As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryTIANFUCHEM-- 589-17-3--High purity 4-Bromobenzyl chloride factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable
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inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
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inquiry4-Bromobenzyl chloride Chemical Properties Melting point 36-40 °C Boiling point 136-139 °C (27 mmHg) density 1.3431 (rough estimate) refractive index 1.5750 (estimate) Fp 106-107°C/10mm form Powder and Granules col
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
4-Bromobenzyl chloride cas 589-17-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryKnown for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Conditions | Yield |
---|---|
With oxalyl dichloride In dichloromethane at 20℃; Appel Halogenation; Reflux; | 98% |
With thionyl chloride In dichloromethane at 0 - 20℃; | 95% |
With thionyl chloride Inert atmosphere; | 95% |
1,1-dimethoxy-1-(4-bromophenyl)methane
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With triethylsilane; acetyl chloride; tin(ll) chloride In dichloromethane for 5h; Ambient temperature; | 92% |
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium chloride for 1h; High speed ball milling; Neat (no solvent); neat (no solvent, solid phase); | 90% |
Multi-step reaction with 2 steps 1: natrium carbonate 2: fuming hydrochloric acid / 150 °C View Scheme |
Conditions | Yield |
---|---|
With sodium hypochlorite; bis(2,2'-bipyridine)dichloronickel(II) In acetonitrile for 0.666667h; Ambient temperature; Yields of byproduct given; | A 85% B n/a |
Conditions | Yield |
---|---|
With N-chloro-succinimide; tetrachlorosilane In acetonitrile at 60 - 70℃; for 8h; | 75% |
With N-chloro-succinimide; N-hydroxyphthalimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 80℃; for 16h; Time; Sealed tube; Inert atmosphere; | 38% |
durch Chlorierung; |
formaldehyd
bromobenzene
A
2-bromobenzylchloride
B
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride; tin(IV) chloride die Trennung der Isomeren erfolgt durch Abkuehlen auf -15grad; |
bromobenzene
bis(2-chloromethyl)ether
(E)-3-Ureido-but-2-enoic acid ethyl ester
A
bis(4-bromophenyl)methane
B
p-bromobenzyl chloride
bromobenzene
bis(2-chloromethyl)ether
A
bis(4-bromophenyl)methane
B
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With zinc(II) chloride | |
With zinc(II) chloride |
Conditions | Yield |
---|---|
With phosphorus pentachloride folgend Destillieren; |
Conditions | Yield |
---|---|
Bromierung; |
Conditions | Yield |
---|---|
(i) HCl, (heating), (ii) /BRN= 1236661/, ZnCl2, HCl; Multistep reaction; |
para-bromotoluene
A
para-chlorotoluene
B
1-Chloro-4-(chloromethyl)benzene
C
4-chlorobenzyl bromide
D
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With sodium chlorite; trichloroacetic acid In dichloromethane for 3h; Chlorination; substitution; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 17 % Chromat. D 25 % Chromat. |
para-bromotoluene
A
para-chlorotoluene
B
1-Chloro-4-(chloromethyl)benzene
C
1-bromomethyl-4-bromobenzene
D
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With sodium chlorite; trichloroacetic acid In dichloromethane for 3h; Bromination; chlorination; substitution; Further byproducts given; | A 20 % Chromat. B 18 % Chromat. C 20 % Chromat. D 25 % Chromat. |
hydrogenchloride
formaldehyd
bromobenzene
tin(IV) chloride
A
2-bromobenzylchloride
B
p-bromobenzyl chloride
Conditions | Yield |
---|---|
Product distribution; folgend Vakuumdestillation; |
sulfuryl dichloride
para-bromotoluene
dibenzoyl peroxide
A
para-chlorotoluene
B
1-Chloro-4-(chloromethyl)benzene
C
1-bromomethyl-4-bromobenzene
D
p-bromobenzyl chloride
Conditions | Yield |
---|---|
at 110℃; |
phosphorus pentachloride
