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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1072.html Product Name 2-(4-Bromomethyl)phenylpropionic acid CAS No.
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inquiry2-[4-(Bromomethyl)phenyl]propinic acid CAS No.: 111128-12-2 CAS Number: 111128-12-2 Name: 2-(4-Bromomethyl)phenylpropionic acid Formula: C10H11BrO2 Molecular Weight: 243.10 Synonyms: 2-[p-(Bromomethyl)phenyl]propionicacid;Benzen
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inquiryUnique advantages of 2-(4-Bromomethyl)phenylpropionic acid Cas 111128-12-2 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White to off-white crystalline powder Storage:cool dry pla
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inquiry2-(4-Bromomethyl)phenylpropionic acid CAS No.:111128-12-2 Name: 2-(4-Bromomethyl)phenylpropionic acid Molecular Structure: Molecular Formula: C10H11BrO2 Molecular
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inquiry2-(4-Bromomethyl)phenylpropionic acid CAS 111128-12-2 4-Bromomethyl Phenyl Propionic Acid CAS no 111128-12-2 4-(BROMOMETHYL)HYDRATROPIC ACID 2-(4-Bromomethyl)phenylpropionic acide CAS 111128-12-2 4-Bromomethyl Phenyl Propionic Acid IN Stock CAS
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inquiry2-(4-bromomethyl) phenylpropionic acid high quality spot supply, low price and rapid delivery Chinese Name: 2-(4-bromomethyl) phenylpropionic acid Chinese aliases: p-bromomethylphenylpropionic acid; 2-(4-bromomethylphenyl) propionic acid; loxopro
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inquiryProduct Name: 2-(4-Bromomethyl)phenylpropionic acid Chemical Name: 2-(4-Bromomethyl)phenylpropionic acid CAS No.: 111128-12-2 Molecular Formula: C10H11BrO2 Molecular Weight: 243.09714 Appearance:White powder Storage:RT
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inquiry2-(4-Bromomethyl)phenylpropionic acid(BMPPA) CAS: 111128-12-2 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure
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inquiry2-(4-Bromomethyl)phenylpropionic acid Product Name: 2-(4-Bromomethyl)phenylpropionic acid Synonyms: 4-(BROMOMETHYL)HYDRATROPIC ACID;2-[4-(BROMOMETHYL)PHENYL]PROPANOIC ACID;2-[4-(BROMOMETHYL)PHENYL]PROPIONIC ACID;2-[(P-BROMOMETHYL)PHENYL]PROPION
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inquiryformaldehyd
hydratropic acid
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide at 35 - 70℃; for 11h; Temperature; | 99% |
With sulfuric acid; hydrogen bromide at 35 - 90℃; for 11.5h; Temperature; | 96% |
Stage #1: formaldehyd; hydratropic acid With hydrogen bromide at 55 - 65℃; Stage #2: With sulfuric acid at 20 - 65℃; | 96% |
(R,S)-2-(4'-methylphenyl) propionic acid
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
With bromine; dibenzoyl peroxide In dichloromethane Reflux; | 92% |
With bromine; dibenzoyl peroxide In dichloromethane at 40℃; for 0.0416667h; Temperature; | 90% |
With hydrogen bromide; bromine In ethyl acetate at 20℃; for 2h; | 79% |
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In dichloromethane Solvent; Reflux; | 42.05 g |
With hydrogen bromide; dihydrogen peroxide; dibenzoyl peroxide In dichloromethane at 10 - 15℃; Irradiation; |
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; phosphonic acid diethyl ester In water; toluene at 5 - 85℃; for 6h; Reagent/catalyst; Inert atmosphere; | 85.3% |
trioxane
hydratropic acid
cetyltrimethylammonim bromide
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
With hydrogen bromide; acetic acid | |
With hydrogen bromide; acetic acid |
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: toluene / 3 h / 35 - 75 °C 2.1: sodium hydroxide / 1 h / 80 °C 3.1: sodium hydroxide / 12.5 h / 105 °C / Reflux 3.2: 0.58 h / pH 3 4.1: sulfuric acid; hydrogen bromide / 11.5 h / 35 - 90 °C View Scheme |
