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inquiryproduct Name 5-Bromosalicylaldehyde Synonyms 5-Bromo-2-hydroxybenzaldehyde; AKOS BBS-00003168; 2-HYDROXY-5-BROMOBENZALDEHYDE; OTAVA-BB BB7018801955; 5-Br-salycylal ; 5-Br-SALICYLAL Molecular Formula C7H5BrO2 Molecular Weight 201.0174 CAS Regis
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 5-Bromosalicylaldehyde CAS No. 1761-61-1
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inquiryProduct name 5-Bromosalicylaldehyde CAS NO. 1761-61-1 MF C7H5BrO2 Appearance light yellow powder Purity 99% Pakcing 25
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
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inquiry5-Bromo-2-hydroxybenzaldehyde CAS: 1761-61-1 Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard Shelf life 2 years Storage should be stored
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inquiry1761-61-1 98%MIN discount 5-Bromosalicylaldehyde factoryAppearance:white powder Storage:Store in cool and dry place. Package:according to customers' requirements Application:Used in the organic synthesis of medicine, spices and dyes intermediates Tr
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediate
Conditions | Yield |
---|---|
With sulfuric acid; C18H16Br4N2O3V; dihydrogen peroxide; potassium bromide In methanol; water at 20℃; for 2.16667h; Catalytic behavior; | 100% |
With sulfuric acid; C20H22Br2N2O5V; dihydrogen peroxide In methanol; water at 20℃; for 1.16667h; Catalytic behavior; | 100% |
With perchloric acid; dihydrogen peroxide; potassium bromide In water at 20℃; for 3.5h; | 99% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 0.05h; Microwave irradiation; | 99% |
With potassium dichromate; sulfuric acid | |
With oxygen In aq. buffer at 45℃; pH=6; Green chemistry; |
ethyl (E)-3-(4-bromo-2-formylphenoxy)acrylate
p-toluidine
A
C29H30NO7Br
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; | A 99% B n/a |
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate In tetrahydrofuran; water for 12h; Heating; | 98% |
With iron(III) p-toluenesulfonate hexahydrate In methanol; water for 4h; Reflux; | 78% |
With copper(II) sulfate; sodium iodide In acetone at 20℃; for 2.75h; | 67% |
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With cetyltrimethylammonium peroxodisulphate In acetonitrile for 0.133333h; Reflux; | 93% |
Conditions | Yield |
---|---|
Stage #1: formaldehyd With triethylamine; magnesium chloride In tetrahydrofuran for 0.166667h; Inert atmosphere; Stage #2: 4-bromo-phenol In tetrahydrofuran at 75℃; Inert atmosphere; regioselective reaction; | 91% |
With triethylamine; magnesium chloride In acetonitrile for 8h; Reflux; | 82% |
Stage #1: 4-bromo-phenol With magnesium methanolate at 20℃; for 0.0166667h; Stage #2: formaldehyd at 20℃; for 0.166667h; Stage #3: With sulfuric acid at 20℃; for 0.166667h; regioselective reaction; | 45% |
ethyl (E)-3-(4-bromo-2-formylphenoxy)acrylate
isopropylamine
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; | A 90% B n/a |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; sulfonic acid functionalized silica In diethyl ether; acetonitrile at 20℃; for 1.58333h; | 87% |
With N-Bromosuccinimide; 1,3-di-n-butyl-imidazolium tetrafluoroborate at 28 - 35℃; for 0.0833333h; | 84% |
With 1,4-dioxane dibromide at 20℃; for 0.5h; | 82% |
With perchloric acid; dihydrogen peroxide; potassium bromide; [K(H2O)2][VO2(pyridoxal-benzohydrazide)] In water for 4h; | 36.5% |
salicylaldehyde
A
2-hydroxy-3-bromobenzaldehyde
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With ammonium metavanadate; oxygen; aluminium bromide In 1,4-dioxane at 80℃; for 8h; | A 11% B 86% |
With ammonium metavanadate; aluminum tri-bromide; oxygen In 1,4-dioxane at 80℃; for 8h; | A 11% B 86% |
With perchloric acid; C12H18MoN2O5; dihydrogen peroxide; potassium bromide In methanol; water at 24.84℃; for 0.25h; Catalytic behavior; | |
With perchloric acid; dihydrogen peroxide; potassium bromide In water at 20℃; for 2h; Catalytic behavior; Reagent/catalyst; Solvent; |
