Products

Refine

Country

Business Type

Certificate

Display

Hubei Mawer Biological Technology Co., Ltd.

Our service: 1.We have experience in exporting Pharmaceutical intermediates . 2.Professional packing with professional materials 3. We have products in stock, and we will deliver them soon when your PO arrived. Meanwhile we will give you the trackin

Raloxifene Hydrochloride

Cas:82640-04-8

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

Raloxifene Hydrochloride CAS NO.82640-04-8

Cas:82640-04-8

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

inquiry

Wuhan Fortuna Chemical Co.,Ltd

USP standard Raloxifene hydrochloride CAS 82640-04-8 with good quality 1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appe

USP standard Raloxifene hydrochloride CAS 82640-04-8 with good quality

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $78.0

Type:Trading Company

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Raloxifene Hydrochlorid

Cas:82640-04-8

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price API 99% Raloxifene hydrochloride 82640-04-8 GMP Manufacturer

Cas:82640-04-8

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hubei DiBo chemical co., LTD

Name:Raloxifene hydrochloride CAS NO:82640-04-8 Grade:Medical scientific research and export Molecular formula: C28H28ClNO4S Molecular weight:510.04 Product Quality 12 years of chemical raw materials Mature operation of the industry Sy

Raloxifene hydrochloride /cas:82640-04-8 /Raw material spot

Cas:82640-04-8

Min.Order:25 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

inquiry

LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc. We are specialized in chemical synthesis, process development of

Raloxifene hydrochloride Manufacturer

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod

Raloxifene hcl

Cas:82640-04-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 82640-04-8 with competitive price

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Food Additives Supplier 82640-04-8 Raloxifene HCl

Cas:82640-04-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd

Raloxifene hydrochlorideCAS82640-04-8

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $20.0 / 28.0

Type:Trading Company

inquiry

Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:light yellow powder Storage:Store in sealed containers at co

Raloxifene Hydrochloride CAS 82640-04-8 anti estrogen steroid

Cas:82640-04-8

Min.Order:100 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

Raloxifene hydrochloride CAS:82640-04-8

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $514.0 / 521.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply High quality Raloxifene HCl CAS 82640-04-8 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China

High quality Raloxifene HCl CAS 82640-04-8

Cas:82640-04-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

We generally use secure shipping methods that do not require you to do any customs clearance. Free shipping to your address without worrying about any customs issues. We have a professional customs clearance team to 100% guarantee the safe delivery o

High Quality CAS 82640-04-8 Hydrochloride Safe Deliveryddp

Cas:82640-04-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several

Raloxifene HCl cas:82640-04-8

Cas:82640-04-8

Min.Order:25 Gram

FOB Price: $90.0 / 100.0

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By

Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Taizhou Crene Biotechnology co.ltd

Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

Raloxifene hydrochloride 82640-04-8

Cas:82640-04-8

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Yuanmeng Biological Technology Co., Ltd.

Hubei Yuanmeng Biological Technology Co., Ltd., which is located in Wuhan, China. We are specializing in the exportation of APIs, and plant extracts ect. Our products has been exported to America, Australia, Brazil, the Europe, Middle East and other

Good Quality Raloxifene Hydrochloride CAS 82640-04-8

Cas:82640-04-8

Min.Order:1 Kilogram

FOB Price: $3.0 / 5.0

Type:Trading Company

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

moderate price & quick delivery Appearance:Light-Yellow Solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:A nonsteroidal, selective estro

Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: Raloxifene hydrochloride Synonyms: RALOXIFENE HCL;RALOXIFENE HYDROCHLORIDE;ly156758;methanone,(6-hydroxy-2-(4-hydroxyphenyl)benzo(b)thien-3-yl)(4-(2-(1-piperidin;KEOXIFENE;KEOXIFENE HYDROCHLORIDE;LY 139481;AKOS 92138 CAS: 8

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Raloxifene hydrochloride Manufacturer/High quality/Best price/In stock

Cas:82640-04-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Quality Manufacturer Raloxifene hydrochloride

Cas:82640-04-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

[2-(4-methoxyphenyl)-6-methoxybenzo[b]thien-3-yl][4-[2-(1-piperidinyl)ethoxy]phenyl]methanone hydrochloride
84541-36-6

