0.37 % Chromat. F n/a G n/a |
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
Stage #1: 4-Cl-benzyl halide With thiourea In ethanol Heating; Stage #2: With water; sodium hydroxide |
Thiobencarb
A
S-(4-chlorobenzyl) ethylthiocarbamate
B
S-(4-chlorobenzyl) acetyl(ethyl)thiocarbamate
C
4-chlorobenzaldehyde
D
(4-chlorophenyl)methanethiol
E
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With water; titanium(IV) oxide UV-irradiation; |
1-Chloro-4-(chloromethyl)benzene
A
1,1’-[thiobis(methylene)]bis[4-chlorobenzene]
B
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With N-Methyldiethanolamine; hydrogen sulfide In toluene at 49.84℃; Temperature; |
Conditions | Yield |
---|---|
With Lawessons reagent In toluene for 48h; Reflux; | |
Multi-step reaction with 3 steps 1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 25 °C / Inert atmosphere 2: diphenylether / 22 h / 200 °C 3: potassium hydroxide / methanol; water / 24 h / 25 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / methanol 2: Lawessons reagent / toluene / 48 h / Reflux View Scheme |
S-(4-chlorobenzyl) N,N-dimethylthiocarbamate
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water at 25℃; for 24h; |
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylether / 22 h / 200 °C 2: potassium hydroxide / methanol; water / 24 h / 25 °C View Scheme |
Conditions | Yield |
---|---|
With pyridine In diethyl ether for 0.5h; | 100% |
(4-chlorophenyl)methanethiol
Trichloroacetyl chloride
trichlorothioacetic acid S-(4-chlorobenzyl) ester
Conditions | Yield |
---|---|
for 2h; | 100% |
ethynyl p-tolyl sulfone
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 0℃; for 0.333333h; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In water | 100% |
(4-chlorophenyl)methanethiol
5-bromo-2(trifluoromethyl)pyridine
5-{[(4-chlorophenyl)methyl]thio}-2-(trifluoromethyl)pyridine
Conditions | Yield |
---|---|
Stage #1: (4-chlorophenyl)methanethiol With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.166667h; Stage #2: 5-bromo-2(trifluoromethyl)pyridine In N,N-dimethyl-formamide at 20℃; for 4h; | 100% |
1-adamantyl bromomethyl ketone
(4-chlorophenyl)methanethiol
1-adamantan-1-yl-2-(4-chlorobenzylsulfanyl)ethanone
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; | 99% |
With triethylamine In acetonitrile at 20℃; for 18h; | 99% |
(4-chlorophenyl)methanethiol
3-crotonoyl-1,3-oxazolidin-2-one
Conditions | Yield |
---|---|
With C43H36F6N4OS In chloroform at -20℃; for 72h; optical yield given as %ee; enantioselective reaction; | 99% |
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tetrakis(actonitrile)copper(I) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; for 0.166667h; Inert atmosphere; Sealed tube; chemoselective reaction; | 99% |
With pyridine; (1,2-dimethoxyethane)dichloronickel(II); (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile In N,N-dimethyl-formamide; acetonitrile at 20℃; for 0.5h; Inert atmosphere; Sealed tube; Irradiation; | 83% |
diethyl (bromoethynyl)phosphonate
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tetrakis(actonitrile)copper(I) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; for 0.166667h; Inert atmosphere; Sealed tube; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With C39H60N4O4; yttrium(III) trifluoromethanesulfonate In dichloromethane at -60℃; for 12h; enantioselective reaction; | 99% |
(4-chlorophenyl)methanethiol
(4S)-N-tert-butoxycarbonyl-4-[[(4'-methylbenzenesulfonyl)oxy]methyl]-2,2-dimethyl-1,3-oxazolidine
4(S)-4-(4-chlorobenzylthiomethyl)-2,2-dimethyloxazolidine-3-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: (4-chlorophenyl)methanethiol With sodium hydride In N,N-dimethyl-formamide at 20℃; Stage #2: (4S)-N-tert-butoxycarbonyl-4-[[(4'-methylbenzenesulfonyl)oxy]methyl]-2,2-dimethyl-1,3-oxazolidine In N,N-dimethyl-formamide at 40℃; for 1h; | 98% |
With sodium hydride In N,N-dimethyl-formamide at 60 - 80℃; |
pyrrolidine
carbon dioxide
(4-chlorophenyl)methanethiol
C12H14ClNOS
Conditions | Yield |
---|---|
Stage #1: pyrrolidine; carbon dioxide In dimethyl sulfoxide at 20℃; for 0.5h; Stage #2: (4-chlorophenyl)methanethiol With triphenylphosphine; diethylazodicarboxylate In dimethyl sulfoxide at 20℃; for 3h; Further stages.; | 98% |