p-bromobenzyl chloride
Conditions | Yield |
---|---|
folgenden Destillieren im Vakuum; |
phosphorus pentachloride
B
p-bromobenzyl chloride
Conditions | Yield |
---|---|
at 130℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4; diethyl ether 2: benzene; pyridine; thionyl chloride View Scheme |
para-bromotoluene
A
para-chlorotoluene
B
p-bromo-α,α-dichlorotoluene
C
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With tetrachloromethane at 250℃; for 7h; Inert atmosphere; Autoclave; | A 24 %Spectr. B 23 %Spectr. C 27 %Spectr. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C 2: thionyl chloride / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2: thionyl chloride / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / methanol / 0.17 h / 20 °C / Cooling with ice 2: thionyl chloride; dmap / dichloromethane / 0.17 h / 20 °C / Cooling with ice View Scheme | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / ethanol / 0 - 20 °C / Inert atmosphere 2: thionyl chloride / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: methanol; sodium tetrahydroborate / 2 h / 0 °C 2: thionyl chloride; 1,2,3-Benzotriazole / dichloromethane / 1.08 h View Scheme |
Conditions | Yield |
---|---|
With pyridine; thionyl chloride In dichloromethane | A 30.1 %Spectr. B 35.6 %Spectr. |
Conditions | Yield |
---|---|
Stage #1: p-bromobenzyl chloride With bis(tri-t-butylphosphine)palladium(0); oxygen In toluene at 20℃; for 0.0166667h; Schlenk technique; Stage #2: phenyllithium In toluene at 0℃; for 0.0833333h; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 78℃; for 5h; | 99% |
With methanol; sodium methylate |
Conditions | Yield |
---|---|
With potassium hydroxide; Aliquat 336 for 3h; Heating; | 99% |
2-biphenyl-3yl-acetic acid methyl ester
p-bromobenzyl chloride
2-biphenyl-3-yl-3-(4-bromo-phenyl)-propionic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: 2-biphenyl-3yl-acetic acid methyl ester With lithium hexamethyldisilazane In tetrahydrofuran at -78 - -40℃; for 1.25h; Stage #2: p-bromobenzyl chloride In tetrahydrofuran at -40 - 20℃; Further stages.; | 99% |
phenylacetylene
p-bromobenzyl chloride
1-(4-bromobenzyl)-4-phenyl-1H-1,2,3-triazole
Conditions | Yield |
---|---|
With sodium azide; sodium L-ascorbate In water at 50℃; for 3h; Huisgen Cycloaddition; Green chemistry; | 99% |
With sodium azide In water at 20℃; for 5h; Green chemistry; | 97% |
With sodium azide In ethanol; water at 20℃; for 0.133333h; Sonication; | 90% |
With copper(l) iodide; sodium azide; eosin Y disodium salt In ethanol; water at 20℃; for 2h; Irradiation; Green chemistry; regioselective reaction; | 86% |
With sodium azide In water at 30℃; for 24h; regioselective reaction; | 83% |
Conditions | Yield |
---|---|
Stage #1: acetone oxime With potassium hydroxide; lithium hydroxide In N,N-dimethyl acetamide; water at 50℃; Stage #2: p-bromobenzyl chloride In N,N-dimethyl acetamide; water at 65℃; for 2.25h; | 98.28% |
p-bromobenzyl chloride
Conditions | Yield |
---|---|
Stage #1: p-bromobenzyl chloride With n-butyllithium; Triisopropyl borate In tetrahydrofuran; hexane at -78℃; for 2h; Stage #2: With potassium hydrogen difluoride In tetrahydrofuran; hexane; water at -78 - 20℃; | 98% |
Stage #1: p-bromobenzyl chloride With n-butyllithium; Triisopropyl borate In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: With potassium hydrogen bifluoride In tetrahydrofuran; hexane; water at -78 - 20℃; | 98% |
p-bromobenzyl chloride
p-bromobenzylazide
Conditions | Yield |
---|---|
With sodium azide; potassium iodide In water; acetone at 20℃; for 60h; Inert atmosphere; | 98% |
With sodium azide In acetonitrile at 80℃; for 20h; | 85% |
With sodium azide; triethylamine In water; tert-butyl alcohol at 20℃; for 0.5h; |
Conditions | Yield |
---|---|