[2-(4-methoxyphenyl)-6-methoxybenzo[b]thien-3-yl][4-[2-(1-piperidinyl)ethoxy]phenyl]methanone hydrochloride

raloxifene hydrochloride

raloxifene hydrochloride

Conditions
ConditionsYield
Stage #1: [2-(4-methoxyphenyl)-6-methoxybenzo[b]thien-3-yl][4-[2-(1-piperidinyl)ethoxy]phenyl]methanone hydrochloride With boron trichloride In dichloromethane at 2 - 20℃; for 52.25h;
Stage #2: With methanol In dichloromethane at 12℃; for 1.08333h; Product distribution / selectivity; Reflux;
95%
Stage #1: [2-(4-methoxyphenyl)-6-methoxybenzo[b]thien-3-yl][4-[2-(1-piperidinyl)ethoxy]phenyl]methanone hydrochloride With boron tribromide In dichloromethane at 2 - 20℃; for 52.25h;
Stage #2: With methanol In dichloromethane for 0.75h; Product distribution / selectivity; Reflux;
95%
With boron trichloride In dichloromethane at 0 - 22℃; for 38.1h; Product distribution / selectivity; Reflux;92.6%
With aluminium trichloride; ethanethiol In dichloromethane for 0.5h; Ambient temperature;77.5%
[6-Methoxy-2-(4-Methoxyphenyl)benzo[b]thien-3-yl]-[4-[2-(1-Piperidinyl)ethoxy]phenyl] Methanone
84541-38-8

[6-Methoxy-2-(4-Methoxyphenyl)benzo[b]thien-3-yl]-[4-[2-(1-Piperidinyl)ethoxy]phenyl] Methanone

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
With N,N-diethylaniline; ethanethiol In dichloromethane at 32 - 34℃; for 2h; Solvent;92%

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride
84449-80-9

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Stage #1: 4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride With pyridine; thionyl chloride In dichloromethane for 1h; Heating / reflux;
Stage #2: 6-acetoxy-2-(4-acetoxyphenyl)benzo[b]thiophene In dichloromethane
Stage #3: With hydrogenchloride; sodium hydroxide; water; aluminum (III) chloride more than 3 stages;
70.4%
3-methoxybenzenethiol
15570-12-4

3-methoxybenzenethiol

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 80.4 percent / KOH / ethanol; H2O; ethyl acetate / Ambient temperature
2: 69 percent / PPA / 1 h / 85 - 90 °C
3: AlCl3 / CH2Cl2 / 1.5 h / 27 - 29 °C
4: 77.5 percent / AlCl3, EtSH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
Multi-step reaction with 3 steps
1.1: bromine / methanol / 2.5 h / 10 °C
1.2: 4 h / 0 - 20 °C
2.1: polyphosphoric acid / 2 h / 65 - 90 °C
3.1: thionyl chloride / N,N-dimethyl-formamide; toluene / 2 h / 80 °C
3.2: 3 h / 20 °C
View Scheme
2-(4'-methoxyphenyl)-6-methoxybenzothiophene
63675-74-1

2-(4'-methoxyphenyl)-6-methoxybenzothiophene

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: AlCl3 / CH2Cl2 / 1.5 h / 27 - 29 °C
2: 77.5 percent / AlCl3, EtSH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
4-(2-(piperidin-1-yl)ethoxy)benzoyl chloride
166975-76-4

4-(2-(piperidin-1-yl)ethoxy)benzoyl chloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: AlCl3 / CH2Cl2 / 1.5 h / 27 - 29 °C
2: 77.5 percent / AlCl3, EtSH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
α-(3-methoxyphenyl-thio)-4-methoxyacetophenone
63675-73-0

α-(3-methoxyphenyl-thio)-4-methoxyacetophenone

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 69 percent / PPA / 1 h / 85 - 90 °C
2: AlCl3 / CH2Cl2 / 1.5 h / 27 - 29 °C
3: 77.5 percent / AlCl3, EtSH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride
84449-80-9

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: SOCl2, DMF / toluene
2: AlCl3 / CH2Cl2 / 1.5 h / 27 - 29 °C
3: 77.5 percent / AlCl3, EtSH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
Multi-step reaction with 3 steps
1.1: thionyl chloride / dichloromethane / 40 °C
2.1: aluminum (III) chloride / dichloromethane / 10 - 35 °C
3.1: potassium hydroxide; water / 105 - 110 °C
3.2: 60 °C / pH 2
View Scheme
2-Bromo-4'-methoxyacetophenone
2632-13-5

2-Bromo-4'-methoxyacetophenone

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 80.4 percent / KOH / ethanol; H2O; ethyl acetate / Ambient temperature
2: 69 percent / PPA / 1 h / 85 - 90 °C
3: AlCl3 / CH2Cl2 / 1.5 h / 27 - 29 °C
4: 77.5 percent / AlCl3, EtSH / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
2-(4'-methoxyphenyl)-6-methoxybenzothiophene
63675-74-1

