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Cas:3179-31-5
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inquiryProduct Description Product Name 1H-1,2,4-Triazole-3-thiol CAS No. 3179-31-5 Appearance White to yellowish crystal Assay ≥99% Capacity 200mt/year Min.packing
Cas:3179-31-5
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inquiryQuick Details CAS No.: 3179-31-5 MF: C2H3N3S Place of Origin: Shaanxi, China (Mainland) Type: Pharmaceutical Intermediates Purity: 99.5% Brand Name: Luyun
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiry1H-1,2,4-Triazole-3-thiol 3179-31-5 1H-1,2,4-Triazole-3-thiol Basic information Product Name: 1H-1,2,4-Triazole-3-thiol Synonyms: TIMTEC-BB SBB004364;S-TRIAZOLE-3-THIOL;MTZ;1,2,4-triaz
Cas:3179-31-5
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct name: O-Methylisourea hemisulfate Alias: Carbamimidic acid, methylester, hemisulfate; methyl carbamimidate sulfate (2:1) CAS No. 52328-05-9 EINECS No: 257-851-8 Molecular formula: C4H14N4O6S Molecular weight: 246.24 Melting
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inquiryProduction information 1H-1,2,4-triazole-3-thiol CAS No.:3179-31-5 molecular formula: Application: Agricultural acaricides: key intermediates of the alpaca mite. Packing: 25KG/drum Appearance:white to yellowish crystal Storage:
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inquiry1H-1,2,4-Triazole-3-thiol CAS: 3179-31-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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Cas:3179-31-5
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inquiryExcellent quality negotiable price 3-Mercapto -1,2,4-Triazole 3179-31-5 in regular stock CAS No. 3179-31-5 3-Mercapto -1,2,4-Triazole Synonym:3-Mercapto-1H-1,2,4-Triazole、1H-1,2,4- Triazole-3-Thiol MF:C2H3N3S Structure: MW: 101.13
Cas:3179-31-5
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:3179-31-5
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Cas:3179-31-5
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Cas:3179-31-5
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inquiryProduct name: 3-Mercapto-1,2,4-Triazole CAS No.: 3179-31-5 Molecule Formula:C2H3N3S Molecule Weight:101.13 Purity: 99.0% Package: 25kg/drum Description:White or light yellow crystalline powder Manufacture Standards:Enterprise Standard
Cas:3179-31-5
Min.Order:1 Kilogram
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inquiryConditions | Yield |
---|---|
Stage #1: formic acid; thiosemicarbazide In water at 100℃; for 1h; Stage #2: With potassium carbonate In water at 110℃; for 3h; | 65% |
Stage #1: formic acid; thiosemicarbazide In water at -10 - 105℃; Stage #2: With sodium carbonate In water at 100℃; for 4h; | 55% |
2-amino-5-mercapto-s-triazole
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
H14[NaP5W30O110] In acetic acid for 24h; Heating; | 57% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 3h; Heating; | 55% |
Conditions | Yield |
---|---|
With sodium carbonate In water at 20 - 100℃; for 4h; | 55% |
3,4,4-trimethyl-Δ2-oxazolinium iodide
thiosemicarbazide
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
In acetonitrile for 75h; Heating; | 50% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 3h; Heating; | 50% |
1-ethoxymethylene thiosemicarbazide
1H-[1,2,4]triazole-3-thiol
