Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:104-83-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryTalent Advantages: The Company features strong technical strength, possesses an efficient and cohesive management team, and enthusiastic and creative talents. The whole team has excellent execution ability, faces the market competition with firm be
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:104-83-6
Min.Order:1 Metric Ton
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Type:Manufacturers
inquiryProduct Description Product Name 4-Chlorobenzyl chloride CAS No. 104-83-6 Appearance Colorless liquid or crystal Assay ≥99% Capacity 1000mt/year Min.packing 100gram
Cas:104-83-6
Min.Order:1 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryTechnology: Technology innovation is our eternal pursuit,or we will be left behind.Our technology experts,all from famous universities and institutes,has rich experience and high achievements in chemical research.This makes sure that our technology
Cas:104-83-6
Min.Order:1 Kilogram
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Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:104-83-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:104-83-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryCAS Number 104-83-6 Product Name 4-chlorobenzyl Chloride Synonyms (4-chlorophenyl)methylchloride; ,4-dichlorotoluene; 1-chloro-4
Cas:104-83-6
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryWe are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat
Cas:104-83-6
Min.Order:1 Kilogram
FOB Price: $4.0 / 5.0
Type:Lab/Research institutions
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White to off white powder Storage:Store in sealed containers
Cas:104-83-6
Min.Order:100 Gram
Negotiable
Type:Other
inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:104-83-6
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:104-83-6
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:104-83-6
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:104-83-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry4-Chlorobenzyl chlorideAppearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by
Product name: 4-Chlorobenzyl Chloride CAS No.:104-83-6 Molecule Formula:C7H6Cl2 Molecule Weight:161.03 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTIN
Cas:104-83-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:104-83-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
1.High quality 2.High purity 3.Best price 4.Best service 5.Professional manufacturer 6.Loyal and honest supplier 7.Fast response to customer within 6 hours Appearance:Colorless to white Crystalline Low Melting Solid Storage:Store at R
Superior quality, moderate price & quick delivery. Appearance:colorless transparent liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used for Pesticide
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:104-83-6
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers 69.Safe and fa
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:104-83-6
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Conditions | Yield |
---|---|
With tetrachloromethane; cross-linked polymer (containing 2.50 mmol of phosphine/g) for 3h; Heating; | 100% |
With ziconium(IV) oxychloride octahydrate; lithium chloride In ethanol; water at 90℃; for 1.5h; | 95% |
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide at 20℃; for 0.25h; chemoselective reaction; | 94% |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium chloride; tetrabutyl-ammonium chloride In water at 20℃; Irradiation; Green chemistry; | 94% |
With N-chloro-succinimide; N-hydroxyphthalimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 80℃; for 3h; Reagent/catalyst; Time; Sealed tube; Inert atmosphere; | 93% |