2-(4'-methoxyphenyl)-6-methoxybenzothiophene

4-[2-(piperidin-1-yl)ethoxy]benzoyl chloride hydrochloride

4-[2-(piperidin-1-yl)ethoxy]benzoyl chloride hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
With boron trichloride In 1,2-dichloro-ethane at 0 - 35℃; for 24h;
aqueous sodium chloride

aqueous sodium chloride

2-(4'-methoxyphenyl)-6-methoxybenzothiophene
63675-74-1

2-(4'-methoxyphenyl)-6-methoxybenzothiophene

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride
84449-80-9

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water; chlorobenzene
With hydrogenchloride; thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water; chlorobenzene
With hydrogenchloride; thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water; chlorobenzene
With hydrogenchloride; thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water; chlorobenzene
With hydrogenchloride; CO; thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water; chlorobenzene
2-(4'-methoxyphenyl)-6-methoxybenzothiophene
63675-74-1

2-(4'-methoxyphenyl)-6-methoxybenzothiophene

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride
84449-80-9

4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
With thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; chlorobenzene
With thionyl chloride; ethanethiol; aluminium trichloride In tetrahydrofuran; N-methyl-acetamide; dichloromethane; chlorobenzene
Stage #1: 4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride With thionyl chloride; N,N-dimethyl-formamide In chlorobenzene at 70 - 75℃; for 1h;
Stage #2: 2-(4'-methoxyphenyl)-6-methoxybenzothiophene With aluminum (III) chloride In dichloromethane; chlorobenzene at 20℃; for 1.75h;
Stage #1: 4-(2-piperidin-1-ylethoxy)benzoic acid hydrochloride With thionyl chloride In N,N-dimethyl-formamide; toluene at 80℃; for 2h;
Stage #2: 2-(4'-methoxyphenyl)-6-methoxybenzothiophene With aluminum (III) chloride In dichloromethane at 20℃; for 3h;
Raloxifen
84449-90-1

Raloxifen

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In tetrahydrofuran; isopropyl alcohol at 5 - 35℃; for 2.25h;
With ammonium chloride In water at 70 - 75℃; for 8.45h; Product distribution / selectivity;
With hydrogenchloride In tetrahydrofuran Product distribution / selectivity;
With hydrogenchloride In methanol; water pH=2;
Stage #1: Raloxifen In methanol; acetone at 25 - 30℃; for 0.166667h;
Stage #2: With hydrogenchloride In methanol; water; acetone pH=1.5 - Ca. 2;
<6-<(methylsulfonyl)oxy>-2-<4-<(methylsulfonyl)oxy>phenyl>benzothien-3-yl><4-<2-(1-pyrrolidinyl)ethoxy>phenyl>methanone hydrochloride
84449-85-4

<6-<(methylsulfonyl)oxy>-2-<4-<(methylsulfonyl)oxy>phenyl>benzothien-3-yl><4-<2-(1-pyrrolidinyl)ethoxy>phenyl>methanone hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Stage #1: <6-<(methylsulfonyl)oxy>-2-<4-<(methylsulfonyl)oxy>phenyl>benzothien-3-yl><4-<2-(1-pyrrolidinyl)ethoxy>phenyl>methanone hydrochloride With water; potassium hydroxide at 105 - 110℃;
Stage #2: With hydrogenchloride In water; acetone at 60℃; pH=2;
Ethyl 4-hydroxybenzoate
120-47-8

Ethyl 4-hydroxybenzoate

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / ethyl acetate; water / 13 - 35 °C / Reflux
2.1: formic acid; sulfuric acid / acetic acid
3.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 5 h / 65 - 70 °C
4.1: iron(III) sulfate pentahydrate; iron / toluene / 99 - 114 °C
4.2: 62 - 66 °C / Inert atmosphere
5.1: sodium hydroxide / tetrabutylammomium bromide / toluene; water / 6 h / Reflux
5.2: 20 °C
6.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
6.2: 2 - 51 °C
7.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
7.2: 1.08 h / 12 °C / Reflux
View Scheme
N-chloroethylpiperidine hydrochloride
2008-75-5

N-chloroethylpiperidine hydrochloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
1.2: 2 - 51 °C
2.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
2.2: 1.08 h / 12 °C / Reflux
View Scheme
[6-methoxy-2-(4-methoxyphenyl)benzo[b]thiophen-3-yl](4-hydroxyphenyl)methanone
63676-19-7