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
Stage #1: 1-formyl-3-thiosemicarbazide With potassium carbonate In water at 100℃; for 4h; Stage #2: With hydrogenchloride In water at -10℃; pH=4 - 5; | 5.6 g |
3-[(3-chloropropyl)oxy]benzonitrile
1H-[1,2,4]triazole-3-thiol
3-{[3-(1H-1,2,4-triazol-3-ylthio)propyl]oxy}benzonitrile
Conditions | Yield |
---|---|
With triethylamine In ethanol at 80℃; for 15h; | 100% |
3-[(4-chlorobutyl)oxy]benzonitrile
1H-[1,2,4]triazole-3-thiol
3-{[4-(1H-1,2,4-triazol-3-ylthio)butyl]oxy}benzonitrile
Conditions | Yield |
---|---|
With triethylamine In ethanol at 80℃; for 15h; | 100% |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 3h; | 100% |
Conditions | Yield |
---|---|
In water at 60℃; | 100% |
1H-[1,2,4]triazole-3-thiol
3-[(2-chloroethyl)oxy]benzonitrile
3-{[2-(1H-1,2,4-triazol-3-ylthio)ethyl]oxy}benzonitrile
Conditions | Yield |
---|---|
With triethylamine In ethanol at 80℃; for 15h; | 98% |
With triethylamine In ethanol at 80℃; for 15h; | 98% |
(E)-N-(3-chloro-4-oxonaphthalen-1(4H)-ylidene)thiophene-2-sulfonamide
1H-[1,2,4]triazole-3-thiol
N-(3-(1H-1,2,4-triazol-5-ylthio)-4-oxonaphthalen-1(4H)-ylidene)thiophene-2-sulfonamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; | 96.5% |
methanesulfonic acid cyclopentylmethyl ester
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In methanol | 96% |
1H-[1,2,4]triazole-3-thiol
3-(1H-1,2,4-triazol-3-yldisulfanyl)-1H-1,2,4-triazole
Conditions | Yield |
---|---|
With pyridine; benzenesulfonyl chloride In dichloromethane at 0 - 25℃; for 20h; | 95.2% |
With pyridine; p-toluenesulfonyl chloride In dichloromethane at 0 - 25℃; for 20h; | 95.2% |
With pyridine; benzenesulfonyl chloride In dichloromethane at 0 - 25℃; for 20h; | 95.2% |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 5h; | 94% |
With triethylamine In tetrahydrofuran at 20℃; for 2.5h; Cooling with ice; | 45% |
With water; triethylamine In tetrahydrofuran at 20℃; |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; | 94% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; | 93% |
1H-[1,2,4]triazole-3-thiol
3-iodopropyltrimethoxysilane
Conditions | Yield |
---|---|
Stage #1: 1H-[1,2,4]triazole-3-thiol With sodium methylate In methanol at 10 - 20℃; for 0.5h; Stage #2: 3-iodopropyltrimethoxysilane In methanol at 27 - 30℃; for 3.66667h; | 92.3% |
Conditions | Yield |
---|---|
In acetate buffer; acetonitrile Electrochemical reaction; | 92% |
Conditions | Yield |
---|---|
In acetate buffer; acetonitrile Electrochemical reaction; | 91% |
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
91% |
2-Iodobenzoic acid
1H-[1,2,4]triazole-3-thiol
1,2,4-Triazolo<5,1-b><1,3>benzothiazin-9-one
Conditions | Yield |
---|---|
With potassium carbonate In N,N,N,N,N,N-hexamethylphosphoric triamide at 80℃; for 24h; Sealed tube; Schlenk technique; | 91% |
Conditions | Yield |
---|---|
Stage #1: 1H-[1,2,4]triazole-3-thiol With sodium In methanol; N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: 3-chloromethylpyridinium chloride In methanol; N,N-dimethyl-formamide at 20℃; | 90% |
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 20℃; for 8h; | 90% |
1H-[1,2,4]triazole-3-thiol
dimethylamino sulfonyl chloride
3-{[1-(dimethylsulfamoyl)-1H-1,2,4-triazol-3-yl]disulfanyl}-N,N-dimethyl-1H-1,2,4-triazole-1-sulfonamide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 28 - 32℃; for 8h; | 90% |