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With β‐cyclodextrin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetone at 20℃; for 3h; | 85% |
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; β‐cyclodextrin In water; acetone at 20℃; for 0.416667h; | 85% |
2-hydroxy-5-bromobenzaldehyde oxime
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With 1H-imidazole; [bis(acetoxy)iodo]benzene; Cu(AAOPD) In acetonitrile at 20℃; for 0.2h; | 85% |
5-bromosalicylaldehyde dimethyl acetal
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With β‐cyclodextrin In methanol; water at 50℃; for 10h; | 80% |
Conditions | Yield |
---|---|
With perchloric acid; C72H100N4O7V2; dihydrogen peroxide; potassium bromide In tetrahydrofuran; methanol; water at 25℃; for 12h; Kinetics; Catalytic behavior; Time; Reagent/catalyst; Solvent; | A 13% B 77% |
With perchloric acid; C74H104N4O7V2; dihydrogen peroxide; potassium bromide In tetrahydrofuran; methanol; water at 25℃; for 12h; Catalytic behavior; Reagent/catalyst; Time; | A n/a B 74% |
With dihydrogen peroxide; sodium bromide In acetic acid at 20℃; Green chemistry; | A 40% B 60% |
6-bromo-2,2-dimethylbenzo[1,3]dioxin-4-one
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In dichloromethane at -78℃; for 2h; | 75% |
ethyl (E)-3-(4-bromo-2-formylphenoxy)acrylate
4-amino-phenol
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In acetone at 20℃; for 12h; | A 75% B n/a |
ethyl (E)-3-(4-bromo-2-formylphenoxy)acrylate
sulfanilamide
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; | A 75% B n/a |
Conditions | Yield |
---|---|
With perchloric acid; C36H50ClN2O3V; dihydrogen peroxide; potassium bromide In tetrahydrofuran; methanol; water at 25℃; for 12h; Kinetics; Catalytic behavior; Time; Reagent/catalyst; Solvent; | A 8% B n/a C 73% |
2-benzyloxy-5-bromobenzaldehyde
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid at 80℃; for 1h; | 70% |
salicylaldehyde
A
2-bromo-6-hydroxybenzaldehyde
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trimethylsilyl bromide; bis(4-chlorophenyl)sulfoxide In acetonitrile at 25℃; for 6h; Inert atmosphere; regioselective reaction; | A n/a B 70% |
2-hydroxy-5-bromobenzaldehyde oxime
A
5-bromosalicyclic acid
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With calcium hypochlorite; montmorillonite K-10 In chloroform at 20℃; for 4h; | A 2.5% B 69% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 0.0666667h; Reimer-Tiemann reaction; Irradiation; | 60% |
With pyridine; sodium hydroxide at 50 - 60℃; zuletzt bei 100grad; | |
With potassium hydroxide at 25℃; for 15h; Irradiation; or with pyridine; | 17.57 % Chromat. |
Conditions | Yield |
---|---|
With palladium diacetate; toluene-4-sulfonic acid; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; acetic acid; 2-Amino-4-chlorobenzoic acid at 90℃; for 24h; Sealed tube; | 56% |
ethyl (E)-3-(4-bromo-2-formylphenoxy)acrylate
benzaldehyde
p-toluidine
A
C29H30NO7Br
B
diethyl 1-(4-methylphenyl)-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate
C
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 3h; | A 55% B 40% C n/a |
ethyl (E)-3-(4-bromo-2-formylphenoxy)acrylate
p-aminoethylbenzoate
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; | A 50% B n/a |
4-bromo-phenol
hexamethylenetetramine
A
2,6-diformyl-4-bromophenol
B
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid at 100℃; for 24h; Duff Aldehyde Synthesis; Inert atmosphere; | A 35% B 25% |
Conditions | Yield |
---|---|
With bromine |
Conditions | Yield |
---|---|
With sodium amalgam; boric acid; sodium sulfite | |
Multi-step reaction with 2 steps 1: trifluoroacetic anhydride; trifluoroacetic acid / 48 h / 20 °C 2: 75 percent / diisobutylaluminum hydride / CH2Cl2 / 2 h / -78 °C View Scheme |
Conditions | Yield |
---|---|
With hydroxide In 1,4-dioxane; water at 37℃; Rate constant; Thermodynamic data; var. temp., ΔH(excit.), ΔS)(excit.); |
6H,12H-6,12-epoxydibenzo[b,f][1,5]dioxocine
bromine
acetic acid
A