[6-methoxy-2-(4-methoxyphenyl)benzo[b]thiophen-3-yl](4-hydroxyphenyl)methanone

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
1.2: 2 - 51 °C
2.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
2.2: 1.08 h / 12 °C / Reflux
View Scheme
ethyl 4-((phenylsulfonyl)oxy)benzoate

ethyl 4-((phenylsulfonyl)oxy)benzoate

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: formic acid; sulfuric acid / acetic acid
2.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 5 h / 65 - 70 °C
3.1: iron(III) sulfate pentahydrate; iron / toluene / 99 - 114 °C
3.2: 62 - 66 °C / Inert atmosphere
4.1: sodium hydroxide / tetrabutylammomium bromide / toluene; water / 6 h / Reflux
4.2: 20 °C
5.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
5.2: 2 - 51 °C
6.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
6.2: 1.08 h / 12 °C / Reflux
View Scheme
p-benzenesulfonyloxybenzoyl chloride

p-benzenesulfonyloxybenzoyl chloride

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: iron(III) sulfate pentahydrate; iron / toluene / 99 - 114 °C
1.2: 62 - 66 °C / Inert atmosphere
2.1: sodium hydroxide / tetrabutylammomium bromide / toluene; water / 6 h / Reflux
2.2: 20 °C
3.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
3.2: 2 - 51 °C
4.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
4.2: 1.08 h / 12 °C / Reflux
View Scheme
benzenesulfonic acid-4-[6-methoxy-2-(4-methoxy-phenyl)-benzo[b]thiophene-3-carbonyl]-phenyl ester
1293362-49-8

benzenesulfonic acid-4-[6-methoxy-2-(4-methoxy-phenyl)-benzo[b]thiophene-3-carbonyl]-phenyl ester

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydroxide / tetrabutylammomium bromide / toluene; water / 6 h / Reflux
1.2: 20 °C
2.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
2.2: 2 - 51 °C
3.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
3.2: 1.08 h / 12 °C / Reflux
View Scheme
4-benzenesulfonyloxy-benzoic acid
7507-41-7

4-benzenesulfonyloxy-benzoic acid

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / toluene / 5 h / 65 - 70 °C
2.1: iron(III) sulfate pentahydrate; iron / toluene / 99 - 114 °C
2.2: 62 - 66 °C / Inert atmosphere
3.1: sodium hydroxide / tetrabutylammomium bromide / toluene; water / 6 h / Reflux
3.2: 20 °C
4.1: sodium hydroxide; tetrabutylammomium bromide / dichloromethane; water / 16 h / 20 °C
4.2: 2 - 51 °C
5.1: boron trichloride / dichloromethane / 52.25 h / 2 - 20 °C
5.2: 1.08 h / 12 °C / Reflux
View Scheme
1-(4-methoxyphenyl)ethanone
100-06-1

1-(4-methoxyphenyl)ethanone

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: bromine / methanol / 2.5 h / 10 °C
1.2: 4 h / 0 - 20 °C
2.1: polyphosphoric acid / 2 h / 65 - 90 °C
3.1: thionyl chloride / N,N-dimethyl-formamide; toluene / 2 h / 80 °C
3.2: 3 h / 20 °C
View Scheme
1-(4-(2-(piperidin-1-yl)ethoxy)phenyl)-2-(2-benzylthio-4-methoxyphenyl)ethanone

1-(4-(2-(piperidin-1-yl)ethoxy)phenyl)-2-(2-benzylthio-4-methoxyphenyl)ethanone

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: trifluoroacetic acid / 6 h / 80 °C
2: N,N-diethylaniline / dichloromethane / 12 h / 40 °C
3: N,N-diethylaniline; ethanethiol / dichloromethane / 2 h / 32 - 34 °C
View Scheme
benzyl-(3-methoxyphenyl)-sulfide

benzyl-(3-methoxyphenyl)-sulfide

raloxifene hydrochloride
82640-04-8

raloxifene hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: periodic acid; iron(III) chloride / toluene / 4 h / 27 °C / Cooling with ice
2: trifluorormethanesulfonic acid / 6 h / 70 °C
3: trifluoroacetic acid / 6 h / 80 °C
4: N,N-diethylaniline / dichloromethane / 12 h / 40 °C
5: N,N-diethylaniline; ethanethiol / dichloromethane / 2 h / 32 - 34 °C
View Scheme

Downstream Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View