With N-hydroxyphthalimide; carbon tetrabromide; trichloroisocyanuric acid; copper(II) acetate monohydrate In dichloromethane at 25℃; for 17h; | 73% |
Conditions | Yield |
---|---|
With dichloromethylsilane; iron(III) chloride In 1,2-dimethoxyethane for 3h; Heating; | 92% |
With chloro-trimethyl-silane; thionyl chloride; 1,1,3,3-Tetramethyldisiloxane; zinc(II) iodide at 70℃; for 0.75h; | 85% |
With indium(III) hydroxide; dimethylmonochlorosilane In chloroform at 20℃; for 2h; | 83% |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / ethanol / 0 - 20 °C / Inert atmosphere 2: thionyl chloride / Reflux View Scheme |
4-chlorophenylacetic Acid
A
1-Chloro-4-(chloromethyl)benzene
B
4-chlorobenzyl bromide
Conditions | Yield |
---|---|
With tetra-N-butylammonium tribromide; 1,3-dichloro-[1,3,5]triazinane-2,4,6-trione In dichloromethane at 20℃; for 2h; Time; Reagent/catalyst; Concentration; Photolysis; | A 6% B 86% |
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With indium(III) hydroxide In chloroform at 20℃; for 2h; | 83% |
Conditions | Yield |
---|---|
With tert-butylhypochlorite; Ag(Phen)2OTf In acetonitrile at 20℃; for 4h; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With triethylsilane; acetyl chloride; tin(ll) chloride In dichloromethane for 12h; Ambient temperature; | 79% |
(4-chlorobenzyl)(fluoromethyl)sulfane
A
monofluoromethylsulfonyl chloride
B
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With water; chlorine In dichloromethane at -5℃; | A 69% B 74% |
C7H6Cl2S
A
bis(4-chlorobenzyl)disulfide
B
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; pentane at 20 - 23℃; for 24h; | A 69% B 17% |
para-Chlorobenzyl alcohol
A
bis(4-chlorobenzyl) ether
B
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In neat (no solvent) at 70 - 75℃; for 24h; Green chemistry; chemoselective reaction; | A 16 %Spectr. B 63% |
styrene
4-chlorobenzylsulfonyl chloride
A
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
dichlorotris(triphenylphosphine)ruthenium(II) at 80℃; for 72h; | A 52% B 21% |
4-chlorophenylacetic Acid
A
1-chloro-4-(dibromomethyl)benzene
B
1-Chloro-4-(chloromethyl)benzene
C
4-chlorobenzyl bromide
Conditions | Yield |
---|---|
With trichloroisocyanuric acid; tetra-N-butylammonium tribromide In dichloromethane at 20℃; for 2h; Reagent/catalyst; Photolysis; | A 12% B 17% C 37% |
A
Ν-(4-bromobenzyl)benzamide
B
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With phosphorus pentachloride at 130℃; |
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With phosphorus pentachloride at 110℃; |
B
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With phosphorus pentachloride at 110℃; |
Conditions | Yield |
---|---|
With iodine durch Chlorierung; |
benzyl chloride
A
1-Chloro-4-(chloromethyl)benzene
B
1-chloro-2-(chloromethyl)benzene
Conditions | Yield |
---|---|
With iodine at 30 - 40℃; beim Chlorieren; |
chloromethyl methyl ether
(E)-3-Ureido-but-2-enoic acid ethyl ester
chlorobenzene
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With sulfuric acid at 25℃; | |
With zinc(II) chloride at 65℃; |
Conditions | Yield |
---|---|
With hydrogenchloride; zinc(II) chloride |
Conditions | Yield |
---|---|
With zinc(II) chloride at 65℃; | |
With sulfuric acid at 25℃; |
Conditions | Yield |
---|---|
With hydrogenchloride; formaldehyd; zinc(II) chloride |
C7H6Cl(1+)
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With tertiary butyl chloride In gaseous matrix at 600℃; chloride affinity; |
(4-chlorobenzyl)trimethylsilane
oxovanadium(V) ethoxydichloride
A
1-chloro-4-(ethoxymethyl)benzene
B
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
In acetonitrile Product distribution; -30 deg C, 2 h; RT, 4 h; |
para-bromotoluene
A
para-chlorotoluene
B
1-Chloro-4-(chloromethyl)benzene
C
4-chlorobenzyl bromide
D