phenylacetonitrile
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: sodium methylate / methanol; toluene / 10 h / 20 °C 2.1: toluene / 3 h / 35 - 75 °C 3.1: sodium hydroxide / 1 h / 80 °C 4.1: sodium hydroxide / 12.5 h / 105 °C / Reflux 4.2: 0.58 h / pH 3 5.1: sulfuric acid; hydrogen bromide / 11.5 h / 35 - 90 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / 15 h / 250 °C / 30003 Torr / Autoclave 2: sodium hydroxide; water / 8 h / 40 °C 3: sulfuric acid; hydrogen bromide / 11 h / 35 - 70 °C View Scheme |
2-methoxycarbonyl-2-phenylpropionitrile
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydroxide / 1 h / 80 °C 2.1: sodium hydroxide / 12.5 h / 105 °C / Reflux 2.2: 0.58 h / pH 3 3.1: sulfuric acid; hydrogen bromide / 11.5 h / 35 - 90 °C View Scheme |
CH3C6H4CH(CH3)OH
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine; calcium chloride / dichloromethane / 40 h 2: dimethyl sulfoxide / 18 h / 90 °C / Reflux 3: hydrogenchloride / 1 h / Reflux 4: hydrogen bromide; bromine / ethyl acetate / 2 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: thionyl chloride / toluene / Reflux 2: tetrabutylammomium bromide / toluene; water / 8 h / 60 - 70 °C 3: sodium hydroxide / 100 - 105 °C 4: dibenzoyl peroxide; bromine / dichloromethane / Reflux View Scheme |
1-(4-methylphenyl)ethyl 4-methylbenzenesulfonate
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dimethyl sulfoxide / 18 h / 90 °C / Reflux 2: hydrogenchloride / 1 h / Reflux 3: hydrogen bromide; bromine / ethyl acetate / 2 h / 20 °C View Scheme |
para-methylacetophenone
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: sodium tetrahydroborate / methanol 2: triethylamine; calcium chloride / dichloromethane / 40 h 3: dimethyl sulfoxide / 18 h / 90 °C / Reflux 4: hydrogenchloride / 1 h / Reflux 5: hydrogen bromide; bromine / ethyl acetate / 2 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: sodium tetrahydroborate / methanol / 15 - 35 °C 2: thionyl chloride / toluene / Reflux 3: tetrabutylammomium bromide / toluene; water / 8 h / 60 - 70 °C 4: sodium hydroxide / 100 - 105 °C 5: dibenzoyl peroxide; bromine / dichloromethane / Reflux View Scheme |
(+/-)-2-(4'-methylphenyl)-propionitrile
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / 1 h / Reflux 2: hydrogen bromide; bromine / ethyl acetate / 2 h / 20 °C View Scheme |
1-(1-chloroethyl)-4-methylbenzene
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: magnesium / tetrahydrofuran / 1.5 h / 20 - 30 °C / Inert atmosphere 2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / dichloromethane / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: magnesium / tetrahydrofuran; ethylene dibromide / 13 h / 60 - 65 °C / Inert atmosphere 1.2: 20 - 25 °C 2.1: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: magnesium / tetrahydrofuran; ethylene dibromide / 13 h / 60 - 65 °C / Inert atmosphere 1.2: 20 - 25 °C 2.1: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere 3.1: tetra-(n-butyl)ammonium iodide; phosphonic acid diethyl ester / water; toluene / 6 h / 5 - 85 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: tetrabutylammomium bromide / toluene; water / 8 h / 60 - 70 °C 2: sodium hydroxide / 100 - 105 °C 3: dibenzoyl peroxide; bromine / dichloromethane / Reflux View Scheme |
1-ethenyl-4-methylbenzene