3,5-Dibromosalicylaldehyde
B
5-bromosalicyclaldehyde
ethyl acetoacetate
5-bromosalicyclaldehyde
3-Acetyl-6-bromo-chromen-2-one
Conditions | Yield |
---|---|
With piperidine In ethanol at 80℃; for 0.0166667h; Knoevenagel Condensation; Microwave irradiation; Green chemistry; | 100% |
With zinc oxide nanoparticle at 120℃; under 7200.72 Torr; for 0.1h; Knoevenagel condensation; Microwave irradiation; Neat (no solvent); | 95% |
With piperidine In acetonitrile at 20℃; for 4h; Knoevenagel Condensation; | 94.1% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran | 100% |
With sodium tetrahydroborate; Dowex1-x8 In tetrahydrofuran at 20℃; for 0.01h; | 98% |
With sodium tetrahydroborate; ethanol at 0 - 5℃; for 2h; Reagent/catalyst; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1.5h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 2h; | 99% |
With potassium carbonate In N,N-dimethyl-formamide | 97% |
5-methylisoxazol-3-ylamine
5-bromosalicyclaldehyde
4-bromo-2-[(5-methyl-3-isoxazolyl)imino]methylphenol
Conditions | Yield |
---|---|
Reflux; | 100% |
In ethanol for 2h; Reflux; | 95% |
In ethanol Heating; |
ethyl bromoacetate
5-bromosalicyclaldehyde
methyl (4-bromo-2-formylphenoxy)acetate
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide for 15h; Ambient temperature; | 100% |
benzyl bromide
5-bromosalicyclaldehyde
2-benzyloxy-5-bromobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 5-bromosalicyclaldehyde With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 4h; | 100% |
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 60℃; for 4h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide for 18h; Inert atmosphere; | 99% |
1-Chloro-4-(chloromethyl)benzene
5-bromosalicyclaldehyde
5-bromo-2-((4-chlorobenzyl)oxy)benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 0.5h; Stage #2: 1-Chloro-4-(chloromethyl)benzene In DMF (N,N-dimethyl-formamide) at 65℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 4h; | 98% |
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere; | 98.9% |
With caesium carbonate In N,N-dimethyl-formamide at 60℃; for 2h; |
Conditions | Yield |
---|---|
In ethanol for 3h; Heating; | 100% |
p-methoxybenzyl chloride
5-bromosalicyclaldehyde
3-bromo-6-((4-methoxybenzyl)oxy)benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 60℃; for 3h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 4h; | 83% |
With caesium carbonate In N,N-dimethyl-formamide at 60℃; for 2h; | |
With potassium carbonate In N,N-dimethyl-formamide at 60℃; | |
Stage #1: 5-bromosalicyclaldehyde With sodium hydride In dichloromethane at 20℃; for 0.5h; Stage #2: p-methoxybenzyl chloride In dichloromethane at 20℃; for 16h; |
5-bromosalicyclaldehyde
2-(bromomethyl)-1,3,5-trifluorobenzene
5-bromo-2-(2,4,6-trifluorobenzyloxy)-benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 55℃; | 100% |
methanol
5-bromosalicyclaldehyde
5-bromosalicylaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With sodium tetrahydroborate at 0 - 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 48h; Inert atmosphere; | 93% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 48h; | 93% |
With potassium carbonate In water; N,N-dimethyl-formamide |
5-bromosalicyclaldehyde
trimethyl orthoformate
5-bromosalicylaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol at 20℃; for 1h; | 100% |
With toluene-4-sulfonic acid for 24h; Heating / reflux; | 89% |
With Amberlyst 15 resin In methanol at 20℃; for 20h; Inert atmosphere; | |
With Amberlyst 15 In methanol at 20℃; for 20h; |
2-(tert-butyldimethylsilyloxy)ethyl bromide
5-bromosalicyclaldehyde
5-bromo-2-(2-(tert-butyldimethylsilyloxy)ethoxy)benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 16h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 20h; Inert atmosphere; | 73% |
2-methylpropylmagnesium chloride
5-bromosalicyclaldehyde
4-bromo-2-(1-hydroxy-2-methylpropyl)phenol
Conditions | Yield |
---|---|