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With sodium chlorite; trichloroacetic acid In dichloromethane for 3h; Chlorination; substitution; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 17 % Chromat. D 25 % Chromat. |
para-bromotoluene
A
para-chlorotoluene
B
1-Chloro-4-(chloromethyl)benzene
C
1-bromomethyl-4-bromobenzene
D
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With sodium chlorite; trichloroacetic acid In dichloromethane for 3h; Bromination; chlorination; substitution; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 20 % Chromat. D 25 % Chromat. |
Conditions | Yield |
---|---|
beim Chlorieren; |
hydrogenchloride
formaldehyd
(E)-3-Ureido-but-2-enoic acid ethyl ester
chlorobenzene
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
lithium tetrakis(pentafluorophenyl)borate for 8h; Friedel-Crafts benzylation; Heating; | 100% |
With phosphonic Acid at 150℃; for 36h; Inert atmosphere; | 56% |
aluminium trichloride In nitromethane at 20℃; Rate constant; | |
With aluminium trichloride |
1-Chloro-4-(chloromethyl)benzene
4-chlorobenzyl azide
Conditions | Yield |
---|---|
With sodium azide In water at 80℃; for 4h; | 100% |
With sodium azide In N,N-dimethyl-formamide at 60℃; for 6h; Inert atmosphere; regioselective reaction; | 91% |
With sodium azide In dimethyl sulfoxide at 20℃; for 5h; | 86% |
4-phenyl-1H-pyrrole-3-carboxylic acid ethyl ester
1-Chloro-4-(chloromethyl)benzene
1-(4-Chloro-benzyl)-4-phenyl-1H-pyrrole-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; | 100% |
4-nitro-phenol
1-Chloro-4-(chloromethyl)benzene
1-chloro-4-((4-nitrophenoxy)methyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 78℃; for 5h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 24h; Williamson Ether Synthesis; | |
With potassium carbonate In N,N-dimethyl-formamide Reflux; |
1-Chloro-4-(chloromethyl)benzene
phenol
1-chloro-4-(phenoxymethyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 78℃; for 5h; | 100% |
With potassium carbonate; sodium iodide In acetonitrile Reflux; | 93% |
With caesium carbonate In neat (no solvent) for 16h; Reagent/catalyst; Milling; Green chemistry; | 72% |
1-Chloro-4-(chloromethyl)benzene
4-(4-nitro-1H-pyrrol-3-yl)-pyridine
Conditions | Yield |
---|---|
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate In dichloromethane; water at 20℃; for 20h; | 100% |
1-Chloro-4-(chloromethyl)benzene
5-bromosalicyclaldehyde
5-bromo-2-((4-chlorobenzyl)oxy)benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 0.5h; Stage #2: 1-Chloro-4-(chloromethyl)benzene In DMF (N,N-dimethyl-formamide) at 65℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 4h; | 98% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 98.9% |
With caesium carbonate In N,N-dimethyl-formamide at 60℃; for 2h; |
2,3-bis(methoxycarbonyl)phenol
1-Chloro-4-(chloromethyl)benzene
3-(4-chloro-benzyloxy)-phthalic acid dimethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In acetone Heating / reflux; | 100% |
5-deoxy-2,3:6,7-di-O-diethylidene-1-O-(4,4'-dimethoxytriphenylmethyl)-D-allo-heptan-1-itol
1-Chloro-4-(chloromethyl)benzene
4-O-(4-chlorobenzyl)-5-deoxy-2,3:6,7-di-O-diethylidene-1-O-(4,4'-dimethoxytriphenylmethyl)-D-allo-heptan-1-itol
Conditions | Yield |
---|---|
Stage #1: 5-deoxy-2,3:6,7-di-O-diethylidene-1-O-(4,4'-dimethoxytriphenylmethyl)-D-allo-heptan-1-itol With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 1-Chloro-4-(chloromethyl)benzene In N,N-dimethyl-formamide at 20℃; for 2h; | 100% |
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
Stage #1: 2-[(4-benzyl-5-{[4-(2-methoxyphenyl)piperazin-1-yl]methyl}-4H-1,2,4-triazol-3-yl)thio]-1-(4-chlorophenyl)ethanol With sodium hydride In tetrahydrofuran at 100℃; for 0.166667h; Sealed tube; Microwave irradiation; Stage #2: 1-Chloro-4-(chloromethyl)benzene In tetrahydrofuran at 125℃; for 0.75h; Time; Temperature; Sealed tube; Microwave irradiation; | 100% |