Conditions | Yield |
---|---|
With pyridine; (1,2-dimethoxyethane)dichloronickel(II); (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile In N,N-dimethyl-formamide; acetonitrile at 20℃; for 0.5h; Inert atmosphere; Sealed tube; Irradiation; | 98% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tetrakis(actonitrile)copper(I) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; for 0.166667h; Inert atmosphere; Sealed tube; chemoselective reaction; | 98% |
With pyridine; (1,2-dimethoxyethane)dichloronickel(II); (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile In N,N-dimethyl-formamide; acetonitrile at 20℃; for 0.5h; Inert atmosphere; Sealed tube; Irradiation; | 78% |
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tetrakis(actonitrile)copper(I) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; for 0.166667h; Reagent/catalyst; Inert atmosphere; Sealed tube; chemoselective reaction; | 98% |
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; tetrakis(actonitrile)copper(I) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; for 0.166667h; Reagent/catalyst; Inert atmosphere; Sealed tube; chemoselective reaction; | 98% |
4-isothiocyanato-1-(methylsulfinyl)-1-butene
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In ethanol; water at 20℃; Inert atmosphere; | 97.1% |
(4-chlorophenyl)methanethiol
bis(4-chlorobenzyl)disulfide
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina for 0.0333333h; microwave irradiation; | 97% |
With (tetrabenzoporphinato)iron(II) In tetrahydrofuran at 20℃; under 760.051 Torr; for 0.333333h; | 97% |
With oxygen In water at 100℃; under 30002.4 Torr; for 2h; | 95% |
Methoxycarbonylsulfenyl chloride
(4-chlorophenyl)methanethiol
(p-Chlorobenzyl)sulfenyl methyl thiocarbonate
Conditions | Yield |
---|---|
97% |
(4-chlorophenyl)methanethiol
(7-methylimidazo<1,2-a>pyridin-3-yl)methanol
Conditions | Yield |
---|---|
With acetic acid at 80℃; for 2h; | 97% |
methyl shikimate
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With sodium methylate In methanol at 20℃; for 2h; | 97% |
benzaldehyde
(4-chlorophenyl)methanethiol
α.α-Bis-(4-chlor-benzylmercapto)-toluol
Conditions | Yield |
---|---|
With butyl ethyl phenyl selenonium tetrafluoroborate at 20℃; for 2h; | 97% |
(4-chlorophenyl)methanethiol
NBD chloride
4-((4-chlorobenzyl)thio)-7-nitrobenzo[c][1,2,5]oxadiazole
Conditions | Yield |
---|---|
With sodium methylate In ethanol at 20℃; for 1h; | 97% |
With sodium methylate In ethanol at 20℃; for 1h; | 97% |
In ethanol for 0.416667h; Reflux; Alkaline conditions; | 83% |
(4-chlorophenyl)methanethiol
(1S,9aR)-1-(chloromethyl)octahydro-2H-quinolizine
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 6h; Heating; | 96% |
Conditions | Yield |
---|---|
Stage #1: 6-Chloropurine riboside With pyridine; trityl resin for 48h; Stage #2: (4-chlorophenyl)methanethiol With triethylamine In methanol at 55℃; for 5h; Stage #3: With chlorotriisopropylsilane; trifluoroacetic acid In dichloromethane for 0.166667h; | 96% |
(4-chlorophenyl)methanethiol
1,3-diphenyl-propen-3-one
(3R)-3-[(4-chlorobenzyl)sulfanyl]-1,3-diphenylpropan-1-one
Conditions | Yield |
---|---|
With C38H54ClFeN2O2 In 1,2-dichloro-ethane at -5℃; Temperature; enantioselective reaction; | 96% |
With C32H28F6N4O3 In toluene at 20℃; for 24h; sulfa-Michael addition; optical yield given as %ee; enantioselective reaction; | 80% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; BF4(1-)*C21H22N3O(1+); copper(II) bis(trifluoromethanesulfonate) In toluene at 20℃; for 4h; Molecular sieve; enantioselective reaction; | 96% |
1-bromo-2-(4-methoxyphenyl)acetylene
(4-chlorophenyl)methanethiol
Conditions | Yield |
---|---|
With pyridine; (1,2-dimethoxyethane)dichloronickel(II); (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile In N,N-dimethyl-formamide; acetonitrile at 20℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Sealed tube; Irradiation; | 96% |
With 2,6-dimethylpyridine; tetrakis(actonitrile)copper(I) hexafluorophosphate; 4,4'-di-tert-butyl-2,2'-bipyridine In acetonitrile at 20℃; for 0.166667h; Inert atmosphere; Sealed tube; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60 - 120℃; for 28h; | 95% |
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