Stage #1: diethyl malonate With sodium ethanolate In ethanol at 20℃; for 0.5h; Stage #2: p-bromobenzyl chloride In ethanol at 0 - 20℃; for 1h; | 98% |
m-tolylboronic acid
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate In water; toluene at 80℃; for 2h; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere; | 98% |
thiomorpholine 1,1-dioxide
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 48h; | 97% |
8-chloro-[1,2,4]triazolo[4,3-a]pyridine-3(2H)-thione
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 90℃; for 0.25h; Microwave irradiation; | 96% |
With sodium hydroxide In N,N-dimethyl-formamide at 90℃; for 0.25h; Microwave irradiation; | 89% |
Conditions | Yield |
---|---|
In acetonitrile for 2h; Heating; | 95% |
2,5-dihydroxycyclohepta-2,4,6-trien-1-one
p-bromobenzyl chloride
2,5-bis(4-bromobenzyloxy)tropone
Conditions | Yield |
---|---|
With sodium hydride In N,N,N,N,N,N-hexamethylphosphoric triamide at 60℃; for 13h; | 95% |
5-(4-methylbenzylidene)-2-thioxoimidazolidin-4-one
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With caesium carbonate In ethanol at 20℃; for 25h; | 95% |
p-bromobenzyl chloride
5-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-2-thioxo-imidazolidin-4-one
Conditions | Yield |
---|---|
With caesium carbonate In ethanol at 20℃; for 25h; | 95% |
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; for 2h; | 95% |
tri(p-tolyl)bismuth
p-bromobenzyl chloride
1-(4-methylbenzyl)-4-bromobenzene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In N,N-dimethyl-formamide at 90℃; for 2h; Schlenk technique; Inert atmosphere; chemoselective reaction; | 95% |
Conditions | Yield |
---|---|
With triethylamine; trifluoroacetic acid In dichloromethane at 20℃; for 9h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 8h; Inert atmosphere; | 95% |
p-bromobenzyl chloride
4-n-methylphenylacetylene
1-(4-bromobenzyl)-4-(4-methylphenyl)-1H-1,2,3-triazole
Conditions | Yield |
---|---|
With sodium azide In ethanol; water at 20℃; for 0.166667h; Sonication; | 95% |
With copper(l) iodide; sodium azide; eosin Y disodium salt In ethanol; water at 20℃; for 2h; Irradiation; Green chemistry; regioselective reaction; | 85% |
Thien-3-ylboronic acid
p-bromobenzyl chloride
3-(4-bromobenzyl)thiophene
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 100℃; for 4h; Suzuki-Miyaura cross-coupling; Inert atmosphere; Large scale reaction; | 94% |
Conditions | Yield |
---|---|
With water; sodium hydroxide at 20℃; for 0.0666667h; Microwave irradiation; | 93% |
With (NH4)4[ZnMo6O18(OH)6]; oxygen In water; acetonitrile at 60℃; under 760.051 Torr; for 12h; | 87% |
With dihydrogen peroxide; vanadia; Aliquat 336 In water for 15h; Heating; | 85% |
(4-pentylphenyl)boronic acid
p-bromobenzyl chloride
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine tetrafluoroborate In water; toluene at 80℃; for 2h; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
Stage #1: 3-mercapto-1,2,4-triazole With sodium In methanol; 1,2-dimethoxyethane at 20℃; for 0.166667h; Stage #2: p-bromobenzyl chloride In methanol; 1,2-dimethoxyethane at 20℃; for 1h; | 92% |
p-bromobenzyl chloride
N,N-dimethyl (trimethylsilyl)methanamide
2-(4-bromophenyl)-N,N-dimethyl acetamide
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In toluene at 65℃; for 20h; | 92% |
sodium methansulfinate
p-bromobenzyl chloride
Conditions | Yield |
---|---|
Stage #1: p-bromobenzyl chloride With Sodium thiosulfate pentahydrate In ethanol; water at 100℃; for 2h; Inert atmosphere; Stage #2: sodium methansulfinate In 1,4-dioxane at 110℃; for 11h; Inert atmosphere; | 92% |
(1-bromoethyl)benzne
urea
p-bromobenzyl chloride
6-(4-bromophenyl)-4-phenyl-1H-pyrimidin-2-one
Conditions | Yield |
---|---|
With pyridine N-oxide In neat (no solvent) at 90℃; for 0.666667h; | 92% |
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