Stage #1: 2-methylpropylmagnesium chloride; 5-bromosalicyclaldehyde In tetrahydrofuran; diethyl ether at 20℃; for 0.25h; Stage #2: With hydrogenchloride; water; ammonium chloride In tetrahydrofuran; methanol; diethyl ether | 100% |
propargyl bromide
5-bromosalicyclaldehyde
5-bromo-2-prop-2-ynyloxy-benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 100% |
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.333333h; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; | 97% |
With potassium carbonate In acetonitrile at 20℃; for 24h; | 95% |
methanol
5-bromosalicyclaldehyde
trimethyl orthoformate
5-bromosalicylaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; for 1h; | 100% |
5-bromosalicyclaldehyde
cyanomethyl bromide
2-(4-bromo-2-formylphenoxy)acetonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; | 100% |
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.25h; Inert atmosphere; Stage #2: cyanomethyl bromide In N,N-dimethyl-formamide Inert atmosphere; | 82% |
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 8h; | 73% |
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.25h; Inert atmosphere; Stage #2: cyanomethyl bromide In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere; | |
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.25h; Inert atmosphere; Stage #2: cyanomethyl bromide In N,N-dimethyl-formamide at 20℃; |
1-(2-chloroethyl)pyrrolidine hydrochloride
5-bromosalicyclaldehyde
5-bromo-2-(2-(pyrrolidin-1-yl)ethoxy)benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 5-bromosalicyclaldehyde With potassium carbonate In tetrahydrofuran at 20℃; for 0.25h; Stage #2: 1-(2-chloroethyl)pyrrolidine hydrochloride In tetrahydrofuran at 80℃; for 12h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 2h; | 22% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
Stage #1: 5-bromosalicyclaldehyde With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.25h; Inert atmosphere; Stage #2: methyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 21℃; Inert atmosphere; | 98% |
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 15h; | 98% |
3-bromo-2-phenylprop-1-ene
5-bromosalicyclaldehyde
5-bromo-2-(2-phenylallyloxy)benzaldehyde
Conditions | Yield |
---|---|
With (Z)-β-bromo-α-methylstyrene; potassium carbonate In N,N-dimethyl-formamide at 20℃; for 13h; Inert atmosphere; | 100% |
2-amino-1-benzylamine
5-bromosalicyclaldehyde
4-bromo-2-[2-(5-bromo-2-hydroxybenzylideneaminomethyl)phenyliminomethyl]phenol
Conditions | Yield |
---|---|
In methanol Warming; | 100% |
In methanol Reflux; | 87.9% |
N-isopropylethane-1,2-diamine
5-bromosalicyclaldehyde
4-bromo-2-[(2-isopropylaminoethylimino)methyl]phenol
Conditions | Yield |
---|---|
In methanol | 100% |
In methanol at 20℃; for 0.166667h; | 95% |
2-cyano-N-cyclohexylacetamide
5-bromosalicyclaldehyde
6-bromo-N-cyclohexyl-2-imino-2H-chromene-3-carboxamide
Conditions | Yield |
---|---|
With sodium carbonate In water at 20℃; | 100% |
With 42H3N*42H(1+)*72Mo(6+)*60Mo(5+)*372O(2-)*72H2O*30C2H3O2(1-) In neat (no solvent) at 110℃; for 0.166667h; Green chemistry; | 90% |
2-(2-Aminoethylamino)ethanol
5-bromosalicyclaldehyde
4-bromo-2-[(2-(2-hydroxyethylamino)ethylimino)methyl]phenol
Conditions | Yield |
---|---|
In methanol | 100% |
N,N-diethylethylenediamine
5-bromosalicyclaldehyde
2-(2-(diethylamino)ethyliminomethyl)-4-bromophenol
Conditions | Yield |
---|---|
In methanol | 100% |
In methanol for 1h; Reflux; | |
In acetonitrile for 1h; |
cyclopropylcarbinyl bromide
5-bromosalicyclaldehyde
5-bromo-2-(cyclopropylmethoxy)benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In tetrahydrofuran at 70℃; for 40h; Inert atmosphere; Reflux; | 83% |
tert-butyldimethylsilyl chloride
5-bromosalicyclaldehyde
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; | 100% |
With 1H-imidazole In dichloromethane at 20℃; Schlenk technique; | |
With 1H-imidazole In dichloromethane at 0℃; Sealed tube; |
ethylenediamine
5-bromosalicyclaldehyde
2-[(2-aminoethylimino)methyl]-4-bromophenol
Conditions | Yield |
---|---|
In methanol for 0.5h; | 100% |
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