ethyl 4-(p-chlorophenyl)-pyrrole-3-carboxylate
1-Chloro-4-(chloromethyl)benzene
1-(4-Chloro-benzyl)-4-(4-chloro-phenyl)-1H-pyrrole-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; | 99.9% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 99.3% |
With caesium carbonate In N,N-dimethyl-formamide at 60℃; for 2h; |
1-Chloro-4-(chloromethyl)benzene
bis(4-chlorobenzyl)disulfide
Conditions | Yield |
---|---|
With piperidine; tetrathio molybdate (VI) In N,N-dimethyl-formamide at 25℃; for 1h; | 99% |
With PEG-400; sodium hydroxide; sulfur In benzene at 65℃; for 1h; | 97% |
With sulfur; PEG-400; sodium hydroxide In N,N-dimethyl-formamide at 65 - 70℃; for 4h; | 97% |
1,2:5,6-diacetone-D-glucose
1-Chloro-4-(chloromethyl)benzene
3-O-(p-chlorobenzyl)-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 50℃; for 4.5h; | 99% |
With potassium hydroxide In tetrahydrofuran for 29h; Heating; | 98% |
carbon monoxide
1-Chloro-4-(chloromethyl)benzene
diethylamine
Thiobencarb
Conditions | Yield |
---|---|
Stage #1: carbon monoxide; diethylamine With potassium carbonate; sulfur In dimethyl sulfoxide at 20℃; under 760 Torr; for 5h; Stage #2: 1-Chloro-4-(chloromethyl)benzene In dimethyl sulfoxide at 20℃; for 1h; | 99% |
With sulfur; selenium In tetrahydrofuran 1.) 30 deg C; 2.) rt.; | 90% |
Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With benzyl alcohol; ethanol; N-benzyl-N,N,N-triethylammonium chloride at 80℃; for 2h; | 99% |
1-Chloro-4-(chloromethyl)benzene
1-[(1,1-dimethylethoxy)carbonyl]-2-[(phenylmethoxy)carbonyl]-2-methylhydrazine
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate In acetonitrile at 50℃; for 24h; Alkylation; | 99% |
1-methoxy-2-methyl-1-trimethylsiloxy-1-propene
1-Chloro-4-(chloromethyl)benzene
3-(4-chlorophenyl)-2,2-dimethylpropanoic acid methyl ester
Conditions | Yield |
---|---|
With indium(III) bromide In dichloromethane at 20℃; for 12h; | 99% |
Stage #1: 1-methoxy-2-methyl-1-trimethylsiloxy-1-propene; 1-Chloro-4-(chloromethyl)benzene With indium(III) bromide In dichloromethane at 20℃; for 12h; Stage #2: With water; sodium hydrogencarbonate In dichloromethane Saturated solution; | 99 %Spectr. |
1-Chloro-4-(chloromethyl)benzene
(E)-1,2-di(4-chlorophenyl)ethene
Conditions | Yield |
---|---|
With benzyl phenyl sulfoxide; potassium tert-butylate at 80℃; for 12h; Green chemistry; stereoselective reaction; | 99% |
With benzyl phenyl sulfoxide; potassium tert-butylate at 80℃; for 12h; Inert atmosphere; | 99% |
With potassium phenyl selenide In 1,2-dimethoxyethane for 0.283333h; Inert atmosphere; Sealed tube; | 97% |
1-Chloro-4-(chloromethyl)benzene
3-oxo-2,8-diazaspiro<4.5>decane-8-carboxylic acid tert-butyl ester
C20H27ClN2O3
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; Reflux; | 99% |
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 2h; | 99% |
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
Stage #1: 1α,2β,3β-trihydroxy-olean-12-en-28-oic acid With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: 1-Chloro-4-(chloromethyl)benzene In N,N-dimethyl-formamide at 20℃; | 98.8% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 98.7% |
With caesium carbonate In N,N-dimethyl-formamide at 60℃; for 2h; | |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 4h; |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile for 0.5h; Alkylation; Heating; | 98.3% |
2,3-dimethyl-2,3-diaminobutane
potassium methacrylate
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
In toluene | 98.2% |
ethyl 1-(4-chlorobenzyl)nipecotate
1-Chloro-4-(chloromethyl)benzene
Conditions | Yield |
---|---|
With LiOH; sodium hydrogencarbonate In tetrahydrofuran; water; acetonitrile | 98.2% |
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