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrogenchloride / water / 6 h / 65 - 70 °C / Inert atmosphere 2.1: magnesium / tetrahydrofuran; ethylene dibromide / 13 h / 60 - 65 °C / Inert atmosphere 2.2: 20 - 25 °C 3.1: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: hydrogen bromide / 5 h / 60 - 65 °C / Inert atmosphere 2: magnesium / tetrahydrofuran; ethylene dibromide / 55 - 65 °C 3: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: hydrogenchloride / water / 6 h / 65 - 70 °C / Inert atmosphere 2.1: magnesium / tetrahydrofuran; ethylene dibromide / 13 h / 60 - 65 °C / Inert atmosphere 2.2: 20 - 25 °C 3.1: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere 4.1: tetra-(n-butyl)ammonium iodide; phosphonic acid diethyl ester / water; toluene / 6 h / 5 - 85 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1: hydrogen bromide / 5 h / 60 - 65 °C / Inert atmosphere 2: magnesium / tetrahydrofuran; ethylene dibromide / 55 - 65 °C 3: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere 4: tetra-(n-butyl)ammonium iodide; phosphonic acid diethyl ester / water; toluene / 6 h / 5 - 85 °C / Inert atmosphere View Scheme |
1-(1-bromoethyl)-4-methylbenzene
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: magnesium / tetrahydrofuran; ethylene dibromide / 55 - 65 °C 2: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: magnesium / tetrahydrofuran; ethylene dibromide / 55 - 65 °C 2: bromine; 2,2'-azobis(isobutyronitrile) / dichloromethane / 40 - 55 °C / Inert atmosphere 3: tetra-(n-butyl)ammonium iodide; phosphonic acid diethyl ester / water; toluene / 6 h / 5 - 85 °C / Inert atmosphere View Scheme |
(R,S)-2-(4'-methylphenyl) propionic acid
A
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); bromine In dichloromethane at 40 - 55℃; Solvent; Reagent/catalyst; Temperature; Inert atmosphere; |
styrene
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrogenchloride / dichloromethane / 5 h / 10 - 20 °C 2.1: magnesium / 2-methyltetrahydrofuran / 5 h / 20 - 30 °C 2.2: 5 h / 20 - 30 °C 3.1: sulfuric acid; hydrogen bromide / 3 h / 50 - 120 °C View Scheme |
methanol
2-(4-(bromomethyl)phenyl)propanoic acid
2-(4-bromomethylphenyl)propionic acid methyl ester
Conditions | Yield |
---|---|
In 2,2,4-trimethylpentane at 65℃; for 0.5h; Solvent; Temperature; | 99.7% |
Stage #1: methanol With sulfuric acid In toluene at 35℃; Stage #2: 2-[4-(bromomethyl)phenyl]propanoic acid In toluene at 281℃; for 5h; | 98.7% |
With sulfuric acid at 0 - 5℃; for 6h; | 98% |
2-(4-(bromomethyl)phenyl)propanoic acid
ethanol
Conditions | Yield |
---|---|
In toluene at 79℃; for 0.333333h; Time; | 97.8% |
2-(4-(bromomethyl)phenyl)propanoic acid
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 96% |
With sodium azide; 15-crown-5 In 1,4-dioxane at 80℃; for 16h; | |
With sodium azide In N,N-dimethyl-formamide at 100℃; for 12h; Temperature; Inert atmosphere; | |
With sodium azide In N,N-dimethyl-formamide at 100℃; for 12h; Inert atmosphere; |
2-(4-(bromomethyl)phenyl)propanoic acid
1-hydroxy-pyrrolidine-2,5-dione
triphenylphosphine
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In acetonitrile at 20℃; for 16h; | 94.9% |
2-(4-(bromomethyl)phenyl)propanoic acid
2-ethoxycarbonyl-1-cyclopentanone
sodium 2-<4-<(2-oxocyclopentyl)methyl>phenyl>propionate
Conditions | Yield |
---|---|
Stage #1: 2-[4-(bromomethyl)phenyl]propanoic acid; 2-ethoxycarbonyl-1-cyclopentanone With sodium hydroxide In N,N-dimethyl-formamide under 760.051 Torr; for 8h; Stage #2: With hydrogenchloride In water; N,N-dimethyl-formamide pH=5 - 6; Further stages; | 92% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 23℃; Inert atmosphere; | 87% |
2-(4-(bromomethyl)phenyl)propanoic acid
dimethylmonochlorosilane
diethyl ether
2-[(4-dimethylsilylmethyl)phenyl]propionic acid
Conditions | Yield |
---|---|
With triethylamine In (2S)-N-methyl-1-phenylpropan-2-amine hydrate | 85% |
2-(4-(bromomethyl)phenyl)propanoic acid
1H-[1,2,4]triazole-3-thiol
Conditions | Yield |
---|---|
In acetone at 40℃; for 12h; Reflux; | 85% |
2-(4-(bromomethyl)phenyl)propanoic acid
5-chloro-2-mercaptobenzothiazole
Conditions | Yield |
---|---|
In acetone at 40℃; for 12h; Reflux; | 85% |
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