1H-[1,2,4]triazole-3-thiol
para-bromophenacyl bromide
2-(1H-1,2,4-triazol-3-ylthio)-1-(4-bromophenyl) ethanone
Conditions | Yield |
---|---|
In ethanol at 20℃; for 14h; Reflux; | 89% |
2-iodoyl-5-methylbenzoic acid
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
With potassium carbonate In N,N,N,N,N,N-hexamethylphosphoric triamide at 80℃; for 24h; Sealed tube; Schlenk technique; | 89% |
Conditions | Yield |
---|---|
Stage #1: 1H-[1,2,4]triazole-3-thiol With sodium In methanol; N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #2: 1-Chloromethylnaphthalene In methanol; N,N-dimethyl-formamide at 20℃; | 88% |
1H-[1,2,4]triazole-3-thiol
tert-butyl alcohol
3-tert-butylsulfanyl-1,2,4-triazole
Conditions | Yield |
---|---|
Stage #1: 1H-[1,2,4]triazole-3-thiol; tert-butyl alcohol With perchloric acid In water at 20℃; for 3h; Stage #2: With sodium hydroxide In water pH=6 - 7; regioselective reaction; | 87% |
1H-[1,2,4]triazole-3-thiol
2,4,6-trimethylaniline
3-(2,4,6-trimethylphenyl)thio-1H-1,2,4-triazole
Conditions | Yield |
---|---|
Stage #1: 2,4,6-trimethylaniline With hydrogenchloride; sodium nitrite In water at 10℃; for 0.00277778h; Flow reactor; Stage #2: 1H-[1,2,4]triazole-3-thiol With sodium hydroxide In methanol; n-heptane; water at 25℃; under 7498.84 Torr; for 0.0111111h; Flow reactor; | 86% |
Stage #1: 2,4,6-trimethylaniline With hydrogenchloride; sodium nitrite In water at -5 - -2℃; for 0.5h; Large scale; Stage #2: 1H-[1,2,4]triazole-3-thiol With sodium hydroxide In methanol; water at 20 - 30℃; for 1.16667h; Temperature; Solvent; Large scale; | 60% |
Stage #1: 2,4,6-trimethylaniline With hydrogenchloride; sodium nitrite In methanol; water for 0.5h; Cooling with ice/sodium chloride; Stage #2: 1H-[1,2,4]triazole-3-thiol With potassium hydroxide In methanol; water at 20℃; for 1.5h; Cooling with ice/sodium chloride; |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 75℃; for 0.333333h; | 86% |
With sodium hydroxide In ethanol; water for 0.333333h; Reflux; |
2-naphthyl 2,3-dibromopropyl sulfone
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 20℃; for 8h; | 85% |
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
With Na2S2O3*5H2O; NaOH In water addn. of an alkaline soln. of ligand to an aq. soln. of iron complex, storage at 6-8°C for 6 d; recrystn. (methanol); elem. anal.; | 85% |
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
With Na2S2O3*5H2O In water 5 equiv. of thiole was dissolved in aq. alkali and added to an aq. mixt.of Fe-compd. and 2 equiv. of Na2S2O3; soln. was filtered and storaged at 6-8 °C for a few days, recrystn. from abs. MeOH, drying in vac. over CaCl2, elem. anal.; | 85% |
1-(12-bromododec-5(Z)-enyl)-3-n-pentylurea
1H-[1,2,4]triazole-3-thiol
C20H37N5OS
Conditions | Yield |
---|---|
Stage #1: 1H-[1,2,4]triazole-3-thiol With sodium methylate In methanol; N,N-dimethyl-formamide for 0.166667h; Stage #2: 1-(12-bromododec-5(Z)-enyl)-3-n-pentylurea In methanol; N,N-dimethyl-formamide | 85% |
Stage #1: 1H-[1,2,4]triazole-3-thiol With sodium methylate In N,N-dimethyl-formamide for 0.166667h; Stage #2: 1-(12-bromododec-5(Z)-enyl)-3-n-pentylurea In N,N-dimethyl-formamide | 85% |
2-(4-(bromomethyl)phenyl)propanoic acid
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
In acetone at 40℃; for 12h; Reflux; | 85% |
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